3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER

Product Name: 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER
CAS No.: 108593-44-8
Chemical Name: 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER
Synonyms: Methyl 3-Methoxy-5-Methylbenzoate;Methyl 5-methoxy-3-methylbenzoate;Methyl 3-methyl-5-(methyloxy)benzoate;3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER;Benzoic acid, 3-Methoxy-5-Methyl-, Methyl ester
CBNumber: CB81010387
Molecular Formula: C10H12O3
Formula Weight: 180.2
MOL File: 108593-44-8.mol

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3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER Property

Boiling point:: 270.8±20.0 °C(Predicted)
Density: 1.075±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2918999090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M354428
Product name: Methyl3-Methoxy-5-methylbenzoate
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: OR907669
Product name: Methyl 5-methoxy-3-methylbenzoate
Packaging: 250mg
Price: $203
Updated: 2021/12/16

AK Scientific

Product number: X8886
Product name: Methyl3-methoxy-5-methylbenzoate
Packaging: 250mg
Price: $203
Updated: 2021/12/16

AK Scientific

Product number: X8886
Product name: Methyl3-methoxy-5-methylbenzoate
Packaging: 1g
Price: $431
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0092411
Product name: 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER
Purity: 95.00%
Packaging: 5MG
Price: $495.88
Updated: 2021/12/16

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3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER Chemical Properties,Usage,Production

Synthesis

2615-71-6

74-88-4

108593-44-8

General procedure for the synthesis of methyl 3-methoxy-5-methylbenzoate from methyl 3-hydroxy-5-methylbenzoate and iodomethane: To a solution of methyl 3-hydroxy-5-methylbenzoate (20.0 g, 120 mmol) in N,N-dimethylformamide (120 mL) was added sequentially iodomethane (11.2 mL, 180 mmol), cesium carbonate (4.65 g, 180 mmol) and catalytic amount of 4-dimethylaminopyridine. 180 mmol) and a catalytic amount of 4-dimethylaminopyridine. The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, it was diluted with water (200 mL) and extracted with ethyl acetate (3 x 150 mL). The organic phases were combined, washed with saturated aqueous sodium chloride solution, dried over anhydrous magnesium sulfate, filtered and concentrated to afford the target product methyl 3-methoxy-5-methylbenzoate (19.9 g, 92% yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 2.38 (s, 3H), 3.84 (s, 3H), 3.91 (s, 3H), 6.93 (s, 1H), 7.37 (s, 1H), 7.48 (s, 1H).

References

[1] Patent: WO2007/105058, 2007, A2. Location in patent: Page/Page column 49
[2] Patent: WO2009/32667, 2009, A1. Location in patent: Page/Page column 137

3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER Suppliers

China 46 India 1 United Kingdom 2 United States 4 Global 53

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View Lastest Price from 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER manufacturers

Career Henan Chemical Co

Product: 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER 108593-44-8
Price: US $1.00/g
Min. Order: 1g
Purity: 98%
Supply Ability: 100KG
Release date: 2020-01-12

108593-44-8, 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTERRelated Search:

Methyl 5-allyl-3-methoxysalicylate METHYL-3-BROMOMETHYL-5-METHOXYBENZOATE BRYOPOGONIC ACID METHYL 5-METHOXY-ISOPHTHALATE METHYL 4-[3,5-BIS(METHOXYCARBONYL)PHENOXY]-3-AMINOBENZOATE STICTIC ACID ethyl 5-allyl-3-methoxysalicylate ravidomycin desacetylravidomycin DC-38-V DIMETHYL 5-METHOXYISOPHTHALATE 6H-Benzo(d)naphtho(1,2-b)pyran-6-one, 4-(6-deoxy-alpha-galactofuranosy l)-1-hydroxy-10,12-dimethoxy-8-methyl- METHYL-3-NITRO-4-(3,5-DICARBOXYMETHYL-PHENOXY)-BENZOATE AURORA KA-6188 AURORA KA-6179 AURORA KA-6187 AURORA KA-6186 AURORA KA-6185

3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER

Methyl 3-Methoxy-5-Methylbenzoate

Benzoic acid, 3-Methoxy-5-Methyl-, Methyl ester

Methyl 3-methyl-5-(methyloxy)benzoate

Methyl 5-methoxy-3-methylbenzoate

108593-44-8