ChemicalBook > CAS DataBase List > 1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE

1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE

Product Name
1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE
CAS No.
73930-39-9
Chemical Name
1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE
Synonyms
1-Phenylcyclopropan-1-amine hydrochloride;TIMTEC-BB SBB008643;1-PhenylcyclopropylaMine HCl;1-PhenylcyclopropanaMine, HCl;1-Phenyl-cyclopropylamine hydroc;1-Phenylcyclopropanamine Hydrochloride;1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE;cyclopropanamine, 1-phenyl-, hydrochloride;1-Phenylcyclopropan-1-aminehydrochloride95%;1-phenyl-cyclopropylamine HCL form, 95%min
CBNumber
CB7836835
Molecular Formula
C9H12ClN
Formula Weight
169.65128
MOL File
73930-39-9.mol
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1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE Property

Melting point:
194.7-194.9 °C
storage temp. 
Inert atmosphere,Room Temperature
form 
solid
Appearance
White to off-white Solid
InChI
InChI=1S/C9H11N.ClH/c10-9(6-7-9)8-4-2-1-3-5-8;/h1-5H,6-7,10H2;1H
InChIKey
ABUWJOHYZALSMF-UHFFFAOYSA-N
SMILES
C1(N)(C2=CC=CC=C2)CC1.Cl
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Safety

HazardClass 
IRRITANT
HS Code 
2921490090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
OTV000611
Product name
1-Phenylcyclopropanamine hydrochloride
Packaging
1 g
Price
$179
Updated
2025/07/31
TCI Chemical
Product number
P3138
Product name
1-Phenylcyclopropan-1-amine Hydrochloride
Packaging
200MG
Price
$60
Updated
2025/07/31
TCI Chemical
Product number
P3138
Product name
1-Phenylcyclopropan-1-amine Hydrochloride
Packaging
1G
Price
$150
Updated
2025/07/31
TRC
Product number
P336613
Product name
1-PhenylcyclopropanamineHydrochloride
Packaging
25mg
Price
$45
Updated
2021/12/16
SynQuest Laboratories
Product number
3630-5-X7
Product name
1-Phenylcyclopropan-1-amine hydrochloride
Purity
95%
Packaging
250mg
Price
$75
Updated
2021/12/16
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1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

6120-95-2

73930-39-9

The general procedure for the synthesis of 1-phenylcyclopropanamine hydrochloride from 1-phenyl-1-cyclopropanecarboxylic acid is as follows: first, 1-phenylcyclopropanecarboxylic acid (1) was reacted with sodium azide and sulfuric acid in chloroform to produce 1-phenylcyclopropanamine (2). Subsequently, 1-phenylcyclopropanamine was reacted with 2-methanesulfonyl chloride in chloroform under alkaline conditions to prepare to obtain the protected derivative (3), i.e., N-(1-phenylcyclopropyl) homotrimethylbenzenesulfonamide. Next, N-(1-phenylcyclopropyl)homotrimethylbenzenesulfonamide (3) was reacted with N-(4-bromobutyl)phthalimide (4) in DMF in the presence of sodium hydride overnight at room temperature to obtain N-(2- homotrimethylbenzenesulfonyl)-N-(1-phenylcyclopropyl)-4-phthalimidobutylamine (5). Then, phthaloyl was removed by reacting N-(2- homotrimethylbenzenesulfonyl)-N-(1-phenylcyclopropyl)-4-phthalimidobutylamine (5) with aniline hydrochloride and sodium methanol in methanol to produce N-(4-aminobutyl)-N-(1-phenylcyclopropyl)-2- homotrimethylbenzenesulfonamide (6). Next, the free amino group was again protected using 2- homotrimethylbenzenesulfonyl chloride in chloroform with hydrogen chloride to give N-(4-(homotrimethylbenzene-2-sulfonylamino)butyl)-N-(1-phenylcyclopropyl)-2- homotrimethylbenzenesulfonamide (7). Subsequently, a derivative of tetra- homotrimethylbenzene-2-sulfonyl-protected 1,2-bis((N-(1-phenylcyclopropyl)-4-aminobutyl)aminomethyl)cyclopropane (8) was prepared by reacting (7) with 1,2-bis(homotrimethylbenzene-2-sulfonyl- protected 1,2-bis((N-(1-phenylcyclopropyl)-4-amino-butyl)aminomethyl)cyclopropane) in DMF, in the presence of sodium hydride, at room temperature, overnight, to obtain (9). Finally, the homotrimethylbenzene-protecting group was removed using HBr in acetic acid and phenol in dichloromethane to give 1,2-bis((N-(1-phenylcyclopropyl)-4-aminobutyl)aminomethyl)cyclopropane (CGC-11255; SL-11255).

References

[1] Patent: WO2006/86773, 2006, A2. Location in patent: Page/Page column 32-34
[2] Patent: WO2011/119704, 2011, A1. Location in patent: Page/Page column 35-36
[3] Synthetic Communications, 1980, vol. 10, # 2, p. 107 - 110

1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE manufacturers

Career Henan Chemical Co
Product
1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE 73930-39-9
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
1000KGS
Release date
2019-12-20

73930-39-9, 1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDERelated Search:

1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE Cyclopropylamine 1-M-TOLYL-CYCLOPROPYLAMINE HYDROCHLORIDE 1-O-TOLYL-CYCLOPROPYLAMINE HYDROCHLORIDE 1-P-TOLYL-CYCLOPROPYLAMINE HYDROCHLORIDE 1-(2,4-DICHLORO-PHENYL)-CYCLOPROPYLAMINE 1-(4-FLUORO-PHENYL)-CYCLOPROPYLAMINE HYDROCHLORIDE 1-(4-CHLORO-PHENYL)-CYCLOPROPYLAMINE 1-(2-CHLORO-PHENYL)-CYCLOPROPYLAMINE 1-(4-CHLORO-PHENYL)-CYCLOPROPYLAMINE HYDROCHLORIDE 1-(3-CHLORO-PHENYL)-CYCLOPROPYLAMINE 1-(4-METHOXY-PHENYL)-CYCLOPROPYLAMINE HYDROCHLORIDE 1-(3-fluorophenyl)cyclopropanamine hydrochloride 1-PHENYL-CYCLOPROPYLAMINE 1-(3-METHOXY-PHENYL)-CYCLOPROPYLAMINE HYDROCHLORIDE 1-(2-METHOXY-PHENYL)-CYCLOPROPYLAMINE HYDROCHLORIDE 1-(3-CHLORO-PHENYL)-CYCLOPROPYLAMINE HYDROCHLORIDE 1-(2-FLUORO-PHENYL)-CYCLOPROPYLAMINE HYDROCHLORIDE

  • 1-PHENYL-CYCLOPROPYLAMINE HYDROCHLORIDE
  • TIMTEC-BB SBB008643
  • 1-Phenylcyclopropanamine Hydrochloride
  • Cyclopropanamine, 1-phenyl-, hydrochloride (1:1)
  • 1-Phenylcyclopropan-1-amine hydrochloride
  • 1-Phenyl-cyclopropylamine hydroc
  • 1-PhenylcyclopropylaMine HCl
  • 1-PhenylcyclopropanaMine, HCl
  • 1-Amino-1-phenylcyclopropane hydrochloride, (1-Aminocycloprop-1-yl)benzene hydrochloride
  • 1-Phenylcyclopropan-1-amine hydrochloride 95%
  • 1-Phenylcyclopropan-1-aminehydrochloride95%
  • cyclopropanamine, 1-phenyl-, hydrochloride
  • 1-phenyl-Cyclopropanamine hydrochloride (1:1)
  • 1-phenyl-cyclopropylamine HCL form, 95%min
  • 73930-39-9
  • API intermediates
  • Amines and Anilines