3-Benzyloxy acetophenone

Product Name: 3-Benzyloxy acetophenone
CAS No.: 34068-01-4
Chemical Name: 3-Benzyloxy acetophenone
Synonyms: NSC 159118;m-benzyloxyacetophenone;3-BENZYLOXYACETOPHENONE;Terbutaline Impurity 25;Terbutaline Impurity 57;Paracetamol Impurity 25;3'-Benzyloxyacetophenone;3-Benzyloxyacetophenone,97%;3'-Benzyloxyacetophenone >3''-BENZYLOXYACETOPHENONE 97%
CBNumber: CB7853522
Molecular Formula: C15H14O2
Formula Weight: 226.27
MOL File: 34068-01-4.mol

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3-Benzyloxy acetophenone Property

Melting point:: 29-30 °C
Boiling point:: 154°C/0.3mmHg(lit.)
Density: 1.0891 (rough estimate)
refractive index: 1.6530 (estimate)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Sparingly), Methanol (Slightly)
form: Low Melting Solid
color: Light yellow
λmax: 305nm(MeOH)(lit.)
CAS DataBase Reference: 34068-01-4(CAS DataBase Reference)

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Safety

Safety Statements: 24/25
HS Code: 29145000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S549053
Product name: 3''-BENZYLOXYACETOPHENONE
Purity: AldrichCPR
Packaging: 50MG
Price: $30.7
Updated: 2025/07/31

TCI Chemical

Product number: B4705
Product name: 3'-Benzyloxyacetophenone
Purity: >98.0%(GC)
Packaging: 5g
Price: $75
Updated: 2025/07/31

TCI Chemical

Product number: B4705
Product name: 3'-Benzyloxyacetophenone
Purity: >98.0%(GC)
Packaging: 25g
Price: $258
Updated: 2025/07/31

TRC

Product number: B285845
Product name: 3-Benzyloxyacetophenone
Packaging: 10g
Price: $485
Updated: 2021/12/16

TRC

Product number: B285845
Product name: 3-Benzyloxyacetophenone
Packaging: 25g
Price: $1110
Updated: 2021/12/16

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3-Benzyloxy acetophenone Chemical Properties,Usage,Production

Chemical Properties

Yellow Liquid

Synthesis

121-71-1

100-44-7

34068-01-4

Example 1 Synthesis of 3-benzyloxyacetophenone: 1 kg (7.35 mol) of 3-hydroxyacetophenone, 1.035 kg (7.5 mol) of anhydrous potassium carbonate, and 0.945 kg (7.5 mol) of benzyl chloride were dissolved in 4.1 L of acetone with mechanical stirring and heated and refluxed for 24 hrs. Subsequently, 0.1035 kg (0.75 mol) of anhydrous potassium carbonate and 0.0945 kg (0.75 mol) of benzyl chloride were added and refluxing was continued. the above additions were repeated after 72 hours and refluxing was continued to a total reaction time of 96 hours. After completion of the reaction, the reaction mixture was cooled, filtered and the filtrate was concentrated by rotary evaporator. To the concentrated filtrate was added 0.202 kg (2.0 mol) of triethylamine and stirred overnight. The reaction mixture was diluted with 1 L of ether and filtered, the filtrate was concentrated by evaporation and the residue was distilled to give 1.429 kg (86% yield) of the target product 3-benzyloxyacetophenone as an oil. Boiling point: 160°C (0.3 Torr).IR (CHCl3) spectrum showed absorption peaks located at 1695, 1605, 1595, 1493 and 1433 cm-1 .PMR (CDCl3) spectrum showed chemical shifts δ 2.52 (s, CH3), 5.03 (s, CH2) and 7.0-7.7 (m, Ph).

References

[1] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988, p. 2491 - 2500
[2] Journal of Medicinal Chemistry, 1992, vol. 35, # 16, p. 3045 - 3049
[3] Tetrahedron Letters, 2007, vol. 48, # 26, p. 4627 - 4630
[4] Chemical and Pharmaceutical Bulletin, 1995, vol. 43, # 5, p. 738 - 747
[5] Bioorganic and Medicinal Chemistry, 2005, vol. 13, # 5, p. 1537 - 1544

3-Benzyloxy acetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Benzyloxy acetophenone Suppliers

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View Lastest Price from 3-Benzyloxy acetophenone manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 3-Benzyloxyacetophenone 34068-01-4
Price: US $1.00/Kg
Min. Order: 1Kg
Purity: 98%
Supply Ability: 20T
Release date: 2024-07-29

Henan Fengda Chemical Co., Ltd

Product: 3-Benzyloxy acetophenone 34068-01-4
Price: US $5.00-0.10/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-16

Career Henan Chemical Co

Product: 3-Benzyloxy acetophenone 34068-01-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: ≥98%
Supply Ability: 200KG
Release date: 2019-08-30

34068-01-4, 3-Benzyloxy acetophenoneRelated Search:

M-(BENZOYLOXY)ACETOPHENONE 3-Benzyloxy acetophenone 3,5-Dibenzyloxyacetophenone 4'-Benzyloxyacetophenone 2'-BENZYLOXYACETOPHENONE 4'-(4-NITROBENZYLOXY)ACETOPHENONE 4'-(4-FLUOROBENZYLOXY)ACETOPHENONE 2-Bromo-4'-Benzyloxy-3'-nitroacetophenone 1-OXO-2,3-DIHYDRO-1H-INDEN-4-YL BENZOATE 3',4'-DIBENZYLOXYACETO-D3-PHENONE 2-HYDROXY-5-BENZYLOXYACETOPHENONE Ansoxetine 4''-BENZYLOXYACETOPHENONE, POLYMER-SUPPORTED, 0.8-1.1 MMOL/G ON WANG RESIN 4-BENZYLOXY-3-HYDROXYACETOPHENONE 3-(3-[(2-CHLORO-6-FLUOROBENZYL)OXY]PHENYL)-3-OXOPROPANAL O-(2,4-DICHLOROBENZYL)OXIME (E)-1-(3-[(2-CHLORO-6-FLUOROBENZYL)OXY]PHENYL)-3-(4-PHENOXYANILINO)-2-PROPEN-1-ONE (E)-3-(4-BROMO-3-METHYLANILINO)-1-(3-[(2-CHLORO-6-FLUOROBENZYL)OXY]PHENYL)-2-PROPEN-1-ONE (E)-1-(3-[(2,4-DICHLOROBENZYL)OXY]PHENYL)-3-(4-PHENOXYANILINO)-2-PROPEN-1-ONE

m-benzyloxyacetophenone

1-(3-Phenylmethoxyphenyl)ethanone

1-[3-(BENZYLOXY)PHENYL]ETHAN-1-ONE

1-(3-BENZYLOXYPHENYL)ETHANONE

3-BENZYLOXYACETOPHENONE

ALPHA-BROMO-3'-BENZYLOXY ACETOPHENONE

1-[3-(phenylmethoxy)phenyl]ethan-1-one

3''-BENZYLOXYACETOPHENONE 97%

NSC 159118

3-Benzyloxyacetophenone,97%

Ethanone, 1-[3-(phenylMethoxy)phenyl]-

3-Benzyloxyacetophenone, 97% 5GR

3'-(Benzyloxy)acetophenone, 1-[3-(Benzyloxy)phenyl]-1-oxoethane, 1-Acetyl-3-(benzyloxy)benzene

2-(3-bromopropyl)-2-phenylpropanedioic acid diethyl ester

Terbutaline Impurity 25

1-[3-(Benzyloxy)phenyl]ethan-1-one 98%

3'-Benzyloxyacetophenone &gt

3'-Benzyloxyacetophenone

Terbutaline Impurity 57

Paracetamol Impurity 25

34068-01-4

C17H19O2

Aromatic Acetophenones & Derivatives (substituted)

Aromatics