5-METHOXYPICOLINALDEHYDE

Product Name: 5-METHOXYPICOLINALDEHYDE
CAS No.: 22187-96-8
Chemical Name: 5-METHOXYPICOLINALDEHYDE
Synonyms: KML-76;KML-108;5-METHOXYPICOLINALDEHYDE;2-ForMyl-5-Methoxypyridine;5-methoxypyridine-2-aldehyde;5-Methoxypyridine-2-carbaldehyde;5-Methoxy-2-Pyridinecarboxaldehyde;5-Methoxypyridine-2-carboxaldehyde;2-Pyridinecarboxaldehyde, 5-Methoxy-
CBNumber: CB7470905
Molecular Formula: C7H7NO2
Formula Weight: 137.14
MOL File: 22187-96-8.mol

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5-METHOXYPICOLINALDEHYDE Property

Boiling point:: 248.4±20.0 °C(Predicted)
Density: 1.159±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 3.16±0.10(Predicted)
form: solid
color: White to off-white
InChI: InChI=1S/C7H7NO2/c1-10-7-3-2-6(5-9)8-4-7/h2-5H,1H3
InChIKey: CTYUCLSCBVSTAA-UHFFFAOYSA-N
SMILES: C1(C=O)=NC=C(OC)C=C1

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M266478
Product name: 5-Methoxypicolinaldehyde
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M266478
Product name: 5-Methoxypicolinaldehyde
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: M266478
Product name: 5-Methoxypicolinaldehyde
Packaging: 500mg
Price: $200
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H15-1-1P
Product name: 2-Formyl-5-methoxypyridine
Packaging: 1g
Price: $343
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0377941
Product name: 5-METHOXYPICOLINALDEHYDE
Purity: 95.00%
Packaging: 5MG
Price: $501.12
Updated: 2021/12/16

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5-METHOXYPICOLINALDEHYDE Chemical Properties,Usage,Production

Synthesis

31181-88-1

124-41-4

22187-96-8

General procedure for the synthesis of 5-methoxypyridine-2-aldehyde from 5-fluoropyridine-2-aldehyde and sodium methanol: 5-fluoropyridine-2-aldehyde (450 mg, 3.60 mmol) and sodium methanol (291 mg, 5.40 mmol) were dissolved in methanol (15 mL), and the reaction was stirred at 55 °C overnight. After completion of the reaction, the reaction mixture was filtered and the filter cake was washed with methanol. The filtrate was concentrated under reduced pressure to give the crude product. The crude product was purified by ISCO medium pressure liquid chromatography (MPLC) system using 30-45% ethyl acetate/hexane as eluent to afford 5-methoxypyridin-2-aldehyde as colorless oil (326 mg, 66.1% yield).1H NMR (CDCl3) δ 9.93 (s, 1H), 8.37 (d, 1H), 7.90 (d, 1H), 7.24 (d, 1H), 7.24 (d, 1H), 7.30 (d, 1H). 1H), 7.24 (dd, 1H), 3.89 (s, 3H).

References

[1] Patent: WO2009/27746, 2009, A1. Location in patent: Page/Page column 111

5-METHOXYPICOLINALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-METHOXYPICOLINALDEHYDE Suppliers

China 97 France 1 Germany 1 India 2 United Kingdom 1 United States 14 Global 116

Shanghai Sealing Biotechnology Co. Ltd..

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J & K SCIENTIFIC LTD.

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Pharmsynth Pharmaceutical (Chengdu) Technology Co.,LTD

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Shanghai Topbiochem Technology Co., Ltd

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Shanghai T&W Pharmaceutical Co., Ltd.

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View Lastest Price from 5-METHOXYPICOLINALDEHYDE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-METHOXYPICOLINALDEHYDE 22187-96-8
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-METHOXYPICOLINALDEHYDE 22187-96-8
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

Career Henan Chemical Co

Product: 5-METHOXYPICOLINALDEHYDE 22187-96-8
Price: US $5.50/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 1kg-100kg
Release date: 2020-01-10

22187-96-8, 5-METHOXYPICOLINALDEHYDERelated Search:

5-METHOXY-PYRIDIN-3-OL 5-Methoxyisoindoline hydrochloride 5-METHOXYPYRIDINE-2-CARBOXYLIC ACID (5-METHOXYPYRIDIN-2-YL)METHANOL 5-Methoxypyridine-3-boronic acid 5-METHOXY-PYRIDINE-3-CARBALDEHYDE 5-METHOXYPICOLINALDEHYDE 6-Bromo-5-methoxypicolinic acid 6-CHLORO-5-ETHOXY-2-PYRIDINECARBOXYLIC ACID 2,3-DIHYDRO[1,4]DIOXINO[2,3-C]PYRIDINE-7-CARBALDEHYDE methyl 6-bromo-5-methoxy-2-pyridinecarboxylate 3-BROMO-5-METHOXYPYRIDINE-2-CARBOXAMIDE N-cyclopropyl-6-(4-fluorophenyl)-5-methoxy-2-pyridinecarboxamide 6-IODO-5-METHOXY-2-PYRIDINECARBOXYLIC ACID 2-Pyridinecarboxylic acid, 5-(2-(trifluoromethyl)phenoxy)-, 2,3-dihydr o-1H-inden-5-yl ester 3-BROMO-5-METHOXYPYRIDINE-2-CARBOXYLIC ACID 5-butoxypicolinic acid Picolinic acid, 5-(p-chlorophenoxy)-, 5-indanyl ester

5-METHOXYPICOLINALDEHYDE

5-Methoxypyridine-2-carboxaldehyde

5-Methoxypyridine-2-carbaldehyde

2-ForMyl-5-Methoxypyridine

5-Methoxy-2-Pyridinecarboxaldehyde

2-Pyridinecarboxaldehyde, 5-Methoxy-

KML-76

KML-108

5-methoxypyridine-2-aldehyde

22187-96-8

Heterocycle-Pyridine series