3,5-Dichloro-4-methylaniline
- Product Name
- 3,5-Dichloro-4-methylaniline
- CAS No.
- 54730-35-7
- Chemical Name
- 3,5-Dichloro-4-methylaniline
- Synonyms
- SKL201;3,5-Dichloro-4-methylaniline;3,5-Dichloro-4-methylbenzenamine;BenzenaMine, 3,5-dichloro-4-Methyl-
- CBNumber
- CB81510074
- Molecular Formula
- C7H7Cl2N
- Formula Weight
- 176.04
- MOL File
- 54730-35-7.mol
3,5-Dichloro-4-methylaniline Property
- Melting point:
- 57-59 °C
- Boiling point:
- 284.6±35.0 °C(Predicted)
- Density
- 1.334±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- Chloroform (Slightly), DMSO (Slightly)
- form
- Solid
- pka
- 2.92±0.10(Predicted)
- color
- Beige to Brown
Safety
- HS Code
- 2921490090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D435125
- Product name
- 3,5-Dichloro-4-methylaniline
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- D435125
- Product name
- 3,5-Dichloro-4-methylaniline
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- FD139569
- Product name
- 3,5-Dichloro-4-methylaniline
- Packaging
- 2g
- Price
- $65
- Updated
- 2021/12/16
- Product number
- HCH0059160
- Product name
- 3,5-DICHLORO-4-METHYLANILINE
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $1147.43
- Updated
- 2021/12/16
- Product number
- HCH0059160
- Product name
- 3,5-DICHLORO-4-METHYLANILINE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $1421.65
- Updated
- 2021/12/16
3,5-Dichloro-4-methylaniline Chemical Properties,Usage,Production
Synthesis
7149-69-1
54730-35-7
General procedure for the synthesis of 3,5-dichloro-4-methylaniline from 1,3-dichloro-2-methyl-5-nitrobenzene: First, 1,3-dichloro-2-methyl-5-nitrobenzene (0.50 g, 2.43 mmol) was dissolved in N,N-dimethylformamide (DMF). Subsequently, tin(II) chloride dihydrate (2.74 g, 12.1 mmol) was added all at once. The reaction mixture was stirred at room temperature for 1 hour. After completion of the reaction, the reaction mixture was diluted with ethyl acetate and filtered through a diatomaceous earth pad. The filtrate was sequentially washed four times with water and twice with brine and then dried with anhydrous magnesium sulfate. The dried organic phase was filtered and concentrated to give a dark-colored oil. Finally, the residue was purified by silica gel column chromatography using a gradient elution with 5% to 10% ethyl acetate in hexane solution to give 342 mg (80% yield) of 3,5-dichloro-4-methylaniline as a white flaky solid.
References
[1] Gazzetta Chimica Italiana, 1996, vol. 126, # 3, p. 179 - 185
[2] Tetrahedron, 1998, vol. 54, # 12, p. 2953 - 2966
[3] Patent: WO2007/127763, 2007, A2. Location in patent: Page/Page column 37
[4] Patent: WO2007/127726, 2007, A2. Location in patent: Page/Page column 40
[5] Journal of the Chemical Society, 1931, p. 79,81
3,5-Dichloro-4-methylaniline Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-Dichloro-4-methylaniline manufacturers
- Product
- 3,5-Dichloro-4-methylaniline 54730-35-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-12-17