ChemicalBook > CAS DataBase List > 1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE

1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE

Product Name: 1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE
CAS No.: 192189-07-4
Chemical Name: 1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE
Synonyms: 1-Boc-3-iodoindole;N-Boc-3-iodoindole;1-Boc-3-iodoindole, 95%;tert-butyl3-iodoindole-1-carboxylate;tert-butyl 3-iodo-1H-indol-1-carboxylate;1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE;1-(Tert-Butoxycarbonyl)-3-iodo-1H-icdole;tert-Butyl 3-iodo-1H-indole-1-carboxylate;3-Iodoindole-1-carboxylic acid tert-butyl ester;3-Iodo-1H-indole-1-carboxylic acid 1,1-dimethylethyl ester
CBNumber: CB7395846
Molecular Formula: C13H14INO2
Formula Weight: 343.16
MOL File: 192189-07-4.mol

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1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE Property

Melting point:: 36-40℃
Boiling point:: 388℃
Density: 1.56
Flash point:: 189℃
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: Light yellow to yellow <36°C Solid,>40°C Liquid
Water Solubility: Insoluble in water.
Sensitive: Light Sensitive
InChI: InChI=1S/C13H14INO2/c1-13(2,3)17-12(16)15-8-10(14)9-6-4-5-7-11(9)15/h4-8H,1-3H3
InChIKey: LOFWPZQNSUAMCV-UHFFFAOYSA-N
SMILES: N1(C(OC(C)(C)C)=O)C2=C(C=CC=C2)C(I)=C1

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B699948
Product name: tert-Butyl3-Iodo-1H-indole-1-carboxylate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB154376
Product name: tert-butyl3-iodoindole-1-carboxylate
Packaging: 250mg
Price: $57.5
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB154376
Product name: tert-butyl3-iodoindole-1-carboxylate
Packaging: 1g
Price: $174
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-H-25
Product name: 3-Iodoindole-1-carboxylic acid tert-butyl ester
Purity: 98%
Packaging: 1g
Price: $98
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB154376
Product name: tert-butyl3-iodoindole-1-carboxylate
Packaging: 500mg
Price: $100
Updated: 2021/12/16

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1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE Chemical Properties,Usage,Production

Uses

1-Boc-3-iodoindole is used as a pharmaceutical intermediate and also used in ceramic manufacturing industry.

Synthesis

26340-47-6

24424-99-5

192189-07-4

In a dry reaction flask, 3-iodo-1H-indole (23.1 g, 95.05 mmol) was dissolved in dichloromethane (200 mL). Subsequently, triethylamine (24 g, 237.6 mmol) and di-tert-butyl dicarbonate (20.75 g, 95.07 mmol) were added sequentially to this solution. The reaction mixture was stirred at room temperature for 12 h. The progress of the reaction was monitored by thin layer chromatography (TLC) until the complete disappearance of the ingredients. After completion of the reaction, water was added to the mixture and extracted with ethyl acetate. The organic phases were combined and dried with anhydrous sodium sulfate. Finally, the solvent was removed by rotary evaporator to afford 1-Boc-3-iodoindole (27.7 g, 85% yield).

References

[1] Organic Letters, 2018, vol. 20, # 7, p. 1978 - 1981
[2] Journal of Organic Chemistry, 2008, vol. 73, # 17, p. 6706 - 6710
[3] Tetrahedron, 2000, vol. 56, # 43, p. 8473 - 8480
[4] Patent: CN104876914, 2017, B. Location in patent: Paragraph 0313-0315
[5] Patent: WO2017/173604, 2017, A1. Location in patent: Page/Page column 19; 20

1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE manufacturers

Career Henan Chemical Co

Product: 1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE 192189-07-4
Price: US $5.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2020-01-12

192189-07-4, 1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLERelated Search:

1-(TERT-BUTOXYCARBONYL)-3-IODO-1H-INDOLE

3-Iodoindole-1-carboxylic acid tert-butyl ester

1-Boc-3-iodoindole, 95%

tert-Butyl 3-iodo-1H-indole-1-carboxylate

N-Boc-3-iodoindole

3-Iodo-1H-indole-1-carboxylic acid 1,1-dimethylethyl ester

1-(Tert-Butoxycarbonyl)-3-iodo-1H-icdole

tert-butyl3-iodoindole-1-carboxylate

tert-butyl 3-iodo-1H-indol-1-carboxylate

1H-Indole-1-carboxylic acid, 3-iodo-, 1,1-dimethylethyl ester

1-Boc-3-iodoindole

192189-07-4

C13H14INO2