ChemicalBook > CAS DataBase List > 3-AMINO-5-CHLORO-BENZONITRILE

3-AMINO-5-CHLORO-BENZONITRILE

Product Name: 3-AMINO-5-CHLORO-BENZONITRILE
CAS No.: 53312-78-0
Chemical Name: 3-AMINO-5-CHLORO-BENZONITRILE
Synonyms: 3-Chloro-5-cyanoanisole;3-Chloro-5-cyanoaniline;5-Cyano-3-chloroaniline;5-Amino-3-chlorobenzonitrile;3-AMINO-5-CHLORO-BENZONITRILE;Benzonitrile, 3-aMino-5-chloro-;3-Amino-5-chlorobenzonitrile 97%
CBNumber: CB8127116
Molecular Formula: C7H5ClN2
Formula Weight: 152.58
MOL File: 53312-78-0.mol

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3-AMINO-5-CHLORO-BENZONITRILE Property

Boiling point:: 309.0±22.0 °C(Predicted)
Density: 1.33
storage temp.: 2-8°C, protect from light
pka: 1.73±0.10(Predicted)
form: Powder
Appearance: Off-white to light yellow Solid

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Safety

Hazard Codes: Xi
Risk Statements: 36
Safety Statements: 26
Hazard Note: Irritant
HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A617728
Product name: 3-Amino-5-chlorobenzonitrile
Packaging: 500mg
Price: $110
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3637-5-X3
Product name: 3-Amino-5-chlorobenzonitrile
Purity: 98%
Packaging: 1g
Price: $117
Updated: 2021/12/16

AK Scientific

Product number: J94223
Product name: 3-Amino-5-chlorobenzonitrile
Packaging: 5g
Price: $165
Updated: 2021/12/16

AK Scientific

Product number: V6448
Product name: 3-Amino-5-chlorobenzonitrile
Packaging: 5g
Price: $221
Updated: 2021/12/16

AK Scientific

Product number: J94223
Product name: 3-Amino-5-chlorobenzonitrile
Packaging: 10g
Price: $295
Updated: 2021/12/16

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3-AMINO-5-CHLORO-BENZONITRILE Chemical Properties,Usage,Production

Synthesis

34662-30-1

53312-78-0

The general procedure for the synthesis of 3-amino-5-chlorobenzonitrile from 3-chloro-5-nitrobenzonitrile was as follows: 3-chloro-5-nitrobenzonitrile was dissolved in DMF at room temperature, and 6 equivalents of SnCl2-2H2O was added, and the reaction was carried out overnight for reduction. After completion of the reaction, the target product was purified by silica gel column chromatography in 40% yield. LCMS analysis of the product (Condition A) showed a retention time of 1.61 min and a molecular ion peak [M+H]+ of 153.1.1 The 1H NMR (500 MHz, CDCl3) data were as follows: δ 6.97 (s, 1H), 6.84 (t, J = 2.0 Hz, 1H), 6.77 (s, 1H).

References

[1] Patent: US2006/287287, 2006, A1. Location in patent: Page/Page column 17-18

3-AMINO-5-CHLORO-BENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-AMINO-5-CHLORO-BENZONITRILE manufacturers

Career Henan Chemical Co

Product: 3-AMINO-5-CHLORO-BENZONITRILE 53312-78-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-08

53312-78-0, 3-AMINO-5-CHLORO-BENZONITRILERelated Search:

3-AMINO-4-BROMOPHENOL 3-Aminophenol hemisulfate 5-Bromopicolinic acid Terpinyl acetate Oseltamivir phosphate 2,5-Dibromo-3-nitropyridine 2-PYRIDYLTHIOUREA 2-tert-Butyl-1,4-benzoquinone 5-Fluorotryptamine hydrochloride 3-AMINO-5-CHLORO-BENZONITRILE 2-Amino-3-chloro-5-nitrobenzonitrile 2-Amino-5-chlorobenzonitrile 2-Amino-4-chlorobenzonitrile 2-Amino-6-chlorobenzonitrile 3-CHLORO-5-NITROBENZONITRILE 2,5-DIAMINO-3-CHLOROBENZONITRILE

3-AMINO-5-CHLORO-BENZONITRILE

3-Chloro-5-cyanoaniline

3-Amino-5-chlorobenzonitrile 97%

3-Chloro-5-cyanoanisole

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Benzonitrile, 3-aMino-5-chloro-

53312-78-0

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