ChemicalBook > CAS DataBase List > 2-CHLORO-6-NITROQUINOLINE

2-CHLORO-6-NITROQUINOLINE

Product Name
2-CHLORO-6-NITROQUINOLINE
CAS No.
29969-57-1
Chemical Name
2-CHLORO-6-NITROQUINOLINE
Synonyms
2-chlor-6-nitro-chinolin;2-CHLORO-6-NITROQUINOLINE;Quinoline, 2-chloro-6-nitro-
CBNumber
CB71490890
Molecular Formula
C9H5ClN2O2
Formula Weight
208.6
MOL File
29969-57-1.mol
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2-CHLORO-6-NITROQUINOLINE Property

Melting point:
236-237 ºC
Boiling point:
363.4±22.0 °C(Predicted)
Density 
1.484
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
-1.42±0.43(Predicted)
form 
solid
color 
Grey
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Safety

HS Code 
2933499090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific
Product number
OR927639
Product name
2-Chloro-6-nitroquinoline
Purity
97%
Packaging
250mg
Price
$72
Updated
2021/12/16
Apolloscientific
Product number
OR927639
Product name
2-Chloro-6-nitroquinoline
Purity
97%
Packaging
1g
Price
$158
Updated
2021/12/16
Matrix Scientific
Product number
118923
Product name
2-Chloro-6-nitroquinoline
Purity
95+%
Packaging
1g
Price
$235
Updated
2021/12/16
Apolloscientific
Product number
OR927639
Product name
2-Chloro-6-nitroquinoline
Purity
97%
Packaging
5g
Price
$472
Updated
2021/12/16
AK Scientific
Product number
W5240
Product name
2-Chloro-6-nitroquinoline
Packaging
5g
Price
$531
Updated
2021/12/16
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2-CHLORO-6-NITROQUINOLINE Chemical Properties,Usage,Production

Synthesis Reference(s)

The Journal of Organic Chemistry, 67, p. 7884, 2002 DOI: 10.1021/jo016196i

Synthesis

22246-16-8

29969-57-1

Step 4 Synthesis of 2-chloro-6-nitroquinoline: To a solution of 6-nitro-3,4-dihydroquinolin-2(1H)-one (8.2 g, 41.9 mmol) in benzene (150 mL) was added DDQ (9.6 g, 42.5 mmol) and phosphorus triclosan (20.5 mL) sequentially, and the homogeneity of the reaction system was maintained during dropwise addition. The reaction mixture was heated to 90 °C with continuous stirring for 3 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the reaction was subsequently quenched by slowly pouring into 500 mL of ice water. The pH was adjusted to 7 with 4N NaOH solution. extraction was carried out with ethyl acetate (3 x 1 L) and the organic phases were combined. The organic phase was concentrated under reduced pressure to give 8.4 g of 2-chloro-6-nitroquinoline in yellow solid form in 95% yield.

References

[1] Heterocycles, 1998, vol. 48, # 12, p. 2637 - 2641
[2] Patent: US2007/27184, 2007, A1. Location in patent: Page/Page column 18; 25
[3] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 20, p. 5270 - 5274
[4] Patent: KR101576386, 2015, B1. Location in patent: Paragraph 0190; 0193-0194

2-CHLORO-6-NITROQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-6-NITROQUINOLINE Suppliers

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View Lastest Price from 2-CHLORO-6-NITROQUINOLINE manufacturers

PUSHAN INDUSTRIAL (SHAANXI) CO.,LTD
Product
2-chloro-6-nitroquinoline 29969-57-1
Price
US $0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
500kgs
Release date
2024-05-15
Career Henan Chemical Co
Product
2-CHLORO-6-NITROQUINOLINE 29969-57-1
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
Customized
Release date
2019-12-18

29969-57-1, 2-CHLORO-6-NITROQUINOLINERelated Search:

4-Chloro-3-nitroquinoline 6-NITROQUINOLINE

  • 2-CHLORO-6-NITROQUINOLINE
  • Quinoline, 2-chloro-6-nitro-
  • 2-chlor-6-nitro-chinolin
  • 29969-57-1