4,4-Diethoxy-N,N-dimethyl-1-butanamine
- Product Name
- 4,4-Diethoxy-N,N-dimethyl-1-butanamine
- CAS No.
- 1116-77-4
- Chemical Name
- 4,4-Diethoxy-N,N-dimethyl-1-butanamine
- Synonyms
- 4,4-diethoxy-N,N-diMethylbutan-1-aMine;Zolmitriptan USP RC H;1-Butanamine,4,4-diethoxy-N,N-;Zolmitriptan Related Compound H;4,4-Diethoxy-N-Dimethylbutylamine;(4,4-DIETHOXY-BUTYL)-DIMETHYL-AMINE;4,4-DIETHOXY-N,N-DIMETHYLBUTANAMINE;Zolmitriptan USP Related Compound H;4-DiMethylaMinobutanol diethylacetal;4,4-DIETHOXY-N, N-DIMETHYL-BUTYLAMINE
- CBNumber
- CB7176364
- Molecular Formula
- C10H23NO2
- Formula Weight
- 189.3
- MOL File
- 1116-77-4.mol
4,4-Diethoxy-N,N-dimethyl-1-butanamine Property
- Boiling point:
- 194-195C
- Density
- 0.844 g/mL at 25 °C(lit.)
- refractive index
- n20/D 1.421(lit.)
- Flash point:
- 158 °F
- storage temp.
- 2-8°C
- solubility
- Chloroform, Ethyl Acetate
- form
- Oil
- pka
- 9.71±0.28(Predicted)
- color
- Colourless to Pale Yellow
- CAS DataBase Reference
- 1116-77-4(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,C
- Risk Statements
- 41-34-10-36/37/38
- Safety Statements
- 26-36/37/39-16-37
- RIDADR
- UN 3267 8 / PGIII
- WGK Germany
- 3
- HS Code
- 29225090
N-Bromosuccinimide Price
- Product number
- 647055
- Product name
- 4,4-Diethoxy-N,N-dimethyl-1-butanamine
- Packaging
- 5g
- Price
- $110
- Updated
- 2024/03/01
- Product number
- 1727097
- Product name
- Zolmitriptan Related Compound H
- Purity
- United States Pharmacopeia (USP) Reference Standard
- Packaging
- 50mg
- Price
- $1580
- Updated
- 2024/03/01
- Product number
- D3973
- Product name
- 4-(Dimethylamino)butyraldehyde Diethyl Acetal
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $34
- Updated
- 2024/03/01
- Product number
- D3973
- Product name
- 4-(Dimethylamino)butyraldehyde Diethyl Acetal
- Purity
- >98.0%(GC)(T)
- Packaging
- 25g
- Price
- $92
- Updated
- 2024/03/01
- Product number
- B24686
- Product name
- 4-Dimethylaminobutyraldehyde diethyl acetal, 97%
- Packaging
- 100g
- Price
- $100
- Updated
- 2021/12/16
4,4-Diethoxy-N,N-dimethyl-1-butanamine Chemical Properties,Usage,Production
Chemical Properties
Light yellow liquid
Uses
4,4-Diethoxy-N,N-dimethyl-1-butanamine is used in organic synthesis and pharmaceutical intermediates, it is an intermediate for Sumatriptan, Rizatriptan, Almotriptan, Zolmitriptan.
Application
4-Dimethylaminobutyraldehyde Diethyl Acetal (Zolmitriptan USP Related Compound H) is used in the preparation of N,N-Dimethyltryptamines, 5-HT1D receptor agonists, for medicinal treatments such as antimigraine drugs.
Preparation
4-Dimethylaminobutyraldehyde diethyl acetal synthesis: The reaction of 1-bromo-3-chloro propane and dimethylamine solution with PEG as a phase transfer catalyst, and obtained 3-dimethylamino-1-chloro propane. 3-dimethylamino-1-chloro propane reacted with magnesium and Grinard reagent was acquired. 4-Dimethylaminobutyraldehyde diethyl acetal is obtained by the reaction of Grinard reagent and triethyl orthoformate. The yield was 70.11%.
Synthesis Reference(s)
Tetrahedron Letters, 35, p. 2401, 1994 DOI: 10.1016/0040-4039(94)85230-8
4,4-Diethoxy-N,N-dimethyl-1-butanamine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4,4-Diethoxy-N,N-dimethyl-1-butanamine manufacturers
- Product
- 4,4-Diethoxy-N,N-dimethyl-1-butanamine 1116-77-4
- Price
- US $5.00-2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10000kg
- Release date
- 2024-08-15
- Product
- 4,4-Diethoxy-N,N-dimethyl-1-butanamine 1116-77-4
- Price
- US $0.10/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10
- Release date
- 2024-07-14
- Product
- 4,4-Diethoxy-N,N-dimethyl-1-butanamine 1116-77-4
- Price
- US $0.00-0.00/KG
- Min. Order
- 50KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2022-09-30