2'-Iodoacetophenone
- Product Name
- 2'-Iodoacetophenone
- CAS No.
- 2142-70-3
- Chemical Name
- 2'-Iodoacetophenone
- Synonyms
- 1-(2-Iodophenyl)ethan-1-one;2-IODOACETOPHENONE;1-(2-iodophenyl)ethanone;2-iodophenone;O-IODOACETOPHENONE;2'-IODOACETOPHENONE;2'-Iodoacetophenone;2'-Iodoacetophenone>2''-IODOACETOPHENONE 97%;2'-IODOACETOPHENONE, 99+%
- CBNumber
- CB7291551
- Molecular Formula
- C8H7IO
- Formula Weight
- 246.05
- MOL File
- 2142-70-3.mol
2'-Iodoacetophenone Property
- Boiling point:
- 139-140°C 12mm
- Density
- 1.72 g/mL at 25 °C(lit.)
- refractive index
- n20/D 1.618(lit.)
- Flash point:
- 218 °F
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- Liquid
- Specific Gravity
- 1.720
- color
- Clear yellow
- Sensitive
- Light Sensitive
- BRN
- 2325078
- CAS DataBase Reference
- 2142-70-3(CAS DataBase Reference)
Safety
- Hazard Codes
- C
- Risk Statements
- 36/38
- Safety Statements
- 26-36-24/25
- WGK Germany
- 3
- HazardClass
- IRRITANT
- HS Code
- 29147000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- 540676
- Product name
- 2′-Iodoacetophenone
- Purity
- 97%
- Packaging
- 1g
- Price
- $30.4
- Updated
- 2023/01/07
- Product number
- I0689
- Product name
- 2'-Iodoacetophenone
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $16
- Updated
- 2024/03/01
- Product number
- I0689
- Product name
- 2'-Iodoacetophenone
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $40
- Updated
- 2024/03/01
- Product number
- B25345
- Product name
- 2'-Iodoacetophenone, 98+%
- Packaging
- 1g
- Price
- $32.65
- Updated
- 2024/03/01
- Product number
- B25345
- Product name
- 2'-Iodoacetophenone, 98+%
- Packaging
- 5g
- Price
- $99.65
- Updated
- 2024/03/01
2'-Iodoacetophenone Chemical Properties,Usage,Production
Chemical Properties
Clear yellow liquid
Uses
2′-Iodoacetophenone (2-Iodoacetophenone) may be used in the synthesis of:
indene derivatives
di-(o-acetylphenyl)acetylene
indenol derivative
Preparation
2'-Iodoacetophenone can be synthesized by diazotization of 2-acetylaniline.
To a solution of p-TsOH (22.80 g, 120 mmol) in CH3CN (160 mL) was added an aromatic amine (40 mmol). The resulting amine salt suspension was cooled to 0-5°C. A solution of NaNO2 (5.52 g, 80 mmol) in H2O (12 mL) and KI (16.6 g, 100 mmol) in H2O (12 mL) were added sequentially. The reaction mixture was stirred for 10 minutes, then allowed to warm to ambient temperature and stirred until all the amine was consumed. To the reaction mixture were then added H2O (700 mL), NaHCO3 (1M; until pH=9-10) and Na2S2O3 (2M, 80 mL). The reaction mixture was extracted with EtOAc and purified by column chromatography (hexanes:EtOAc, 9:1 v/v) to give 2'-iodoacetophenone:yellow oil in 94% yield.
Reactions
2'-Iodoacetophenone is a bioactive molecule that reacts with boronic acids to form aryl boronic acid derivatives. This reaction can be carried out in chlorobenzene or dihedral solvents, and it is scalable and applicable to a variety of boronic acids. The product of this reaction is an organocatalyst for the synthesis of bioactive molecules. 2'-Iodoacetophenone also reacts with dipole-containing additives to form dichlorodiphenyldichloroethane, which has been used as a fungicide, insecticide, and herbicide.
General Description
2′-Iodoacetophenone is a halogenated aromatic ketone.
2'-Iodoacetophenone Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2'-Iodoacetophenone manufacturers
- Product
- 2'-Iodoacetophenone 2142-70-3
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- JD 793
- Release date
- 2019-09-02