Synthesis
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Phenyl-t-butylether

Synthesis
Product Name
Phenyl-t-butylether
CAS No.
6669-13-2
Chemical Name
Phenyl-t-butylether
Synonyms
NSC 78717;tert-Butoxybenzene;Phenyl tert-butyl ether;Ether, tert-butyl phenyl;2-Methyl-2-phenoxypropane;(1,1-Dimethylethoxy)benzene;tert-Butyl phenyl ether, 98%;Benzene, (1,1-dimethylethoxy)-;Inchi=1/C10H14o/C1-10(2,3)11-9-7-5-4-6-8-9/H4-8H,1-3h
CBNumber
CB81073270
Molecular Formula
C10H14O
Formula Weight
150.22
MOL File
6669-13-2.mol
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Phenyl-t-butylether Property

Melting point:
-17--16℃
Boiling point:
184°C
Density 
0.924
refractive index 
1.488
Flash point:
184°C
storage temp. 
Sealed in dry,Room Temperature
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Safety

HS Code 
2909309090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Alfa Aesar
Product number
H27689
Product name
tert-Butyl phenyl ether
Purity
98%
Packaging
250mg
Price
$130
Updated
2021/12/16
Alfa Aesar
Product number
H27689
Product name
tert-Butyl phenyl ether
Purity
98%
Packaging
1g
Price
$325
Updated
2021/12/16
Alfa Aesar
Product number
H27689
Product name
tert-Butyl phenyl ether
Purity
98%
Packaging
5g
Price
$996
Updated
2021/12/16
TRC
Product number
T205643
Product name
tert-Butoxybenzene
Packaging
500mg
Price
$330
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0079387
Product name
TERT-BUTOXYBENZENE
Purity
95.00%
Packaging
1G
Price
$989.6
Updated
2021/12/16
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Phenyl-t-butylether Chemical Properties,Usage,Production

Synthesis

A 4-mL vial was charged with bromobenzene (63 mg, 0.40 mmol), Pd(dba)2 (11.5 mg, 0.0200 mmol), Ph5FcP-(t-Bu)2 (14.2 mg, 0.0200 mmol), and sodium tert-butoxide (47 mg, 0.48 mmol). Anhydrous toluene (2 mL) was added, and the vial was sealed with a cap containing a PTFE septum and removed from the dry box. The reaction mixture was stirred at room temperature for 23 h. The reaction solution was then adsorbed onto silica gel, and the product was isolated by eluting with EtOAc/hexanes (0 to 10% gradient) to give the ether (58 mg, 97%).
Reference: Kataoka, N.; Shelby, Q.; Stambuli, J. P.; Hartwig, J. F. J. Org. Chem. 2002, 67, 5553–5566.

Uses

tert-Butoxybenzene was studied in the analysis of the color and flavor improvement of different starter cultures on northern air-dried sausage.

Phenyl-t-butylether Preparation Products And Raw materials

Raw materials

Preparation Products

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Phenyl-t-butylether Suppliers

Fisher Scientific Uk Ltd.
Tel
--
Fax
--
Email
.international@thermofisher.com
Country
United Kingdom
ProdList
2932
Advantage
58
Key Organics Ltd.
Tel
--
Fax
--
Email
enquiries@keyorganics.net
Country
United Kingdom
ProdList
851
Advantage
58
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View Lastest Price from Phenyl-t-butylether manufacturers

Career Henan Chemical Co
Product
Phenyl-t-butylether 6669-13-2
Price
US $9.80/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
1kg -1000kg
Release date
2020-01-02

6669-13-2, Phenyl-t-butyletherRelated Search:


  • (1,1-Dimethylethoxy)benzene
  • tert-Butyl phenyl ether, 98%
  • 2-Methyl-2-phenoxypropane
  • Phenyl tert-butyl ether
  • tert-Butoxybenzene
  • Benzene, (1,1-dimethylethoxy)-
  • Inchi=1/C10H14o/C1-10(2,3)11-9-7-5-4-6-8-9/H4-8H,1-3h
  • NSC 78717
  • Ether, tert-butyl phenyl
  • 6669-13-2