2'-Iodoacetophenone

Product Name: 2'-Iodoacetophenone
CAS No.: 2142-70-3
Chemical Name: 2'-Iodoacetophenone
Synonyms: 1-(2-Iodophenyl)ethan-1-one;2-IODOACETOPHENONE;1-(2-iodophenyl)ethanone;2-iodophenone;O-IODOACETOPHENONE;2'-Iodoacetophenone;2'-Iodoacetophenone>2''-IODOACETOPHENONE 97%;2'-IODOACETOPHENONE, 99+%;2'-Iodoacetophenone, 98+%
CBNumber: CB7291551
Molecular Formula: C8H7IO
Formula Weight: 246.05
MOL File: 2142-70-3.mol

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2'-Iodoacetophenone Property

Boiling point:: 139-140°C 12mm
Density: 1.72 g/mL at 25 °C(lit.)
refractive index: n20/D 1.618(lit.)
Flash point:: 218 °F
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: Liquid
Specific Gravity: 1.720
color: Clear yellow
Sensitive: Light Sensitive
BRN: 2325078
CAS DataBase Reference: 2142-70-3(CAS DataBase Reference)

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Safety

Hazard Codes: C
Risk Statements: 36/38
Safety Statements: 26-36-24/25
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 29147000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 540676
Product name: 2′-Iodoacetophenone
Purity: 97%
Packaging: 1g
Price: $30.4
Updated: 2023/01/07

TCI Chemical

Product number: I0689
Product name: 2'-Iodoacetophenone
Purity: >98.0%(GC)
Packaging: 1g
Price: $16
Updated: 2024/03/01

TCI Chemical

Product number: I0689
Product name: 2'-Iodoacetophenone
Purity: >98.0%(GC)
Packaging: 5g
Price: $40
Updated: 2024/03/01

Alfa Aesar

Product number: B25345
Product name: 2'-Iodoacetophenone, 98+%
Packaging: 1g
Price: $32.65
Updated: 2024/03/01

Alfa Aesar

Product number: B25345
Product name: 2'-Iodoacetophenone, 98+%
Packaging: 5g
Price: $99.65
Updated: 2024/03/01

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2'-Iodoacetophenone Chemical Properties,Usage,Production

Chemical Properties

Clear yellow liquid

Uses

2′-Iodoacetophenone (2-Iodoacetophenone) may be used in the synthesis of:
indene derivatives
di-(o-acetylphenyl)acetylene
indenol derivative

Preparation

2'-Iodoacetophenone can be synthesized by diazotization of 2-acetylaniline.
To a solution of p-TsOH (22.80 g, 120 mmol) in CH3CN (160 mL) was added an aromatic amine (40 mmol). The resulting amine salt suspension was cooled to 0-5°C. A solution of NaNO2 (5.52 g, 80 mmol) in H2O (12 mL) and KI (16.6 g, 100 mmol) in H2O (12 mL) were added sequentially. The reaction mixture was stirred for 10 minutes, then allowed to warm to ambient temperature and stirred until all the amine was consumed. To the reaction mixture were then added H2O (700 mL), NaHCO3 (1M; until pH=9-10) and Na2S2O3 (2M, 80 mL). The reaction mixture was extracted with EtOAc and purified by column chromatography (hexanes:EtOAc, 9:1 v/v) to give 2'-iodoacetophenone:yellow oil in 94% yield.

Reactions

2'-Iodoacetophenone is a bioactive molecule that reacts with boronic acids to form aryl boronic acid derivatives. This reaction can be carried out in chlorobenzene or dihedral solvents, and it is scalable and applicable to a variety of boronic acids. The product of this reaction is an organocatalyst for the synthesis of bioactive molecules. 2'-Iodoacetophenone also reacts with dipole-containing additives to form dichlorodiphenyldichloroethane, which has been used as a fungicide, insecticide, and herbicide.

General Description

2′-Iodoacetophenone is a halogenated aromatic ketone.

2'-Iodoacetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

Benzoylacetone

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2'-Iodoacetophenone Suppliers

Americas 1 Belgium 1 China 136 Europe 1 Germany 2 India 5 Japan 2 Switzerland 2 The Netherlands 1 United Kingdom 9 United States 19 Global 179

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View Lastest Price from 2'-Iodoacetophenone manufacturers

Career Henan Chemical Co

Product: 2'-Iodoacetophenone 2142-70-3
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: JD 793
Release date: 2019-09-02

2142-70-3, 2'-IodoacetophenoneRelated Search:

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2-IODOACETOPHENONE

O-IODOACETOPHENONE

2''-IODOACETOPHENONE 97%

2'-Iodoacetophenone, 98+%

2'-IODOACETOPHENONE, 99+%

1-(2-iodophenyl)ethanone

Ethanone, 1-(2-iodophenyl)-

1-(2-Iodophenyl)ethan-1-one

1-(2-nitrophenyl)-N-[4-[(E)-(2-nitrophenyl)methylideneamino]-1-piperazinyl]methanimine

2'-Iodoacetophenone&gt

2-iodophenone

2'-Iodoacetophenone

2142-70-3

IC6H4COCH3

Organic Building Blocks

Ketones

Building Blocks

Carbonyl Compounds

C7 to C8

Aromatic Acetophenones & Derivatives (substituted)

Adehydes, Acetals & Ketones

Iodine Compounds

C7 to C8

Carbonyl Compounds

Ketones