2-CHLORO-4-METHOXYBENZONITRILE

Product Name: 2-CHLORO-4-METHOXYBENZONITRILE
CAS No.: 127666-99-3
Chemical Name: 2-CHLORO-4-METHOXYBENZONITRILE
Synonyms: BUTTPARK 120\07-70;3-Chloro-4-cyanoanisole;2-CHLORO-4-METHOXYBENZONITRILE;Benzonitrile,2-chloro-4-methoxy-;2-chloro-4-Methoxy benzene nitrile;2-BROMO-7-METHYLH-IMIDAZO[1,4-A]PYRIDINE*;2-chloro-4-(trifluoromethoxy)benzonitrile;3-Chloro-4-cyanoanisole, 2-Chloro-p-anisonitrile
CBNumber: CB8149686
Molecular Formula: C8H6ClNO
Formula Weight: 167.59
MOL File: 127666-99-3.mol

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2-CHLORO-4-METHOXYBENZONITRILE Property

Melting point:: 71-75°C
Boiling point:: 296.6±20.0 °C(Predicted)
Density: 1.25±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
Hazard Note: Irritant
HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: C428508
Product name: 2-Chloro-4-methoxybenzonitrile
Packaging: 250mg
Price: $55
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4637-5-Y6
Product name: 2-Chloro-4-methoxybenzonitrile
Purity: 99%
Packaging: 1g
Price: $26
Updated: 2021/12/16

Matrix Scientific

Product number: 084655
Product name: 2-Chloro-4-methoxybenzonitrile
Purity: 97%
Packaging: 1g
Price: $55
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4637-5-Y6
Product name: 2-Chloro-4-methoxybenzonitrile
Purity: 99%
Packaging: 5G
Price: $87
Updated: 2021/12/16

Matrix Scientific

Product number: 084655
Product name: 2-Chloro-4-methoxybenzonitrile
Purity: 97%
Packaging: 5g
Price: $203
Updated: 2021/12/16

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2-CHLORO-4-METHOXYBENZONITRILE Chemical Properties,Usage,Production

Chemical Properties

Off-white crystalline

Synthesis

3336-16-1

74-88-4

127666-99-3

General procedure for the synthesis of 2-chloro-4-methoxybenzonitrile from 2-chloro-4-hydroxybenzonitrile and iodomethane: To a stirred solution of 2-chloro-4-hydroxybenzonitrile (2.5 g, 16 mmol) in DMF (25 mL) was slowly added NaH (0.431 g, 18.0 mmol) at 0 °C. After 30 min, iodomethane (3.47 g, 24.4 mmol), followed by continued stirring of the reaction mixture for 1 h at room temperature. After completion of the reaction, the reaction mixture was quenched with ice water and extracted with ether. The organic layer was washed sequentially with water and saturated NaCl solution, dried over Na2SO4 and concentrated in vacuum to afford the target product 2-chloro-4-methoxybenzonitrile as a brown solid (2.7 g, 98% yield).

References

[1] Patent: WO2010/65760, 2010, A1. Location in patent: Page/Page column 133-134
[2] Patent: WO2006/8046, 2006, A1. Location in patent: Page/Page column 47

2-CHLORO-4-METHOXYBENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-4-METHOXYBENZONITRILE Suppliers

China 90 France 1 India 3 Switzerland 1 United Kingdom 6 United States 11 Global 112

Shijiazhuang Sdyano Fine Chemical Co., Ltd.

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Syntechem Co.,Ltd

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Hangzhou Yuhao Chemical Technology Co., Ltd

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View Lastest Price from 2-CHLORO-4-METHOXYBENZONITRILE manufacturers

Career Henan Chemical Co

Product: 2-CHLORO-4-METHOXYBENZONITRILE 127666-99-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-11

127666-99-3, 2-CHLORO-4-METHOXYBENZONITRILERelated Search:

2-CHLORO-4-METHOXYPHENOL 2-Chloro-4-methylbenzaldehyde 2-CHLORO-4-METHOXYBENZONITRILE 2-CHLORO-4-(PIPERIDIN-4-YLOXY)BENZONITRILE 2-CHLORO-3,4-DIMETHOXYBENZONITRILE 3-Chloro-4-methoxybenzonitrile, 97+%,3-CHLORO-4-METHOXYBENZONITRILE 3-chloro-5-methoxybenzonitrile 5-CHLORO-2-METHOXYBENZONITRILE 4-(Trifluoromethoxy)benzonitrile 2-CHLORO-5-METHOXYBENZONITRILE 2-CHLORO-6-METHOXYBENZONITRILE 4-CHLORO-3-METHOXYBENZONITRILE 4-chloro-2-methoxybenzonitrile 2-CHLORO-4-(PIPERIDIN-3-YLOXY)-BENZONITRILE 3-(3-Chloro-4-cyano-phenoxy)-pyrrolidine-1-carboxylic acid tert-butyl ester 3-(3-Chloro-4-cyano-phenoxy)-piperidine-1-carboxylic acid tert-butyl ester (2S,4R)-1-(tert-butoxycarbonyl)-4-(3-chloro-4-cyanophenoxy)pyrrolidine-2-carboxylic acid 3-(3-Chloro-4-cyano-phenoxy)-azetidine-1-carboxylic acid tert-butyl ester

2-CHLORO-4-METHOXYBENZONITRILE

BUTTPARK 120\07-70

2-chloro-4-Methoxy benzene nitrile

3-Chloro-4-cyanoanisole

3-Chloro-4-cyanoanisole, 2-Chloro-p-anisonitrile

2-chloro-4-(trifluoromethoxy)benzonitrile

Benzonitrile,2-chloro-4-methoxy-

2-BROMO-7-METHYLH-IMIDAZO[1,4-A]PYRIDINE*

127666-99-3

C8H6NOCl

Phenyls & Phenyl-Het