ChemicalBook > CAS DataBase List > 2-BROMODIPHENYLMETHANE

2-BROMODIPHENYLMETHANE

Product Name: 2-BROMODIPHENYLMETHANE
CAS No.: 23450-18-2
Chemical Name: 2-BROMODIPHENYLMETHANE
Synonyms: 2-BROMODIPHENYLMETHANE;1-bromo-2-(phenylmethyl)benzene;Benzene, 1-bromo-2-(phenylmethyl)-
CBNumber: CB7150649
Molecular Formula: C13H11Br
Formula Weight: 247.13
MOL File: 23450-18-2.mol

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2-BROMODIPHENYLMETHANE Property

Boiling point:: 109 °C
Density: 1.34
storage temp.: Store at room temperature
form: solid
Specific Gravity: 1.34
Appearance: Colorless to light yellow Liquid
CAS DataBase Reference: 23450-18-2(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HazardClass: IRRITANT
HS Code: 2902900000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B699588
Product name: 2-Bromodiphenylmethane
Packaging: 10mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 1700-9-06
Product name: 2-Bromodiphenylmethane
Purity: 98%
Packaging: 1g
Price: $79
Updated: 2021/12/16

AK Scientific

Product number: 7940AD
Product name: 2-Bromodiphenylmethane
Packaging: 1g
Price: $86
Updated: 2021/12/16

Matrix Scientific

Product number: 005721
Product name: 2-Bromodiphenylmethane
Purity: 98%
Packaging: 5g
Price: $118
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0018859
Product name: 2-BROMODIPHENYLMETHANE
Purity: 95.00%
Packaging: 1G
Price: $232.05
Updated: 2021/12/16

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2-BROMODIPHENYLMETHANE Chemical Properties,Usage,Production

Synthesis

5467-74-3

100-44-7

2116-36-1

23450-18-2

The general procedure for the synthesis of 1-benzyl-4-bromobenzene and 1-benzyl-2-bromobenzene from 4-bromophenylboronic acid and benzyl chloride was as follows: to a 10 mL reaction tube fitted with a magnetic stirrer were added (4-bromophenyl)boronic acid (201 mg, 1.0 mmol), lithium tertiary-butanol (80 mg, 1.0 mmol), trifluorotoluene (2 mL) and benzyl chloride (63 mg, 0.5 mmol). After sealing the reaction tube, it was placed in an oil bath at 100 °C and reacted under magnetic stirring for 24 hours. After completion of the reaction, the reaction mixture was cooled to room temperature and the organic solvent was removed by rotary evaporator. The crude product was purified by column chromatography to give a mixture of 1-benzyl-4-bromobenzene and 1-benzyl-2-bromobenzene (82 mg, 63% yield). The mixture was a colorless oily liquid.

References

[1] Patent: CN106478326, 2017, A. Location in patent: Paragraph 0098; 0099; 0100; 0101; 0102
[2] Tetrahedron, 2016, vol. 72, # 49, p. 8022 - 8030

2-BROMODIPHENYLMETHANE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-BROMODIPHENYLMETHANE manufacturers

Career Henan Chemical Co

Product: 2-BROMODIPHENYLMETHANE 23450-18-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%
Supply Ability: 500kg
Release date: 2018-08-19

23450-18-2, 2-BROMODIPHENYLMETHANERelated Search:

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2-BROMODIPHENYLMETHANE

1-bromo-2-(phenylmethyl)benzene

Benzene, 1-bromo-2-(phenylmethyl)-

23450-18-2

23450-18-0

ARYL HALIDE