5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER
- Product Name
- 5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER
- CAS No.
- 57800-76-7
- Chemical Name
- 5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER
- Synonyms
- Ethyl 5-chloro-4-nitrothiophene-2-carboxylate;Methyl 5-chloro-4-nitrothiophene-2-carboxylate;AKOS 91745;Methyl 5-chloro-4-nitro-2-thiophenecarboxylate;5-Chlor-4-nitro-2-thiophencarbonsaeureMethylester;5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER;2-Thiophenecarboxylic acid, 5-chloro-4-nitro-, methyl ester;5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER, 95+%
- CBNumber
- CB7160152
- Molecular Formula
- C6H4ClNO4S
- Formula Weight
- 221.62
- MOL File
- 57800-76-7.mol
5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER Property
- Melting point:
- 83-84 °C
- Boiling point:
- 349.3±37.0 °C(Predicted)
- Density
- 1.576±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- Appearance
- White to light brown Solid
Safety
- HS Code
- 2934999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M219958
- Product name
- Methyl5-Chloro-4-nitrothiophene-2-carboxylate
- Packaging
- 500mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- W7113
- Product name
- Ethyl5-chloro-4-nitrothiophene-2-carboxylate
- Packaging
- 1g
- Price
- $161
- Updated
- 2021/12/16
- Product number
- W7113
- Product name
- Ethyl5-chloro-4-nitrothiophene-2-carboxylate
- Packaging
- 5g
- Price
- $377
- Updated
- 2021/12/16
- Product number
- COR0003335
- Product name
- 5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $831.6
- Updated
- 2021/12/16
- Product number
- COR0003335
- Product name
- 5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $1519.98
- Updated
- 2021/12/16
5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER Chemical Properties,Usage,Production
Synthesis
35475-03-7
57800-76-7
Step 2: Preparation of methyl 5-chloro-4-nitrothiophene-2-carboxylate Fuming nitric acid (15 mL) was placed in an ice bath and cooled with saturated brine. Methyl 5-chlorothiophene-2-carboxylate (4.99 g, 28.3 mmol) was added slowly in small batches to avoid violent reaction. After addition, the reaction mixture was stirred in an ice bath for 1 hour. Upon completion of the reaction, the mixture was poured into ice water and a solid was precipitated. The precipitate was collected by filtration, washed with water and dried under vacuum to afford methyl 5-chloro-4-nitrothiophene-2-carboxylate (3.88 g, 58% yield). The product was characterized by 1H-NMR (400 MHz, DMSO-d6): δ 8.17 (1H, s).
References
[1] Patent: EP1688420, 2006, A1. Location in patent: Page/Page column 122
[2] Patent: CN107903208, 2018, A. Location in patent: Paragraph 0136; 0137; 0139
[3] Journal of the American Chemical Society, 1952, vol. 74, p. 2965,2969
5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER Suppliers
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- Country
- India
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View Lastest Price from 5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER manufacturers
- Product
- 5-CHLORO-4-NITROTHIOPHENE-2-CARBOXYLIC ACID METHYL ESTER 57800-76-7
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 1000KGS
- Release date
- 2020-01-14