ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE
- Product Name
- ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE
- CAS No.
- 885272-94-6
- Chemical Name
- ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE
- Synonyms
- KY003015;Ethyl 6-Bromoindazole-3-carboxylate;ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE;6-BROMO-1H-INDAZOLE-3-CARBOXYLIC ACID ETHYL ESTER;6-BroMo-1H-indazole-3-carboxyile acid ethyl ester;1H-Indazole-3-carboxylic acid, 6-broMo-, ethyl ester
- CBNumber
- CB81463107
- Molecular Formula
- C10H9BrN2O2
- Formula Weight
- 269.09
- MOL File
- 885272-94-6.mol
ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- FB56590
- Product name
- 6-Bromo-1H-indazole-3-carboxylic acid ethyl ester
- Packaging
- 250mg
- Price
- $102.5
- Updated
- 2021/12/16
- Product number
- FB56590
- Product name
- 6-Bromo-1H-indazole-3-carboxylic acid ethyl ester
- Packaging
- 500mg
- Price
- $165
- Updated
- 2021/12/16
- Product number
- 187916
- Product name
- Ethyl 6-bromo-1H-indazole-3-carboxylate
- Packaging
- 1g
- Price
- $224
- Updated
- 2021/12/16
- Product number
- Y4506
- Product name
- Ethyl6-bromo-1H-indazole-3-carboxylate
- Packaging
- 500mg
- Price
- $252
- Updated
- 2021/12/16
- Product number
- Y4506
- Product name
- Ethyl6-bromo-1H-indazole-3-carboxylate
- Packaging
- 1g
- Price
- $320
- Updated
- 2021/12/16
ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE Chemical Properties,Usage,Production
Synthesis
660823-36-9
885272-94-6
To a solution of 6-bromoindazole-3-carboxylic acid (4.4 g, 18.25 mmol) in ethanol (100 mL) was slowly added thionyl chloride (666 mL, 91 mmol), followed by heating and refluxing the reaction mixture for 3 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure and purified by fast column chromatography to afford ethyl 6-bromo-1H-indazole-3-carboxylate (2.1 g, 39% yield) as a tan solid. Mass spectrum (ESI) m/z: 270.9 (M + H). NMR hydrogen spectrum (400MHz, CDCl3) δ 8.08 (d, J = 8.6Hz, 1H), 7.95 (s, 1H), 7.44 (d, J = 8.6Hz, 1H), 4.57 (q, J = 7.0Hz, 2H), 1.51 (t, J = 7.2Hz, 3H).
References
[1] Patent: WO2017/123860, 2017, A1. Location in patent: Page/Page column 248
ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE Preparation Products And Raw materials
Raw materials
Preparation Products
ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE Suppliers
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View Lastest Price from ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE manufacturers
- Product
- Ethyl 6-bromo-1H-indazole-3-carboxylate 885272-94-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kgs
- Release date
- 2020-02-18