3-CHLORO-2-FLUORONITROBENZENE

Product Name: 3-CHLORO-2-FLUORONITROBENZENE
CAS No.: 2106-49-2
Chemical Name: 3-CHLORO-2-FLUORONITROBENZENE
Synonyms: 5-Chloro-2-fluoroaniline;1-CHLORO-2-FLUORO-3-NITRO-BENZENE;3-chioro-2-fluoronitrobenzene;2-Fluoro-3-nitrochlorobenzene;3-CHLORO-2-FLUORONITROBENZENE;2-FLUORO-3-CHLORO-NITROBENZENE;3-Chloro-2-fluoro-1-nitrobenzene;3-CHLORO-2-FLUORONITROBENZENE,99%;Benzene, 1-chloro-2-fluoro-3-nitro-;1-Chloro-2-fluoro-3-nitrobenzene,97%
CBNumber: CB7384301
Molecular Formula: C6H3ClFNO2
Formula Weight: 175.54
MOL File: 2106-49-2.mol

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3-CHLORO-2-FLUORONITROBENZENE Property

Melting point:: 36-40
Boiling point:: 106 °C(Press: 5 Torr)
Density: 1.494±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
form: Liquid
color: Yellow
Water Solubility: Soluble in water.
CAS DataBase Reference: 2106-49-2(CAS DataBase Reference)

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Safety

Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39
RIDADR: 2810
Hazard Note: Harmful
HazardClass: 6.1
PackingGroup: Ⅲ
HS Code: 2904990090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H331Toxic if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: C585060
Product name: 1-Chloro-2-fluoro-3-nitrobenzene
Packaging: 500mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C585060
Product name: 1-Chloro-2-fluoro-3-nitrobenzene
Packaging: 2.5g
Price: $65
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-7-32
Product name: 3-Chloro-2-fluoronitrobenzene
Purity: 98%
Packaging: 1g
Price: $16
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-7-32
Product name: 3-Chloro-2-fluoronitrobenzene
Purity: 98%
Packaging: 5G
Price: $18
Updated: 2021/12/16

Matrix Scientific

Product number: 073102
Product name: 3-Chloro-2-fluoronitrobenzene
Purity: 95+%
Packaging: 25g
Price: $18
Updated: 2021/12/16

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3-CHLORO-2-FLUORONITROBENZENE Chemical Properties,Usage,Production

Uses

1-Chloro-2-fluoro-3-nitrobenzene is used as pharmaceutical intermediates, agrochemical intermediates, intermediates of medicine.

Synthesis

3209-22-1

2106-49-2

General procedure for the synthesis of 3-chloro-2-fluoronitrobenzene from 2,3-dichloronitrobenzene: 500 g (2.08 mol) of 2,3-dichloronitrobenzene was added to a four-necked flask fitted with a stirrer, a thermometer, and a condenser tube, and heated to 140 °C. Subsequently, 112 g (1.93 mol) of potassium fluoride (KF) was added to the reaction system, subjected to a decompression dehydration operation and held at 140-150 °C for 3 hours. After dehydration was completed, the temperature of the reaction system was raised to 140 °C, and then 6.6 g (0.06 mol) of tetramethylammonium chloride was slowly added between 150 and 160 °C. After the addition was completed, the reaction temperature was adjusted to 165±5°C and the reaction was continued for 8 hours. At the end of the reaction, the heating was stopped and the reaction mixture was allowed to cool to room temperature and washed with deionized water. The organic phase was separated and layered by distillation to recover 100 g of unreacted 2,3-dichloronitrobenzene, and finally 240 g of the target product 3-chloro-2-fluoronitrobenzene was obtained, which had a purity of 99.6% and a yield of 87.6%.

References

[1] Patent: CN102249881, 2016, B. Location in patent: Paragraph 0015; 0039-0040
[2] Journal of Medicinal Chemistry, 2001, vol. 44, # 10, p. 1516 - 1529
[3] Journal of the American Chemical Society, 1959, vol. 81, p. 94,95, 97
[4] Patent: US5476976, 1995, A
[5] Patent: US5545768, 1996, A

3-CHLORO-2-FLUORONITROBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-CHLORO-2-FLUORONITROBENZENE Suppliers

China 177 Germany 3 India 2 United Kingdom 7 United States 17 Global 206

J & K SCIENTIFIC LTD.

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View Lastest Price from 3-CHLORO-2-FLUORONITROBENZENE manufacturers

Anhui Zhongda Biotechnology Co., Ltd

Product: 3-CHLORO-2-FLUORONITROBENZENE 2106-49-2
Price: US $10.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100T
Release date: 2023-10-31

Zhuozhou Wenxi import and Export Co., Ltd

Product: 3-CHLORO-2-FLUORONITROBENZENE 2106-49-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-27

Career Henan Chemical Co

Product: 3-CHLORO-2-FLUORONITROBENZENE 2106-49-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-06-25

2106-49-2, 3-CHLORO-2-FLUORONITROBENZENERelated Search:

3-CHLORO-4-FLUORO-5-NITROBENZOTRIFLUORIDE 3-CHLORO-2,4-DIFLUORONITROBENZENE (3-CHLORO-4-FLUORO-5-NITRO)BENZENEBORONIC ACID 3-CHLORO-2-FLUORONITROBENZENE 2,4-Difluoro-3,5-dichloronitrobenzene 3-CHLORO-4-FLUORONITROBENZENE,3-Chloro-4-fluoronitrobenzene98%,3-Chloro-4-fluoronitrobenzene 98% 2,6-DIFLUOROPHENYLACETONITRILE 1-chloro-3-fluoro-5-nitro benzene 5-CHLORO-2-FLUORONITROBENZENE 2-CHLORO-6-FLUORONITROBENZENE 4-CHLORO-2-FLUORONITROBENZENE,4-Chloro-5-fluoronitrobenzene,4-CHLORO-2-FLUORONITROBENZENE 95+% 2-CHLORO-4-FLUORONITROBENZENE,2-CHLORO-4-FLUORONITROBENZENE 98% 1,2-DICHLORO-4-FLUORO-5-NITROBENZENE 4-CHLORO-3-FLUORONITROBENZENE 2,4-Dichloro-5-fluoronitrobenzene 2-Chloro-5-fluoronitrobenzene 99%,2-Chloro-5-fluoronitrobenzene99%,2-CHLORO-5-FLUORONITROBENZENE 2-CHLORO-3-FLUORONITROBENZENE 2-AMINO-3-CHLORO-4-FLUORONITROBENZENE

3-CHLORO-2-FLUORONITROBENZENE

2-FLUORO-3-CHLORO-NITROBENZENE

3-CHLORO-2-FLUORONITROBENZENE / 1-CHLORO-2-FLUORO-3-NITROBENZENE

2-Fluoro-3-nitrochlorobenzene

Benzene, 1-chloro-2-fluoro-3-nitro-

3-Chloro-2-fluoro-1-nitrobenzene

5-Chloro-2-fluoroaniline

1-CHLORO-2-FLUORO-3-NITRO-BENZENE

3-chioro-2-fluoronitrobenzene

1-Chloro-2-fluoro-3-nitrobenzene,97%

3-CHLORO-2-FLUORONITROBENZENE ISO 9001：2015 REACH

3-CHLORO-2-FLUORONITROBENZENE,99%

2106-49-2

FC6H3ClNO2

Fluorine series