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2-CHLORO-6-METHOXYBENZONITRILE

Product Name
2-CHLORO-6-METHOXYBENZONITRILE
CAS No.
6575-10-6
Chemical Name
2-CHLORO-6-METHOXYBENZONITRILE
Synonyms
6-Chloro-o-anisonitrile;2-Methoxy-6-chlorobenzonitrile;2-CHLORO-6-METHOXYBENZONITRILE;Benzonitrile, 2-chloro-6-methoxy-;2-Chloro-6-methoxybenzonitrile,97%
CBNumber
CB0365828
Molecular Formula
C8H6ClNO
Formula Weight
167.59
MOL File
6575-10-6.mol
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2-CHLORO-6-METHOXYBENZONITRILE Property

Melting point:
98-100°C
Boiling point:
294.7±20.0 °C(Predicted)
Density 
1.25±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform, Ethyl Acetate
form 
Solid
color 
White
CAS DataBase Reference
6575-10-6
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Safety

Hazard Codes 
Xn
Risk Statements 
22
HS Code 
2926907090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C367935
Product name
2-Chloro-6-methoxybenzonitrile
Packaging
500mg
Price
$90
Updated
2021/12/16
TRC
Product number
C367935
Product name
2-Chloro-6-methoxybenzonitrile
Packaging
2g
Price
$285
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC20153
Product name
2-Chloro-6-methoxybenzonitrile
Packaging
500mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC20153
Product name
2-Chloro-6-methoxybenzonitrile
Packaging
1g
Price
$120
Updated
2021/12/16
SynQuest Laboratories
Product number
4637-5-0D
Product name
2-Chloro-6-methoxybenzonitrile
Packaging
1g
Price
$138
Updated
2021/12/16
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2-CHLORO-6-METHOXYBENZONITRILE Chemical Properties,Usage,Production

Chemical Properties

White Needles

Uses

2-Chloro-6-methoxybenzonitrile (cas# 6575-10-6) is a compound useful in organic synthesis.

Synthesis

668-45-1

124-41-4

6575-10-6

To a 100 mL solution of 2-chloro-6-fluorobenzonitrile (1.55 g, 10.0 mmol) in anhydrous methanol was added sodium methanolate (4.32 g, 80 mmol). The reaction mixture was heated at 85 °C and stirred overnight. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure. The residue was diluted with 400 mL of dichloromethane (DCM) and washed sequentially with saturated aqueous sodium bicarbonate (NaHCO3) and aqueous ammonium chloride (NH4Cl, 2 x 20 mL). The organic phase was dried over anhydrous sodium sulfate (Na2SO4) and concentrated in vacuum. The crude product was purified by column chromatography (petroleum ether: ethyl acetate = 10:1) to afford 2-chloro-6-methoxycyanobenzene (1.5 g, 89.8% yield) as a light yellow solid. LC-MS showed [MH]+ = 168.0.

References

[1] Patent: WO2017/221092, 2017, A1. Location in patent: Paragraph 00151

2-CHLORO-6-METHOXYBENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-6-METHOXYBENZONITRILE Suppliers

Canada 1 China 35 France 1 Germany 2 India 1 United Kingdom 5 United States 12 Global 57
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6575-10-6, 2-CHLORO-6-METHOXYBENZONITRILERelated Search:

3-CHLORO-4-METHOXYBENZONITRILE,3-Chloro-4-methoxybenzonitrile, 97+% 2-CHLORO-4-METHOXYBENZONITRILE 5-CHLORO-2-METHOXYBENZONITRILE 2-CHLORO-6-PHENOXYBENZONITRILE 3-chloro-5-methoxybenzonitrile 4-(3-CHLORO-2-CYANOPHENOXY)BENZENE-1-SULFONYL CHLORIDE NPS 2143 4-chloro-2-methoxybenzonitrile 2-chloro-6-benzyloxybenzonitrile 2-CHLORO-6-METHOXYBENZONITRILE 2-(4-ACETYLPHENOXY)-6-CHLOROBENZENECARBONITRILE 4-CHLORO-3-METHOXYBENZONITRILE 2-CHLORO-5-METHOXYBENZONITRILE 2-CHLORO-3-METHOXYBENZONITRILE 2-CHLORO-6-METHOXYBENZONITRILE 100MG [R] 2-CHLORO-6-(4-([3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]METHYL)PHENOXY)BENZENECARBONITRILE 2-CHLORO-6-[4-(1-METHYL-1H-PYRAZOL-3-YL)PHENOXY]BENZENECARBONITRILE 2-chloro-4,6-dimethoxybenzonitrile

  • 2-CHLORO-6-METHOXYBENZONITRILE
  • Benzonitrile, 2-chloro-6-methoxy-
  • 2-Chloro-6-methoxybenzonitrile,97%
  • 2-Methoxy-6-chlorobenzonitrile
  • 6-Chloro-o-anisonitrile
  • 6575-10-6
  • Aromatics Compounds
  • Aromatics