ChemicalBook > CAS DataBase List > ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE

ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE

Product Name
ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE
CAS No.
885272-94-6
Chemical Name
ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE
Synonyms
KY003015;Ethyl 6-Bromoindazole-3-carboxylate;ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE;6-BROMO-1H-INDAZOLE-3-CARBOXYLIC ACID ETHYL ESTER;6-BroMo-1H-indazole-3-carboxyile acid ethyl ester;1H-Indazole-3-carboxylic acid, 6-broMo-, ethyl ester
CBNumber
CB81463107
Molecular Formula
C10H9BrN2O2
Formula Weight
269.09
MOL File
885272-94-6.mol
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ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE Property

storage temp. 
Sealed in dry,Room Temperature
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FB56590
Product name
6-Bromo-1H-indazole-3-carboxylic acid ethyl ester
Packaging
100mg
Price
$82
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB56590
Product name
6-Bromo-1H-indazole-3-carboxylic acid ethyl ester
Packaging
250mg
Price
$102.5
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB56590
Product name
6-Bromo-1H-indazole-3-carboxylic acid ethyl ester
Packaging
500mg
Price
$165
Updated
2021/12/16
Matrix Scientific
Product number
187916
Product name
Ethyl 6-bromo-1H-indazole-3-carboxylate
Packaging
1g
Price
$224
Updated
2021/12/16
AK Scientific
Product number
Y4506
Product name
Ethyl6-bromo-1H-indazole-3-carboxylate
Packaging
500mg
Price
$252
Updated
2021/12/16
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ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE Chemical Properties,Usage,Production

Synthesis

660823-36-9

885272-94-6

To a solution of 6-bromoindazole-3-carboxylic acid (4.4 g, 18.25 mmol) in ethanol (100 mL) was slowly added thionyl chloride (666 mL, 91 mmol), followed by heating and refluxing the reaction mixture for 3 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure and purified by fast column chromatography to afford ethyl 6-bromo-1H-indazole-3-carboxylate (2.1 g, 39% yield) as a tan solid. Mass spectrum (ESI) m/z: 270.9 (M + H). NMR hydrogen spectrum (400MHz, CDCl3) δ 8.08 (d, J = 8.6Hz, 1H), 7.95 (s, 1H), 7.44 (d, J = 8.6Hz, 1H), 4.57 (q, J = 7.0Hz, 2H), 1.51 (t, J = 7.2Hz, 3H).

References

[1] Patent: WO2017/123860, 2017, A1. Location in patent: Page/Page column 248

ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE manufacturers

Career Henan Chemical Co
Product
Ethyl 6-bromo-1H-indazole-3-carboxylate 885272-94-6
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kgs
Release date
2020-02-18

885272-94-6, ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATERelated Search:


  • KY003015
  • 6-BroMo-1H-indazole-3-carboxyile acid ethyl ester
  • 1H-Indazole-3-carboxylic acid, 6-broMo-, ethyl ester
  • ETHYL 6-BROMO-1H-INDAZOLE-3-CARBOXYLATE
  • 6-BROMO-1H-INDAZOLE-3-CARBOXYLIC ACID ETHYL ESTER
  • Ethyl 6-Bromoindazole-3-carboxylate
  • 885272-94-6