5-bromo-1H-pyrazolo[3,4-c]pyridine

Product Name: 5-bromo-1H-pyrazolo[3,4-c]pyridine
CAS No.: 929617-35-6
Chemical Name: 5-bromo-1H-pyrazolo[3,4-c]pyridine
Synonyms: 4-c]pyridine;6-Aza-5-bromo-1H-indazole;5-BroMo-1H-pyrazolo[3,4-c...;5-bromo-1H-pyrazolo[3,4-c]pyridin;5-bromo-1H-pyrazolo[3,4-c]pyridine;1H-Pyrazolo[3,4-c]pyridine,5-broMo-;5-bromo-1h-pyrazole [3, 4-C] pyridine
CBNumber: CB71856144
Molecular Formula: C6H4BrN3
Formula Weight: 198.02
MOL File: 929617-35-6.mol

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5-bromo-1H-pyrazolo[3,4-c]pyridine Property

Boiling point:: 384.0±22.0 °C(Predicted)
Density: 1.894
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 9.68±0.40(Predicted)
form: powder
color: Yellow

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Safety

Hazard Codes: Xn
Risk Statements: 22
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B698808
Product name: 5-Bromo-1h-pyrazolo[3,4-c]pyridine
Packaging: 250mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-9-T1
Product name: 5-Bromo-1H-pyrazolo[3,4-c]pyridine
Packaging: 250mg
Price: $21
Updated: 2021/12/16

ChemScene

Product number: CS-0006627
Product name: 5-Bromo-1H-pyrazolo[3,4-c]pyridine
Purity: >98.0%
Packaging: 1g
Price: $31
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-9-T1
Product name: 5-Bromo-1H-pyrazolo[3,4-c]pyridine
Packaging: 1g
Price: $53
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB153487
Product name: 5-Bromo-1H-pyrazolo[3,4-c]pyridine
Packaging: 250mg
Price: $60
Updated: 2021/12/16

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5-bromo-1H-pyrazolo[3,4-c]pyridine Chemical Properties,Usage,Production

Synthesis

156118-16-0

929617-35-6

General procedure for the synthesis of 5-bromo-1H-pyrazolo[3,4-c]pyridine from 2-bromo-4-methyl-5-aminopyridine: to a solution of 2-bromo-4-methyl-5-aminopyridine (4.00 g, 21.4 mmol) in acetic acid (300 ml) was added sodium nitrite (1.48 g, 21.4 mmol) and the reaction mixture was stirred at room temperature overnight. After completion of the reaction, the mixture was concentrated under vacuum. The residue was diluted with ethyl acetate and washed sequentially with saturated aqueous sodium bicarbonate solution and brine. The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent: 0-50% hexane solution of ethyl acetate) to afford 5-bromo-1H-pyrazolo[3,4-c]pyridine as a yellow solid (2.48 g, 59% yield).1H NMR (300 MHz, CDCl3): δ 7.86-7.90 (m,1H), 8.09-8.14 (m,1H) 8.83-8.88 (m, 1H). ms ESI/APCI Dual m/z: 198 [M + H].

References

[1] Bioorganic and Medicinal Chemistry Letters, 2015, vol. 25, # 22, p. 5258 - 5264
[2] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 15, p. 3441 - 3446
[3] Bioorganic and Medicinal Chemistry, 2007, vol. 15, # 6, p. 2441 - 2452
[4] Patent: WO2017/23984, 2017, A1. Location in patent: Paragraph 0611
[5] Patent: WO2017/23980, 2017, A1. Location in patent: Paragraph 0612

5-bromo-1H-pyrazolo[3,4-c]pyridine Preparation Products And Raw materials

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5-bromo-1H-pyrazolo[3,4-c]pyridine Suppliers

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View Lastest Price from 5-bromo-1H-pyrazolo[3,4-c]pyridine manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 5-Bromo-1H-pyrazolo[3,4-c]pyridine 929617-35-6
Price: US $1.10-9.90/KG
Min. Order: 1KG
Purity: 99% min
Supply Ability: 100kg
Release date: 2025-08-18

Career Henan Chemical Co

Product: 5-bromo-1H-pyrazolo[3,4-c]pyridine 929617-35-6
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10000KGS
Release date: 2020-01-09

Career Henan Chemical Co

Product: 5-bromo-1H-pyrazolo[3,4-c]pyridine 929617-35-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-08

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