2-BROMODIPHENYLMETHANE
- Product Name
- 2-BROMODIPHENYLMETHANE
- CAS No.
- 23450-18-2
- Chemical Name
- 2-BROMODIPHENYLMETHANE
- Synonyms
- 2-BROMODIPHENYLMETHANE;1-bromo-2-(phenylmethyl)benzene;Benzene, 1-bromo-2-(phenylmethyl)-
- CBNumber
- CB7150649
- Molecular Formula
- C13H11Br
- Formula Weight
- 247.13
- MOL File
- 23450-18-2.mol
2-BROMODIPHENYLMETHANE Property
- Boiling point:
- 109 °C
- Density
- 1.34
- storage temp.
- Store at room temperature
- form
- solid
- Specific Gravity
- 1.34
- Appearance
- Colorless to light yellow Liquid
- CAS DataBase Reference
- 23450-18-2(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HazardClass
- IRRITANT
- HS Code
- 2902900000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B699588
- Product name
- 2-Bromodiphenylmethane
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 005721
- Product name
- 2-Bromodiphenylmethane
- Purity
- 98%
- Packaging
- 1g
- Price
- $27
- Updated
- 2021/12/16
- Product number
- 1700-9-06
- Product name
- 2-Bromodiphenylmethane
- Purity
- 98%
- Packaging
- 250mg
- Price
- $43
- Updated
- 2021/12/16
- Product number
- 1700-9-06
- Product name
- 2-Bromodiphenylmethane
- Purity
- 98%
- Packaging
- 1g
- Price
- $79
- Updated
- 2021/12/16
- Product number
- 7940AD
- Product name
- 2-Bromodiphenylmethane
- Packaging
- 1g
- Price
- $86
- Updated
- 2021/12/16
2-BROMODIPHENYLMETHANE Chemical Properties,Usage,Production
Synthesis
5467-74-3
100-44-7
2116-36-1
23450-18-2
The general procedure for the synthesis of 1-benzyl-4-bromobenzene and 1-benzyl-2-bromobenzene from 4-bromophenylboronic acid and benzyl chloride was as follows: to a 10 mL reaction tube fitted with a magnetic stirrer were added (4-bromophenyl)boronic acid (201 mg, 1.0 mmol), lithium tertiary-butanol (80 mg, 1.0 mmol), trifluorotoluene (2 mL) and benzyl chloride (63 mg, 0.5 mmol). After sealing the reaction tube, it was placed in an oil bath at 100 °C and reacted under magnetic stirring for 24 hours. After completion of the reaction, the reaction mixture was cooled to room temperature and the organic solvent was removed by rotary evaporator. The crude product was purified by column chromatography to give a mixture of 1-benzyl-4-bromobenzene and 1-benzyl-2-bromobenzene (82 mg, 63% yield). The mixture was a colorless oily liquid.
References
[1] Patent: CN106478326, 2017, A. Location in patent: Paragraph 0098; 0099; 0100; 0101; 0102
[2] Tetrahedron, 2016, vol. 72, # 49, p. 8022 - 8030
2-BROMODIPHENYLMETHANE Preparation Products And Raw materials
Raw materials
Preparation Products
2-BROMODIPHENYLMETHANE Suppliers
- Tel
- +91-22-26355700
- Fax
- +91-22-26355701
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- Country
- India
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- Advantage
- 58
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- India
- ProdList
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View Lastest Price from 2-BROMODIPHENYLMETHANE manufacturers
- Product
- 2-BROMODIPHENYLMETHANE 23450-18-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95%
- Supply Ability
- 500kg
- Release date
- 2018-08-19