2-CHLORO-5-FLUOROBENZYL ALCOHOL
- Product Name
- 2-CHLORO-5-FLUOROBENZYL ALCOHOL
- CAS No.
- 261762-59-8
- Chemical Name
- 2-CHLORO-5-FLUOROBENZYL ALCOHOL
- Synonyms
- RARECHEM AL BD 1381;2-CHLORO-5-FLUOROBENZYL ALCOHOL;(2-Chloro-5-fluorophenyl)methanol;Benzenemethanol, 2-chloro-5-fluoro-;2-CHLORO-5-FLUOROBENZYL ALCOHOL ISO 9001：2015 REACH
- CBNumber
- CB7229516
- Molecular Formula
- C7H6ClFO
- Formula Weight
- 160.57
- MOL File
- 261762-59-8.mol
2-CHLORO-5-FLUOROBENZYL ALCOHOL Property
- Melting point:
- 68-72°C
- Boiling point:
- 229.6±25.0 °C(Predicted)
- Density
- 1.344±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 13.65±0.10(Predicted)
- Appearance
- White to off-white Solid
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HazardClass
- IRRITANT
- HS Code
- 2906290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- C584920
- Product name
- 2-Chloro-5-fluorobenzylalcohol
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- C584920
- Product name
- 2-Chloro-5-fluorobenzylalcohol
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 005624
- Product name
- 2-Chloro-5-fluorobenzylalcohol
- Packaging
- 5g
- Price
- $60
- Updated
- 2021/12/16
- Product number
- PC0057
- Product name
- 2-Chloro-5-fluorobenzylalcohol
- Purity
- 97%
- Packaging
- 1g
- Price
- $15
- Updated
- 2021/12/16
- Product number
- 2601-7-X0
- Product name
- 2-Chloro-5-fluorobenzyl alcohol
- Purity
- 97%
- Packaging
- 1g
- Price
- $16
- Updated
- 2021/12/16
2-CHLORO-5-FLUOROBENZYL ALCOHOL Chemical Properties,Usage,Production
Synthesis
The synthesis of 2-chloro-5-fluorobenzyl alcohol proceeded as follows:
Step 1: Compound Z-A-1-a (35g, 0.2 mol) was dissolved in methanol (500mL) and concentrated sulfuric acid (5mL) was added slowly. The reaction solution was stirred under the protection of N 2 at 70??C for 18 h. Most of the solvent was spun off, then 200 mL of water was added and extracted with ethyl acetate (3x250 mL), dried and spun dry to obtain the red oily material Z-A-1-b (38 g, 100% yield).
Step 2: Compound Z-A-1-b (38g, 0.2 mol) was dissolved in THF (200mL) and methanol (50mL), sodium borohydride (15.4g, 0.4 mol) was added slowly at 0??C, and the reaction was stirred at room temperature for 2h. The disappearance of the reaction material was monitored by TLC, and the reaction solution was cooled down to 0??C with the addition of 300mL of water, and was extracted with dichloromethane (3x300mL), the organic phase was washed with saturated sodium bicarbonate (500mL), the organic phase was dried and spun dry to obtain a yellow solid 2-chloro-5-fluorobenzyl alcohol (32g, yield 99%).
2-CHLORO-5-FLUOROBENZYL ALCOHOL Preparation Products And Raw materials
Raw materials
Preparation Products
2-CHLORO-5-FLUOROBENZYL ALCOHOL Suppliers
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View Lastest Price from 2-CHLORO-5-FLUOROBENZYL ALCOHOL manufacturers
- Product
- 2-CHLORO-5-FLUOROBENZYL ALCOHOL 261762-59-8
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2020-02-16