2-CHLORO-3-METHOXYPHENOL

Product Name: 2-CHLORO-3-METHOXYPHENOL
CAS No.: 72232-49-6
Chemical Name: 2-CHLORO-3-METHOXYPHENOL
Synonyms: KML-88;KML-57;2-CHLORO-3-METHOXYPHENOL;Phenol, 2-chloro-3-methoxy-;2-Chloro-3-methoxyphenol 98%
CBNumber: CB7185517
Molecular Formula: C7H7ClO2
Formula Weight: 158.58
MOL File: 72232-49-6.mol

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2-CHLORO-3-METHOXYPHENOL Property

storage temp.: Sealed in dry,Room Temperature
Appearance: Off-white to yellow Solid

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Safety

Risk Statements: 41
Safety Statements: 26-39
HS Code: 2909500090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C368248
Product name: 2-Chloro-3-methoxyphenol
Packaging: 50mg
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC139619
Product name: 2-Chloro-3-methoxyphenol
Packaging: 1g
Price: $74
Updated: 2021/12/16

Apolloscientific

Product number: OR399014
Product name: 2-Chloro-3-methoxyphenol
Purity: 98%
Packaging: 1g
Price: $76
Updated: 2021/12/16

Matrix Scientific

Product number: 071966
Product name: 2-Chloro-3-methoxyphenol
Purity: 95+%
Packaging: 1g
Price: $85
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC139619
Product name: 2-Chloro-3-methoxyphenol
Packaging: 2g
Price: $129
Updated: 2021/12/16

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2-CHLORO-3-METHOXYPHENOL Chemical Properties,Usage,Production

Synthesis

6201-65-6

77-78-1

72232-49-6

A) General procedure for synthesizing 2-chloro-3-methoxyphenol: 2-chloro-1,3-benzenediol (22.8 g) was added to an aqueous solution (100 mL) of potassium hydroxide (11.0 g). Subsequently, dimethyl sulfate (19.9 g) was slowly added while maintaining the temperature of the reaction mixture at 10 °C to 20 °C. The reaction mixture was stirred at 100 °C for 2 days. After completion of the reaction, the reaction mixture was acidified with 2N hydrochloric acid and extracted with dichloromethane. The organic layer was dried with anhydrous sodium sulfate and evaporated under reduced pressure to remove the solvent. The residue was purified by silica gel column chromatography (eluent: ethyl acetate/petroleum ether) to afford the target product 2-chloro-3-methoxyphenol (18.0 g). The product was characterized by 1H NMR (400 MHz, DMSO-d6) with chemical shifts of δ 3.78 (3H, s), 6.54-6.58 (2H, m), 7.05 (1H, t, J = 8.4 Hz), 10.04 (1H, brs).

References

[1] Patent: WO2015/163485, 2015, A1. Location in patent: Paragraph 0411

2-CHLORO-3-METHOXYPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-3-METHOXYPHENOL Suppliers

China 77 India 1 United Kingdom 3 United States 11 Global 92

Shanghai Harvest Chemical Industrial Co., Ltd.

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T&W GROUP

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Bide Pharmatech Ltd.

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View Lastest Price from 2-CHLORO-3-METHOXYPHENOL manufacturers

Career Henan Chemical Co

Product: 2-CHLORO-3-METHOXYPHENOL 72232-49-6
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: JD 648
Release date: 2019-09-01

72232-49-6, 2-CHLORO-3-METHOXYPHENOLRelated Search:

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2-CHLORO-3-METHOXYPHENOL

2-Chloro-3-methoxyphenol 98%

Phenol, 2-chloro-3-methoxy-

KML-57

KML-88

72232-49-6