FMOC-PHE-OL

Product Name: FMOC-PHE-OL
CAS No.: 129397-83-7
Chemical Name: FMOC-PHE-OL
Synonyms: FMOC-PHE-OL;Fmoc-L-Phe-OL;FMOC-PHENYLALANINOL;FMOC-L-PHENYLALANINOL;FMOC-PHE-OL USP/EP/BP;Fmoc-DL-Phenylalaninol;N-FMOC-L-PHENYLALANINOL;N-Fmoc-L-phenylalaninol,95%;N-Fmoc-L-phenylalaninol 98%;N-ALPHA-FMOC-L-PHENYLALANINOL
CBNumber: CB8118024
Molecular Formula: C24H23NO3
Formula Weight: 373.44
MOL File: 129397-83-7.mol

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FMOC-PHE-OL Property

Melting point:: 129-130 °C
Boiling point:: 606.1±50.0 °C(Predicted)
Density: 1.219±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,2-8°C
solubility: Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
pka: 11.44±0.46(Predicted)
form: Solid
Appearance: White to off-white Solid
CAS DataBase Reference: 129397-83-7(CAS DataBase Reference)

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Safety

Safety Statements: 24/25
HazardClass: IRRITANT
HS Code: 29051990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: F861020
Product name: Fmoc-l-phenylalaninol
Packaging: 1g
Price: $75
Updated: 2021/12/16

Usbiological

Product number: 276993
Product name: Fmoc-L-phenylalaninol
Packaging: 2g
Price: $333
Updated: 2021/12/16

ChemPep

Product number: 201605
Product name: Fmoc-Phenylalaninol
Purity: ≥98%
Packaging: 5g
Price: $336
Updated: 2021/12/16

Chem-Impex

Product number: 03213
Product name: Fmoc-L-phenylalaninol,≥99%(HPLC)
Purity: ≥99%(HPLC)
Packaging: 25G
Price: $396.03
Updated: 2021/12/16

Chem-Impex

Product number: 03213
Product name: Fmoc-L-phenylalaninol,≥99%(HPLC)
Purity: ≥99%(HPLC)
Packaging: 5G
Price: $87.36
Updated: 2021/12/16

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FMOC-PHE-OL Chemical Properties,Usage,Production

Chemical Properties

White to off-white powder

Synthesis

35661-40-6

129397-83-7

The general procedure for the synthesis of Fmoc-L-phenylalaninol from Fmoc-L-phenylalanine was as follows: Fmoc-L-phenylalanine (10 mmol) was dissolved in THF (10 mL) at 0 °C, followed by the sequential addition of DIPEA (11 mmol, 1.42 mL) and EtOAc solution of 50% T3P (20 mmol, 6.36 mL). The reaction mixture was stirred at this temperature for about 10 minutes. Next, aqueous NaBH4 solution (10 mmol, 388 mg, dissolved in 0.3 mL H2O) was slowly added to the reaction system at the same temperature. The reaction progress was monitored by TLC until the reaction was complete. After completion of the reaction, the solvent was removed by rotary evaporation and the crude product was extracted with EtOAc. The organic phase was washed sequentially with 5% citric acid solution (10 mL × 2), 5% Na2CO3 solution (10 mL × 2), water and saturated saline. Finally, the organic phase was dried over anhydrous Na2SO4 and concentrated under reduced pressure to obtain the target product Fmoc-L-phenylalaninol.

References

[1] Tetrahedron Letters, 2012, vol. 53, # 38, p. 5059 - 5063
[2] Journal of Organic Chemistry, 2001, vol. 66, # 25, p. 8454 - 8462
[3] Tetrahedron Letters, 2000, vol. 41, # 32, p. 6131 - 6135
[4] Organic Letters, 2008, vol. 10, # 10, p. 1881 - 1884
[5] Tetrahedron Letters, 1999, vol. 40, # 23, p. 4395 - 4396

FMOC-PHE-OL Preparation Products And Raw materials

Raw materials

Preparation Products

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FMOC-PHE-OL Suppliers

Canada 1 China 102 Germany 3 India 5 Japan 2 Switzerland 1 United Kingdom 3 United States 19 Global 136

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
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Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 4006356688 18621169109
Fax: 86-21-61259102
Email: market03@meryer.com
Country: China
ProdList: 40228
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ChemFuture PharmaTech (Jiangsu) Ltd

Tel: 5108538618
Fax: 86 510 85386988-8017
Email: suger.wang@chemfuture.com
Country: China
ProdList: 832
Advantage: 65

GL Biochem (Shanghai) Ltd

Tel: 21-61263452 13641803416
Fax: 86-21-61263399
Email: ymbetter@glbiochem.com
Country: China
ProdList: 9981
Advantage: 64

Capot Chemical Co., Ltd

Tel: +86 (0) 571 85 58 67 18
Fax: 0086-571-85864795
Country: China
ProdList: 18207
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Shanghai Sinch Parmaceuticals Tech. Co. Ltd.

Tel: +86-21-54098501
Fax: +86-21-54096319
Email: sales@sinch.com.cn
Country: China
ProdList: 11598
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Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
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Chemsky (shanghai) International Co.,Ltd

Tel: 021-50135380
Email: shchemsky@sina.com
Country: China
ProdList: 15402
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ChemPep, Inc.

Tel: +1 (888) 615-9178 / (561) 791-8787
Fax: +1 (561) 791-8728
Email: service@chempep.com
Country: United States
ProdList: 2138
Advantage: 57

ZhengZhou HuaWen Chemical Co.Ltd

Tel: 0370-2785118 17550508557
Fax: QQ：3470079902
Email: 675141927@qq.com
Country: China
ProdList: 3199
Advantage: 55

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View Lastest Price from FMOC-PHE-OL manufacturers

Career Henan Chemical Co

Product: FMOC-PHE-OL 129397-83-7
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2020-01-29

129397-83-7, FMOC-PHE-OLRelated Search:

FMOC-D-ALLO-ILE-OH FMOC-D-ORN(BOC)-OH FMOC-D-TRP(ME)-OH Fmoc-Tyr(tBu)-OH Fmoc-O-benzyl-L-tyrosine Fmoc-N-methyl-L-phenylalanine FMOC-PHE-OH FMOC-TYR(2-BR-Z)-OH FMOC-D-4-Chlorophe Fmoc-4-nitro-L-phenylalanine Nalpha-Fmoc-L-tyrosine FMOC-TIC-OH (S)-N-Fmoc-1-Naphthylalanine FMOC-3,5-DIIODO-L-TYROSINE FMOC-2-NAL-OH FMOC-PHE-OL 99+%,FMOC-PHE-OL 98+% L-Phenylglycinol DL-PHENYLALANINOL

N-FMOC-L-PHENYLALANINOL

N-ALPHA-FMOC-L-PHENYLALANINOL

N-(9-FLUORENYLMETHOXYCARBONYL)-L-PHENYLALANINOL

FMOC-L-PHENYLALANINOL

FMOC-PHENYLALANINOL

FMOC-PHE-OL

FMOC-(S)-2-AMINO-3-PHENYL-1-PROPANOL

Fmoc-DL-Phenylalaninol

NALPHA-9-Fluorenylmethoxycarbonyl-L-phenylalaninol

(S)-2-(9-Fluorenylmethyloxycarbonyl)amino-3-phenyl-1-propanol, N-alpha-(9-Fluorenylmethyloxycarbonyl)-L-phenylalaninol

(S)-(9H-fluoren-9-yl)methyl 1-hydroxy-3-phenylpropan-2-ylcar

(S)-(9H-fluoren-9-yl)methyl 1-hydroxy-3-phenylpropan-2-ylcarbamate

(9H-fluoren-9-yl)methyl 1-hydroxy-3-phenylpropan-2-ylcarbamate

REF DUPL: Fmoc-Phenylalaninol

(S)-(9H-fluoren-9-yl)Methyl 1-hydroxy-3-phenylpropan-2-ylcarbaMa

FMoc-PhenylalaninolFMoc-Phenylalan

9H-fluoren-9-ylmethyl N-[(2S)-1-hydroxy-3-phenylpropan-2-yl]carbamate

Fmoc-L-Phe-OL

Fmoc-L-phenylalaninol≥ 99% (HPLC)

(S)-2-(Fmoc-amino)-3-phenyl-1-propanol

Carbamic acid, N-[(1S)-1-(hydroxymethyl)-2-phenylethyl]-, 9H-fluoren-9-ylmethyl ester

N-Fmoc-L-phenylalaninol,95%

FMOC-PHE-OL USP/EP/BP

N-Fmoc-L-phenylalaninol 98%

129397-83-7

Amino Alcohols

Fmoc-Amino acid series

Amino Acids

peptides