ChemicalBook > CAS DataBase List > methyl 4-methoxy-2-methylbenzoate

methyl 4-methoxy-2-methylbenzoate

Product Name
methyl 4-methoxy-2-methylbenzoate
CAS No.
35598-05-1
Chemical Name
methyl 4-methoxy-2-methylbenzoate
Synonyms
Methyl 2-Methyl-p-anisate;Methyl 4-Methoxy-o-toluate;methyl 4-methoxy-2-methylbenzoate;2-Methyl-p-anisic Acid Methyl Ester;4-Methoxy-o-toluic Acid Methyl Ester;2-methyl-4-methoxybenzoic acid methyl ester;Benzoic acid, 4-Methoxy-2-Methyl-, Methyl ester
CBNumber
CB7947096
Molecular Formula
C10H12O3
Formula Weight
180.2
MOL File
35598-05-1.mol
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methyl 4-methoxy-2-methylbenzoate Property

Boiling point:
98°C/0.5mmHg(lit.)
Density 
1.075±0.06 g/cm3(Predicted)
refractive index 
1.5360 to 1.5400
storage temp. 
Sealed in dry,Room Temperature
form 
clear liquid
color 
White to Light yellow
InChI
InChI=1S/C10H12O3/c1-7-6-8(12-2)4-5-9(7)10(11)13-3/h4-6H,1-3H3
InChIKey
OGYAVWKYDVBIMW-UHFFFAOYSA-N
SMILES
C(OC)(=O)C1=CC=C(OC)C=C1C
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Safety

HS Code 
2918999090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical
Product number
M2889
Product name
Methyl 4-Methoxy-2-methylbenzoate
Purity
>98.0%(GC)
Packaging
1g
Price
$38
Updated
2025/07/31
TCI Chemical
Product number
M2889
Product name
Methyl 4-Methoxy-2-methylbenzoate
Purity
>98.0%(GC)
Packaging
5g
Price
$191
Updated
2025/07/31
TRC
Product number
M338518
Product name
Methyl 4-Methoxy-2-methylbenzoate
Packaging
100mg
Price
$60
Updated
2021/12/16
TRC
Product number
M338518
Product name
Methyl 4-Methoxy-2-methylbenzoate
Packaging
500mg
Price
$130
Updated
2021/12/16
AK Scientific
Product number
7404AH
Product name
Methyl 4-Methoxy-2-methylbenzoate
Packaging
1g
Price
$60
Updated
2021/12/16
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methyl 4-methoxy-2-methylbenzoate Chemical Properties,Usage,Production

Synthesis

67-56-1

6245-57-4

35598-05-1

Thionyl chloride (1.3 mL, 17.8 mmol) was added slowly and dropwise to a stirred mixed solution of 4-methoxy-2-methylbenzoic acid (1.0 g, 6 mmol) and methanol (50 mL) at room temperature and under nitrogen protection. The reaction mixture was heated to reflux and maintained for 3 hours. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated under reduced pressure to give a light yellow crude product. The crude product was purified by silica gel column chromatography with the eluent of petroleum ether: ethyl acetate (9:1, v/v) to afford methyl 4-methoxy-2-methylbenzoate (1.11 g, 100% yield) in colorless liquid form. The product was characterized by 1H NMR (400 MHz, DMSO-d6) and ESI-MS: 1H NMR δ 7.81 (d, J = 9 Hz, 1H), 6.86 (d, J = 3 Hz, 1H), 6.83 (dd, J = 9, 3 Hz, 1H), 3.78 (s, 3H), 3.75 (s, 3H), 2.49 (s, 3H); ESI -MS m/z 181 ([M+H]+).

References

[1] Patent: WO2009/5998, 2009, A1. Location in patent: Page/Page column 214
[2] Patent: WO2004/14856, 2004, A1. Location in patent: Page 9; 14
[3] Patent: WO2008/20306, 2008, A2. Location in patent: Page/Page column 35
[4] Journal of Medicinal Chemistry, 2013, vol. 56, # 21, p. 8561 - 8578
[5] Tetrahedron, 2018, vol. 74, # 2, p. 224 - 239

methyl 4-methoxy-2-methylbenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from methyl 4-methoxy-2-methylbenzoate manufacturers

Qingdao RENAS Polymer Material Co., Ltd.
Product
methyl 4-methoxy-2-methylbenzoate 35598-05-1
Price
US $0.00/kg
Min. Order
20kg
Purity
99%
Supply Ability
20 tons
Release date
2025-05-06

35598-05-1, methyl 4-methoxy-2-methylbenzoate Related Search:

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  • methyl 4-methoxy-2-methylbenzoate
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  • 2-Methyl-p-anisic Acid Methyl Ester
  • 4-Methoxy-o-toluic Acid Methyl Ester
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  • 2-methyl-4-methoxybenzoic acid methyl ester
  • 35598-05-1