ChemicalBook > CAS DataBase List > 2-CHLORO-6-METHOXYBENZONITRILE
2-CHLORO-6-METHOXYBENZONITRILE
- Product Name
- 2-CHLORO-6-METHOXYBENZONITRILE
- CAS No.
- 6575-10-6
- Chemical Name
- 2-CHLORO-6-METHOXYBENZONITRILE
- Synonyms
- 6-Chloro-o-anisonitrile;2-Methoxy-6-chlorobenzonitrile;2-CHLORO-6-METHOXYBENZONITRILE;Benzonitrile, 2-chloro-6-methoxy-;2-Chloro-6-methoxybenzonitrile,97%
- CBNumber
- CB0365828
- Molecular Formula
- C8H6ClNO
- Formula Weight
- 167.59
- MOL File
- 6575-10-6.mol
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2-CHLORO-6-METHOXYBENZONITRILE Property
- Melting point:
- 98-100°C
- Boiling point:
- 294.7±20.0 °C(Predicted)
- Density
- 1.25±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Chloroform, Ethyl Acetate
- form
- Solid
- color
- White
- CAS DataBase Reference
- 6575-10-6
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- C367935
- Product name
- 2-Chloro-6-methoxybenzonitrile
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
TRC
- Product number
- C367935
- Product name
- 2-Chloro-6-methoxybenzonitrile
- Packaging
- 2g
- Price
- $285
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FC20153
- Product name
- 2-Chloro-6-methoxybenzonitrile
- Packaging
- 10g
- Price
- $500
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 072414
- Product name
- 2-Chloro-6-methoxybenzonitrile
- Purity
- 95+%
- Packaging
- 5g
- Price
- $798
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0011509
- Product name
- 2-CHLORO-6-METHOXYBENZONITRILE
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $865
- Updated
- 2021/12/16
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2-CHLORO-6-METHOXYBENZONITRILE Chemical Properties,Usage,Production
Chemical Properties
White Needles
Uses
2-Chloro-6-methoxybenzonitrile (cas# 6575-10-6) is a compound useful in organic synthesis.
Synthesis
668-45-1
124-41-4
6575-10-6
To a 100 mL solution of 2-chloro-6-fluorobenzonitrile (1.55 g, 10.0 mmol) in anhydrous methanol was added sodium methanolate (4.32 g, 80 mmol). The reaction mixture was heated at 85 °C and stirred overnight. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure. The residue was diluted with 400 mL of dichloromethane (DCM) and washed sequentially with saturated aqueous sodium bicarbonate (NaHCO3) and aqueous ammonium chloride (NH4Cl, 2 x 20 mL). The organic phase was dried over anhydrous sodium sulfate (Na2SO4) and concentrated in vacuum. The crude product was purified by column chromatography (petroleum ether: ethyl acetate = 10:1) to afford 2-chloro-6-methoxycyanobenzene (1.5 g, 89.8% yield) as a light yellow solid. LC-MS showed [MH]+ = 168.0.
References
[1] Patent: WO2017/221092, 2017, A1. Location in patent: Paragraph 00151
2-CHLORO-6-METHOXYBENZONITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
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2-CHLORO-6-METHOXYBENZONITRILE Suppliers
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6575-10-6, 2-CHLORO-6-METHOXYBENZONITRILERelated Search:
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