ChemicalBook > CAS DataBase List > 3,5-Dichloro-4-methylaniline

3,5-Dichloro-4-methylaniline

Product Name: 3,5-Dichloro-4-methylaniline
CAS No.: 54730-35-7
Chemical Name: 3,5-Dichloro-4-methylaniline
Synonyms: SKL201;3,5-Dichloro-4-methylaniline;3,5-Dichloro-4-methylbenzenamine;BenzenaMine, 3,5-dichloro-4-Methyl-
CBNumber: CB81510074
Molecular Formula: C7H7Cl2N
Formula Weight: 176.04
MOL File: 54730-35-7.mol

Less

3,5-Dichloro-4-methylaniline Property

Melting point:: 57-59 °C
Boiling point:: 284.6±35.0 °C(Predicted)
Density: 1.334±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: Chloroform (Slightly), DMSO (Slightly)
form: Solid
pka: 2.92±0.10(Predicted)
color: Beige to Brown

Less

Safety

HS Code: 2921490090

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Less

N-Bromosuccinimide Price

TRC

Product number: D435125
Product name: 3,5-Dichloro-4-methylaniline
Packaging: 500mg
Price: $65
Updated: 2021/12/16

TRC

Product number: D435125
Product name: 3,5-Dichloro-4-methylaniline
Packaging: 250mg
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD139569
Product name: 3,5-Dichloro-4-methylaniline
Packaging: 2g
Price: $65
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0059160
Product name: 3,5-DICHLORO-4-METHYLANILINE
Purity: 95.00%
Packaging: 2.5G
Price: $1147.43
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0059160
Product name: 3,5-DICHLORO-4-METHYLANILINE
Purity: 95.00%
Packaging: 5G
Price: $1421.65
Updated: 2021/12/16

Less

3,5-Dichloro-4-methylaniline Chemical Properties,Usage,Production

Synthesis

7149-69-1

54730-35-7

General procedure for the synthesis of 3,5-dichloro-4-methylaniline from 1,3-dichloro-2-methyl-5-nitrobenzene: First, 1,3-dichloro-2-methyl-5-nitrobenzene (0.50 g, 2.43 mmol) was dissolved in N,N-dimethylformamide (DMF). Subsequently, tin(II) chloride dihydrate (2.74 g, 12.1 mmol) was added all at once. The reaction mixture was stirred at room temperature for 1 hour. After completion of the reaction, the reaction mixture was diluted with ethyl acetate and filtered through a diatomaceous earth pad. The filtrate was sequentially washed four times with water and twice with brine and then dried with anhydrous magnesium sulfate. The dried organic phase was filtered and concentrated to give a dark-colored oil. Finally, the residue was purified by silica gel column chromatography using a gradient elution with 5% to 10% ethyl acetate in hexane solution to give 342 mg (80% yield) of 3,5-dichloro-4-methylaniline as a white flaky solid.

References

[1] Gazzetta Chimica Italiana, 1996, vol. 126, # 3, p. 179 - 185
[2] Tetrahedron, 1998, vol. 54, # 12, p. 2953 - 2966
[3] Patent: WO2007/127763, 2007, A2. Location in patent: Page/Page column 37
[4] Patent: WO2007/127726, 2007, A2. Location in patent: Page/Page column 40
[5] Journal of the Chemical Society, 1931, p. 79,81

3,5-Dichloro-4-methylaniline Preparation Products And Raw materials

Raw materials

Preparation Products

Less

3,5-Dichloro-4-methylaniline Suppliers

China 59 India 1 Switzerland 1 United Kingdom 1 United States 5 Global 67

Capot Chemical Co., Ltd

Tel: +86 (0) 571 85 58 67 18
Fax: 0086-571-85864795
Country: China
ProdList: 18207
Advantage: 66

Shanghai Harvest Chemical Industrial Co., Ltd.

Tel: 021-31038972,31038973 17321035817
Fax: +86-21-51385350
Email: sales@harvest-chem.com
Country: China
ProdList: 2816
Advantage: 64

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

Shanghai Sunway Pharmaceutical Technology Co., Ltd

Tel: 18270980682
Fax: 021 51613951
Email: mlcheng@sunwaypharm.cn
Country: China
ProdList: 8669
Advantage: 57

Hangzhou Sage Chemical Co., Ltd.

Tel: +86057186818502 13588463833
Fax: Pls mail us for more information!
Email: info@sagechem.com
Country: China
ProdList: 10266
Advantage: 58

Suzhou Sibian Chemical Technology Co.,Ltd.

Tel: 0512-65617459 18915409046
Fax: 0512-65617459
Email: sales@sibian-chem.com
Country: China
ProdList: 1922
Advantage: 55

Shanghai Topbiochem Technology Co., Ltd

Tel: +86-21-60341587
Fax: +86-21-61294319
Email: sales@topbiochem.com
Country: China
ProdList: 6175
Advantage: 58

SynAsst Chemical.

Tel: 021-60343070
Fax: 021-35122006
Country: China
ProdList: 12740
Advantage: 55

Tianjin Anhao Biological Technology Co., Ltd.

Tel
Email: sales@ahpharmatech.com
Country: China
ProdList: 5734
Advantage: 55

Shanghai HuanChuan Industry Co.,Ltd.

Tel: 021-61478794
Fax: 021-61478794
Email: sales@hcshhai.com
Country: China
ProdList: 9793
Advantage: 50

Shanghai Yongye Biotechnology Co., Ltd.

Tel: 86-021-61559134 15921386130
Fax: 021-55068248
Email: 3423497944@qq.com
Country: China
ProdList: 8144
Advantage: 55

Shanghai Jovan Biochemical Technology Co. Ltd.

Tel: +86-021-61654350
Fax: +86-021-61654350
Email: 1245958370@qq.com
Country: China
ProdList: 2982
Advantage: 50

Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

Tel: 025-66028182 18626450290
Email: yftan@aikonchem.com
Country: China
ProdList: 16679
Advantage: 50

Changzhou Anxuan Chemical, Co., Ltd.

Tel: 13912302692 13912302692;
Fax: 0519-88064678
Email: sales@anxuanchem.com
Country: China
ProdList: 4828
Advantage: 58

NovoChemy Ltd.

Tel: 86-(0)21-31261262 373522135
Fax: 86-(0)21-33250524
Email: sales@novochemy.com
Country: China
ProdList: 6498
Advantage: 58

Zhengzhou AiXi Technology Co., Ltd.

Tel: 0371-56787280 13137706083
Fax: -
Email: m18539565376@163.com
Country: China
ProdList: 970
Advantage: 55

Chengdu Xiaojia Technology Co., Ltd.

Tel: 15902830537
Email: zhanghao@happysyn.com
Country: China
ProdList: 3180
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Shanghai CR Corporation Limited

Tel: 13062833949; 4006653949 4006653949
Fax: QQ: 2136646215
Email: fred.wen@crcorporation.cn
Country: China
ProdList: 9754
Advantage: 58

Hangzhou Molcore Biopharmatech Co.,Ltd

Tel: 400-711-5280 86-571-81025280
Fax: 86-571-85806285
Email: sales@molcore.com
Country: China
ProdList: 9967
Advantage: 58

Capot Chemical Co.,Ltd.

Tel: +86-（0）57185586718; +8613336195806
Fax: +86-571-85864795
Email: sales@capot.com
Country: China
ProdList: 29735
Advantage: 60

Nanjing SynTitan Pharmaceutical Co., Ltd.

Tel: 025-57027686 17372956142
Fax: 025-57027686
Email: li_lan@syntitan.com
Country: China
ProdList: 9998
Advantage: 58

Shanghai SPAR pharmaceutical technology co., LTD

Tel: 021-000000
Email: admin@jingshipharmatech.com
Country: China
ProdList: 9852
Advantage: 58

Hefei TNJ Chemical Industry Co.,Ltd.

Tel: +86-0551-65418671 +8618949823763
Fax: 0551-65418697
Email: sales@tnjchem.com
Country: China
ProdList: 34563
Advantage: 58

Labnetwork lnc.

Tel: +86-27-50766799 +8618062016861
Email: contact@labnetwork.com
Country: China
ProdList: 19987
Advantage: 58

CD Chemical Group Limited

Tel: +8615986615575
Fax: 0086-13651442114
Email: info@codchem.com
Country: China
ProdList: 20342
Advantage: 58

Win-Win chemical CO., Limited

Tel: +86-0086-577-64498589 +86-15355981851
Fax: 0086-577-56994596
Email: sales@win-winchemical.com
Country: China
ProdList: 14359
Advantage: 58

Henan Weituxi Chemical Technology Co., Ltd.

Tel: 0371-63284658 18135795563
Fax: QQ:2885349392
Email: 2885349392@qq.com
Country: China
ProdList: 9989
Advantage: 58

Chemwill Asia Co.,Ltd.

Tel: 86-21-51086038
Fax: 86-21-51861608
Email: chemwill_asia@126.com
Country: CHINA
ProdList: 23912
Advantage: 58

Zhejiang Lianshuo Biotechnology Co., Ltd.

Tel: 18616526224
Email: lianshuo@vip.126.com
Country: China
ProdList: 9607
Advantage: 58

Qi Qi hang Biotechnology Co., Ltd.

Tel: 18151111370
Email: 1046215251@qq.com
Country: China
ProdList: 5999
Advantage: 58

Tianjin Nuokang Pharmaceutical Technology Co., Ltd.

Tel: 022-23989838 13810451150
Email: 44766350@qq.com
Country: China
ProdList: 2349
Advantage: 58

CONIER CHEM AND PHARMA LIMITED

Tel: +8618523575427
Email: sales@conier.com
Country: China
ProdList: 49975
Advantage: 58

career henan chemical co

Tel: +86-0371-86658258 +8613203830695
Fax: 0086-371-86658258
Email: factory@coreychem.com
Country: China
ProdList: 29798
Advantage: 58

Shaanxi Dideu Medichem Co. Ltd

Tel: +86-29-87569266 +86-17392581500
Fax: 029-88380327
Email: 1015@dideu.com
Country: China
ProdList: 3987
Advantage: 58

Beijing Haite lesk Technology Co., Ltd

Tel: 15210893940; 15116916250
Fax: QQ: 237008221
Email: chemistryliu@163.com
Country: China
ProdList: 7327
Advantage: 58

Fuxin Pharmaceutical

Tel: +86-021-021-50872116 +8613122107989
Email: contact@fuxinpharm.com
Country: China
ProdList: 10000
Advantage: 58

Guangzhou Yuheng Pharmaceutical Technology Co., Ltd

Tel: +8613580539051
Email: joe@yuhengpharm.com
Country: CHINA
ProdList: 21142
Advantage: 58

Shanghai Sunmonth Technology Co., LTD

Tel: 15216675652
Email: xuanyuelj@163.com
Country: China
ProdList: 2864
Advantage: 58

Shanghai Xiushi Biomedical Co., LTD

Tel: 15002184385 15021598081 15002184385
Email: product001@xiushipharm.com
Country: China
ProdList: 4719
Advantage: 58

Shandong Territorial sea Biological Technology Co., LTD

Tel: 15092083467
Email: 18660263263@163.com
Country: China
ProdList: 2811
Advantage: 58

QUALITY CONTROL SOLUTIONS LTD.

Tel: +86-0755-66853366 +86-13670046396
Email: export03@qcsrm.com
Country: China
ProdList: 24342
Advantage: 58

ChemeGen

Tel: 18818260767
Fax: QQ 3610331285
Email: 2625930290@qq.com
Country: China
ProdList: 6973
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-1647117 13681763483
Email: product02@bidepharm.com
Country: China
ProdList: 59936
Advantage: 58

Jiaxing Zhejia Biotechnology Co., LTD

Tel: 0573-85609002 18367600069;
Email: zhejia01@163.com
Country: China
ProdList: 8887
Advantage: 58

Henan Evonik Biotechnology Co. LTD

Tel: 15672878902
Email: hnyingchuang@163.com
Country: China
ProdList: 3905
Advantage: 58

Zhengzhou Hong Sheng Pharmaceutical Technology Co. Ltd.

Tel: 0371-55695890 15637198702
Email: 1677336983@qq.com
Country: China
ProdList: 13191
Advantage: 58

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 18621169109
Email: market03@meryer.com
Country: China
ProdList: 27987
Advantage: 58

Shanghai Haohong Scientific Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Less

View Lastest Price from 3,5-Dichloro-4-methylaniline manufacturers

Career Henan Chemical Co

Product: 3,5-Dichloro-4-methylaniline 54730-35-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-12-17

54730-35-7, 3,5-Dichloro-4-methylanilineRelated Search:

6-Amino-2,4-dichloro-3-methylphenol hydrochloride 6-Acetamino-2,4-dichloro-3-methylphenol Diclazuril 2,4-Dichloro-3-ethyl-6-nitrophenol N-(3,5-DICHLORO-2-HYDROXY-4-METHYLPHENYL)-2-(2,4-DI-TERT-PENTYLPHENOXY)-ACETAMIDE 2,4-Dichloro-3-methyl-6-nitrophenol 2-[2,4-Bis(tert-pentyl)phenoxy]-N-(3,5-dichloro-2-hydroxy-p-tolyl)butyramide Letrazuril 1,3-DICHLORO-2-METHYL-5-NITROBENZENE 2,4-Dichloro-3-ethyl-6-aminophenol hydrochloride 3,5-Dichloro-4-methylaniline 2,4-DICHLORO-3,5-DIMETHYL-6-NITROPHENOL 3,5-DICHLORO-4-(TRIFLUOROMETHYL)ANILINE 2,6-DICHLORO-4-AMINO ACETOPHENONE RARECHEM AL BO 2267 3',5'-DICHLOROFOLIC ACID 4-AMINO-2,6-DICHLORO-ALPHA-(4-CHLOROPHENYL)BENZYL CYANIDE 1,3,4-TRICHLORO-2-ETHYL-5-NITROBENZENE

3,5-Dichloro-4-methylaniline

BenzenaMine, 3,5-dichloro-4-Methyl-

3,5-Dichloro-4-methylbenzenamine

SKL201

54730-35-7