N-Ethyl-3-carbazolecarboxaldehyde
- Product Name
- N-Ethyl-3-carbazolecarboxaldehyde
- CAS No.
- 7570-45-8
- Chemical Name
- N-Ethyl-3-carbazolecarboxaldehyde
- Synonyms
- AKOS B000241;AKOS BBS-00003258;TIMTEC-BB SBB000622;3-FORMYL-N-ETHYLCARBAZOLE;N-ethyl-3-formylcarbazole;N-ETHYL CARBAZOLE-3-ALDEHYDE;9-Ethyl-carbazole-3-aldehyde;9-Ethyl-3-formyl-9H-carbazole;9-ETHYLCARBAZOL-3-CARBALDEHYDE;N-Ethyl-3-carbazolecarbaldehyde
- CBNumber
- CB7774627
- Molecular Formula
- C15H13NO
- Formula Weight
- 223.27
- MOL File
- 7570-45-8.mol
N-Ethyl-3-carbazolecarboxaldehyde Property
- Melting point:
- 85-87 °C (lit.)
- Boiling point:
- 255 °C / 15mmHg
- Density
- 1.0707 (rough estimate)
- refractive index
- 1.5500 (estimate)
- storage temp.
- 2-8°C
- solubility
- soluble in Benzene,Toluene
- form
- Crystalline Powder or Granules
- color
- Yellow to ochre
- CAS DataBase Reference
- 7570-45-8(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- 151483
- Product name
- 9-Ethyl-3-carbazolecarboxaldehyde
- Purity
- 98%
- Packaging
- 25g
- Price
- $168
- Updated
- 2025/07/31
- Product number
- 151483
- Product name
- 9-Ethyl-3-carbazolecarboxaldehyde
- Purity
- 98%
- Packaging
- 100g
- Price
- $418
- Updated
- 2023/06/20
- Product number
- E0359
- Product name
- N-Ethylcarbazole-3-carboxaldehyde
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $49
- Updated
- 2025/07/31
- Product number
- E0359
- Product name
- N-Ethylcarbazole-3-carboxaldehyde
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $181
- Updated
- 2025/07/31
- Product number
- E945888
- Product name
- 9-Ethyl-9H-carbazole-3-carbaldehyde
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
N-Ethyl-3-carbazolecarboxaldehyde Chemical Properties,Usage,Production
Chemical Properties
yellow to ochre crystalline powder or granules
Uses
9-Ethyl-3-carbazolecarboxaldehyde was used in the synthesis of poly(vinyl acetal)s (PVAcs).
Synthesis
86-28-2
68-12-2
7570-45-8
Phosphorus oxychloride (POCl3, 1.4 mL, 10.2 mmol) was slowly added dropwise to stirring N,N-dimethylformamide (DMF, 3.2 mL, 40.8 mmol) under ice bath conditions for a controlled period of 10 minutes. The resulting slightly reddish solution was continued to be stirred for 1 h at room temperature. Subsequently, 9-ethyl-9H-carbazole (1.0 g, 5.1 mmol) was added over 10 minutes and the reaction mixture was placed in a microwave reactor at 100 °C for 1 hour. Upon completion of the reaction, the reaction mixture was cooled to room temperature and then carefully poured into crushed ice to quench the reaction. After the mixture was warmed to room temperature, it was extracted with ethyl acetate (EtOAc). The organic phases were combined, washed sequentially with water and saturated saline, dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography with different ratios of heptane/ethyl acetate (EtOAc) as eluent to afford N-ethylcarbazole-3-carbaldehyde as a white solid (1.054 g, 93% yield). The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3) and 13C NMR (101 MHz, CDCl3).
References
[1] European Journal of Medicinal Chemistry, 2018, vol. 159, p. 74 - 89
[2] Synthetic Communications, 2004, vol. 34, # 12, p. 2127 - 2133
[3] Chemistry Letters, 2008, vol. 37, # 6, p. 570 - 571
[4] Patent: WO2013/106460, 2013, A2. Location in patent: Paragraph 0198
[5] Journal of Molecular Structure, 2005, vol. 734, # 1-3, p. 35 - 44
N-Ethyl-3-carbazolecarboxaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-Ethyl-3-carbazolecarboxaldehyde manufacturers
- Product
- 9-Ethyl-9H-carbazole-3-carbaldehyde 7570-45-8
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-31
- Product
- N-Ethyl-3-carbazolecarboxaldehyde 7570-45-8
- Price
- US $2.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2018-12-23