ChemicalBook > CAS DataBase List > 3-((2,2,2- trifluoroethyl)thio)aniline

3-((2,2,2- trifluoroethyl)thio)aniline

Product Name
3-((2,2,2- trifluoroethyl)thio)aniline
CAS No.
1445684-99-0
Chemical Name
3-((2,2,2- trifluoroethyl)thio)aniline
Synonyms
NA12878;CarolGold;PBA-PEG-AC;WKPep Erasin;Palm-Glu-OtBu;Fmoc-D-Ala-Ala-OH;CarolGold (Lutein);Magnolol & Honokiol;BOC-(D)-HIS(TRT)-AIB;Octa(OtBu)-D-Glu-OtBu
CBNumber
CB71459710
Molecular Formula
C8H8F3NS
Formula Weight
207.22
MOL File
1445684-99-0.mol
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3-((2,2,2- trifluoroethyl)thio)aniline Property

InChI
InChI=1S/C8H8F3NS/c9-8(10,11)5-13-7-3-1-2-6(12)4-7/h1-4H,5,12H2
InChIKey
KMYQCBMXXMOPSD-UHFFFAOYSA-N
SMILES
C1(N)=CC=CC(SCC(F)(F)F)=C1
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

chempep
Product number
181931
Product name
Boc-His(Trt)-Aib-Glu(OtBu)-Gly-OH
Packaging
1g
Price
$300
Updated
2021/12/16
Iris Biotech GmbH
Product number
FAA7750
Product name
Fmoc-D-Lys(Palm-D-Glu-OtBu)-OH
Packaging
1g
Price
$607.5
Updated
2021/12/16
chempep
Product number
181931
Product name
Boc-His(Trt)-Aib-Glu(OtBu)-Gly-OH
Packaging
5g
Price
$900
Updated
2021/12/16
chempep
Product number
181931
Product name
Boc-His(Trt)-Aib-Glu(OtBu)-Gly-OH
Packaging
25g
Price
$2000
Updated
2021/12/16
Iris Biotech GmbH
Product number
FAA7750
Product name
Fmoc-D-Lys(Palm-D-Glu-OtBu)-OH
Packaging
5G
Price
$2160
Updated
2021/12/16
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3-((2,2,2- trifluoroethyl)thio)aniline Chemical Properties,Usage,Production

Uses

3-((2,2,2-trifluoroethyl)thio)aniline can be used as an intermediate in pharmaceutical research.

Synthesis

To a solution of 3-aminobenzenethiol (4.43 g, 35.4 mmol) in THF (225 mL) was added sodium hydride (1.77 g, 44.3 mmol) at 0 °C and stirred for 30 min. Then, 2,2,2-trifluoroethyl 4- methylbenzenesulfonate (9.0 g, 35.4 mmol) was added and the reaction mixture was stirred for 18 h. The reaction mixture was quenched with water (20 mL) and extracted with EtOAc (2x50 mL). The combined organic extracts were washed with water, dried over Na2SO4, fdtered, and concentrated under reduced pressure. The crude residue was purified by flash chromatography through a Redi-Sep pre-packed silica gel column, eluting with a gradient of 5 % to 10 % EtOAc in hexanes, to give 3-((2,2,2- trifluoroethyl)thio)aniline (5 g, 68 % yield) as a pale brown oil.

3-((2,2,2- trifluoroethyl)thio)aniline Preparation Products And Raw materials

Raw materials

Preparation Products

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3-((2,2,2- trifluoroethyl)thio)aniline Suppliers

Chengdu Pukang Biotechnology Co., Ltd
Tel
028-82550498 19102685862
Fax
086-28-82550468
Email
sales@pu-kang.com
Country
China
ProdList
485
Advantage
58
Deyang Yuehe Bio-Pharmaceutical Co.,Ltd
Tel
028-82729560 18030702676
Fax
028-82729560
Email
sales@yuehepharm.com
Country
China
ProdList
179
Advantage
58
Taizhou GreenChem Pharmaceutical Co., Ltd.
Tel
0514-86654616 15366892466
Email
greenchem@tzglmk.com
Country
China
ProdList
498
Advantage
56
ATK CHEMICAL COMPANY LIMITED
Tel
021-51619050 13301662590
Fax
+86-21-51619052
Email
mandy@atkchemical.com
Country
China
ProdList
8026
Advantage
55
Tianjin Kailiqi Biotechnology Co., Ltd.
Tel
15076683720
Fax
022-23754520
Email
klq@cw-bio.com
Country
China
ProdList
4602
Advantage
55
Wuxi Asia Peptide Biotechnology Limited Company
Tel
0510-83583050 13771062561
Fax
0510-83583039
Email
willsun@peptide-search.com
Country
China
ProdList
6716
Advantage
58
XinYao(Shenzhen) Biological Technology Co., Ltd.
Tel
0755-89880280
Fax
0755-89880280
Email
3004662104@qq.com
Country
China
ProdList
1829
Advantage
58
Hangzhou Peptidego Biotech Co.,Ltd.
Tel
0571-87213919
Fax
0571-87213919
Email
Eric@peptidego.com
Country
China
ProdList
6756
Advantage
58
PI & PI BIOTECH INC.
Tel
020-81716320 17788709170
Fax
020-81716319
Email
Sales@pipitech.com
Country
China
ProdList
2649
Advantage
58
Shenzhen Readline Biotech CO., LTD.
Tel
0755-26659310 15915457431
Fax
0755-26659310
Email
linkunsheng@szreadline.com
Country
China
ProdList
110
Advantage
58
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View Lastest Price from 3-((2,2,2- trifluoroethyl)thio)aniline manufacturers

Career Henan Chemical Co
Product
4-Chluoro-2-bromotoluene 1445684-99-0
Price
US $1.00/ASSAYS
Min. Order
1ASSAYS
Purity
98%
Supply Ability
1kg,2kg,100kg
Release date
2019-07-09

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