4,6-DIIODO-2-METHYLPYRIMIDINE
- Product Name
- 4,6-DIIODO-2-METHYLPYRIMIDINE
- CAS No.
- 66298-49-5
- Chemical Name
- 4,6-DIIODO-2-METHYLPYRIMIDINE
- Synonyms
- 2-methyl-4，6-diiodopyrimidin;4,6-DIIODO-2-METHYLPYRIMIDINE;Pyrimidine, 4,6-diiodo-2-methyl-;4,6-diiodo-2-methylpyrimidine - [AC78565];4,6-DIIODO-2-METHYLPYRIMIDINE ISO 9001：2015 REACH
- CBNumber
- CB81502479
- Molecular Formula
- C5H4I2N2
- Formula Weight
- 345.91
- MOL File
- 66298-49-5.mol
4,6-DIIODO-2-METHYLPYRIMIDINE Property
- storage temp.
- 2-8°C(protect from light)
- Appearance
- Off-white to light brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- FD142934
- Product name
- 4,6-Diiodo-2-methylpyrimidine
- Packaging
- 500mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- FD142934
- Product name
- 4,6-Diiodo-2-methylpyrimidine
- Packaging
- 1g
- Price
- $227
- Updated
- 2021/12/16
- Product number
- 072539
- Product name
- 4,6-Diiodo-2-methylpyrimidine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $278
- Updated
- 2021/12/16
- Product number
- FD142934
- Product name
- 4,6-Diiodo-2-methylpyrimidine
- Packaging
- 2g
- Price
- $394
- Updated
- 2021/12/16
- Product number
- FD142934
- Product name
- 4,6-Diiodo-2-methylpyrimidine
- Packaging
- 250mg
- Price
- $75
- Updated
- 2021/12/16
4,6-DIIODO-2-METHYLPYRIMIDINE Chemical Properties,Usage,Production
Synthesis
1780-26-3
66298-49-5
General procedure for the synthesis of 4,6-diiodo-2-methylpyrimidine from 4,6-dichloro-2-methylpyrimidine: Synthesis of the key intermediate 6-iodo-2-methylpyrimidin-4-ylamine (Part A): Potassium iodide (3.5 M aqueous solution, 30.0 mL) was added to a solution of acetone (150 mL) containing 4,6-dichloro-2-methylpyrimidine (5.00 g, 0.03 mol) and sodium iodide (23.0 g, 0.15 mol) at room temperature. The reaction mixture was stirred at room temperature for 16 hours before being poured into an ice-water mixture (about 1:1, 250 mL) and allowed to warm slowly to room temperature. The solid formed was collected by diafiltration and washed with deionized water. The solid was dried in air to give 4,6-diiodo-2-methylpyrimidine (9.80 g, 92% yield) as an off-white solid.LC-MS (m/z): 347 ([M+H]+).
References
[1] Patent: WO2007/75852, 2007, A2. Location in patent: Page/Page column 33
[2] Patent: US2007/197523, 2007, A1. Location in patent: Page/Page column 8
[3] Patent: WO2017/12576, 2017, A1. Location in patent: Page/Page column 99
[4] Patent: WO2018/137619, 2018, A1. Location in patent: Page/Page column 52; 78
[5] Patent: WO2018/137618, 2018, A1. Location in patent: Page/Page column 46; 57; 58
4,6-DIIODO-2-METHYLPYRIMIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
4,6-DIIODO-2-METHYLPYRIMIDINE Suppliers
- Tel
- --
- Fax
- --
- sales@carbosynth.com
- Country
- United Kingdom
- ProdList
- 6005
- Advantage
- 58
View Lastest Price from 4,6-DIIODO-2-METHYLPYRIMIDINE manufacturers
- Product
- 4,6-DIIODO-2-METHYLPYRIMIDINE 66298-49-5
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-12-07