N-METHYLPIPERIDINE-4-CARBOXAMIDE
- Product Name
- N-METHYLPIPERIDINE-4-CARBOXAMIDE
- CAS No.
- 1903-69-1
- Chemical Name
- N-METHYLPIPERIDINE-4-CARBOXAMIDE
- Synonyms
- N-Methyl-piperidin-4-carboxamide;N-Methyl-4-piperidinecarboxaMide;4-Piperidinecarboxamide, N-methyl-;N-methylpiperidin-4-carboxylic acid amide
- CBNumber
- CB81491915
- Molecular Formula
- C7H14N2O
- Formula Weight
- 142.2
- MOL File
- 1903-69-1.mol
N-METHYLPIPERIDINE-4-CARBOXAMIDE Property
- Melting point:
- 123~125℃
- Boiling point:
- 318.5±31.0 °C(Predicted)
- Density
- 0.997±0.06 g/cm3(Predicted)
- pka
- 16.06±0.20(Predicted)
- form
- powder
- color
- Yellow
Safety
- HazardClass
- IRRITANT
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- M104460
- Product name
- N-methylpiperidine-4-carboxamide
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR949865
- Product name
- N-Methylpiperidine-4-carboxamide
- Purity
- 95%
- Packaging
- 1g
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 6412AD
- Product name
- N-Methylpiperidine-4-carboxamide
- Packaging
- 250mg
- Price
- $83
- Updated
- 2021/12/16
- Product number
- 016440
- Product name
- N-Methylpiperidine-4-carboxamide
- Packaging
- 500mg
- Price
- $184
- Updated
- 2021/12/16
- Product number
- 009970
- Product name
- Piperidine-4-carboxylicacidmethylamide
- Purity
- 95%
- Packaging
- 5g
- Price
- $190
- Updated
- 2021/12/16
N-METHYLPIPERIDINE-4-CARBOXAMIDE Chemical Properties,Usage,Production
Synthesis
544696-01-7
1903-69-1
GENERAL STEPS: 1-Boc-4-piperidinyl-N-methylamide (68 mg, 0.28 mmol) was dissolved in methanol (2 mL) and cooled to 0°C. A 1,4-dioxane solution (2 mL) of 4 M hydrogen chloride was slowly added. The reaction mixture was stirred at 0°C for 15 minutes and then gradually warmed to room temperature and continued stirring for 3 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The crude product was purified by SCX-2 column chromatography, eluting first with methanol and then with 0.5 M ammonia in methanol solution to afford N-methylpiperidine-4-carboxamide as a colorless oil (41 mg, 99% yield). The product was detected by infrared spectroscopy (CHCl3) with characteristic absorption peaks of 1308, 2948, 1663, 1525, 1227, 1119 cm-1; mass spectrometry (ESI) analysis showed that the theoretical value of the [M+H]+ ion peak of C7H15N2O was 143.1179 and the measured value was 143.1178.
References
[1] Patent: WO2010/41054, 2010, A1. Location in patent: Page/Page column 32
N-METHYLPIPERIDINE-4-CARBOXAMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-METHYLPIPERIDINE-4-CARBOXAMIDE manufacturers
- Product
- N-METHYLPIPERIDINE-4-CARBOXAMIDE 1903-69-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 100kg
- Release date
- 2020-01-14