methyl 2-fluoro-3-nitrobenzoate

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methyl 2-fluoro-3-nitrobenzoate

Product Name: methyl 2-fluoro-3-nitrobenzoate
CAS No.: 946126-94-9
Chemical Name: methyl 2-fluoro-3-nitrobenzoate
Synonyms: 2-fluoro-3-nitrobenzoate;methyl 2-fluoro-3-nitrobenzoate;2-Fluoro-3-(methoxycarbonyl)nitrobenzene;Benzoic acid, 2-fluoro-3-nitro-, Methyl ester
CBNumber: CB81553204
Molecular Formula: C8H6FNO4
Formula Weight: 199.14
MOL File: 946126-94-9.mol

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methyl 2-fluoro-3-nitrobenzoate Property

Melting point:: 77- 80° C
Boiling point:: 310.8±27.0 °C(Predicted)
Density: 1.388±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Solid
color: Off-White to Pale Yellow

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Safety

HS Code: 2916310090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M305423
Product name: Methyl2-fluoro-3-nitrobenzoate
Packaging: 500mg
Price: $60
Updated: 2021/12/16

TRC

Product number: M305423
Product name: Methyl2-fluoro-3-nitrobenzoate
Packaging: 1g
Price: $70
Updated: 2021/12/16

AK Scientific

Product number: W9697
Product name: Methyl2-fluoro-3-nitrobenzoate
Packaging: 250mg
Price: $63
Updated: 2021/12/16

Oakwood

Product number: 066784
Product name: Methyl2-Fluoro-3-nitrobenzoate
Purity: 97%
Packaging: 1g
Price: $30
Updated: 2021/12/16

Apolloscientific

Product number: PC49297
Product name: Methyl2-fluoro-3-nitrobenzoate
Purity: 99%
Packaging: 1g
Price: $37
Updated: 2021/12/16

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methyl 2-fluoro-3-nitrobenzoate Chemical Properties,Usage,Production

Uses

Methyl 2-fluoro-3-nitrobenzoate can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.

Synthesis

A solution of 2-fluoro-3-nitrobenzoic acid (5 g, 27.0 mmol) in MeOH (50 mL) was treated with concentrated H2SO4 (1.4 mL, 27.0 mmol) and the resulting reaction was stirred at 50 °C for 16 h. The solvent was removed under reduced pressure and the residue was diluted with EtO Ac. The organic solution was washed with saturated aqueous NaHCO3 solution until the water phase reached neutral pH. The two phases were separated. Organics were washed with water, brine and dried (Na2SO4). The solution was filtered and concentrated to give crude methyl 2-fluoro-3-nitrobenzoate which was used as is in the next step. (5.1 g, 25.2 mmol, 93 %) as a pale yellow solid.

methyl 2-fluoro-3-nitrobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from methyl 2-fluoro-3-nitrobenzoate manufacturers

Shandong Deshang Chemical Co., Ltd.

Product: methyl 2-fluoro-3-nitrobenzoate 946126-94-9
Price: US $8.90-3.20/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10 tons
Release date: 2024-08-20

Hebei Yanxi Chemical Co., Ltd.

Product: methyl 2-fluoro-3-nitrobenzoate 946126-94-9
Price: US $0.00/kg
Min. Order: 1kg
Purity: 0.99
Supply Ability: 20 tons
Release date: 2023-11-27

Hebei Weibang Biotechnology Co., Ltd

Product: methyl 2-fluoro-3-nitrobenzoate 946126-94-9
Price: US $30.00-10.00/KG
Min. Order: 50KG
Purity: 99%
Supply Ability: 500000kg
Release date: 2024-10-24

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946126-94-9