7-Chloro-1H-indole-3-carbaldehyde
- Product Name
- 7-Chloro-1H-indole-3-carbaldehyde
- CAS No.
- 1008-07-7
- Chemical Name
- 7-Chloro-1H-indole-3-carbaldehyde
- Synonyms
- 7-CHLORO-3-FORMYLINDOLE;7-Chloro-3-formyl-1H-indole;7-Chloroindole-3-carbaldehyde;7-Chloro-3-indolecarboxaldehyde;7-Chloro-1H-indol-3-carbaldehyde;7-CHLORO-1H-INDOLE-3-CARBALDEHYDE;1H-Indole-3-carboxaldehyde, 7-chloro-;7-chloro-3-formylindole, CAS 1008-07-7
- CBNumber
- CB81519693
- Molecular Formula
- C9H6ClNO
- Formula Weight
- 179.6
- MOL File
- 1008-07-7.mol
7-Chloro-1H-indole-3-carbaldehyde Property
- Melting point:
- 181-182 °C(Solv: ethyl acetate (141-78-6))
- Boiling point:
- 373.4±22.0 °C(Predicted)
- Density
- 1.431±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 13.92±0.30(Predicted)
- Appearance
- White to yellow Solid
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B418635
- Product name
- 7-Chloro-1H-indole-3-carbaldehyde
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 0274AA
- Product name
- 7-Chloro-1H-indole-3-carbaldehyde
- Packaging
- 100mg
- Price
- $73
- Updated
- 2021/12/16
- Product number
- FC144366
- Product name
- 7-Chloro-1H-indole-3-carbaldehyde
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 024709
- Product name
- 7-Chloroindole-3-carboxaldehyde
- Purity
- 98%
- Packaging
- 1g
- Price
- $92
- Updated
- 2021/12/16
- Product number
- FC144366
- Product name
- 7-Chloro-1H-indole-3-carbaldehyde
- Packaging
- 1g
- Price
- $120
- Updated
- 2021/12/16
7-Chloro-1H-indole-3-carbaldehyde Chemical Properties,Usage,Production
Synthesis
53924-05-3
1008-07-7
The general procedure for the synthesis of 7-chloro-1H-indole-3-aldehyde from 7-chloro-1H-indole was as follows: phosphoryl chloride (0.66 mL, 7 mmol) was slowly added dropwise to anhydrous DMF (5 mL) at 0 °C and under argon protection. Subsequently, a solution of 7-chloro-1H-indole (1 g, 6.6 mmol) dissolved in anhydrous DMF (15 mL) was added dropwise to the above mixture at room temperature. The reaction mixture was stirred continuously for 2 hours at room temperature. After completion of the reaction, the mixture was slowly poured into a mixture of ice water and saturated NaHCO3 solution and extracted with ethyl acetate. The organic phases were combined, washed with saturated NaCl solution (10 mL x 3), dried over anhydrous MgSO4, filtered and concentrated to give 990 mg of the target product 7-chloro-1H-indole-3-aldehyde as a yellow-orange solid in 83% yield.
References
[1] Patent: US2005/119260, 2005, A1. Location in patent: Page/Page column 36
7-Chloro-1H-indole-3-carbaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 7-Chloro-1H-indole-3-carbaldehyde manufacturers
- Product
- 7-Chloro-1H-indole-3-carbaldehyde 1008-07-7
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-03-19
- Product
- 7-CHLORO-3-FORMYLINDOLE 1008-07-7
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000KG
- Release date
- 2024-07-30
- Product
- 7-chloro-3-forMylindole 1008-07-7
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27