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methyl 2-fluoro-3-nitrobenzoate

Product Name
methyl 2-fluoro-3-nitrobenzoate
CAS No.
946126-94-9
Chemical Name
methyl 2-fluoro-3-nitrobenzoate
Synonyms
2-fluoro-3-nitrobenzoate;methyl 2-fluoro-3-nitrobenzoate;2-Fluoro-3-(methoxycarbonyl)nitrobenzene;Benzoic acid, 2-fluoro-3-nitro-, Methyl ester
CBNumber
CB81553204
Molecular Formula
C8H6FNO4
Formula Weight
199.14
MOL File
946126-94-9.mol
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methyl 2-fluoro-3-nitrobenzoate Property

Melting point:
77- 80° C
Boiling point:
310.8±27.0 °C(Predicted)
Density 
1.388±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform (Slightly), Methanol (Slightly)
form 
Solid
color 
Off-White to Pale Yellow
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Safety

HS Code 
2916310090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
M305423
Product name
Methyl2-fluoro-3-nitrobenzoate
Packaging
500mg
Price
$60
Updated
2021/12/16
TRC
Product number
M305423
Product name
Methyl2-fluoro-3-nitrobenzoate
Packaging
1g
Price
$70
Updated
2021/12/16
AK Scientific
Product number
W9697
Product name
Methyl2-fluoro-3-nitrobenzoate
Packaging
250mg
Price
$63
Updated
2021/12/16
Oakwood
Product number
066784
Product name
Methyl2-Fluoro-3-nitrobenzoate
Purity
97%
Packaging
1g
Price
$30
Updated
2021/12/16
Apolloscientific
Product number
PC49297
Product name
Methyl2-fluoro-3-nitrobenzoate
Purity
99%
Packaging
1g
Price
$37
Updated
2021/12/16
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methyl 2-fluoro-3-nitrobenzoate Chemical Properties,Usage,Production

Uses

Methyl 2-fluoro-3-nitrobenzoate can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.

Synthesis

A solution of 2-fluoro-3-nitrobenzoic acid (5 g, 27.0 mmol) in MeOH (50 mL) was treated with concentrated H2SO4 (1.4 mL, 27.0 mmol) and the resulting reaction was stirred at 50 °C for 16 h. The solvent was removed under reduced pressure and the residue was diluted with EtO Ac. The organic solution was washed with saturated aqueous NaHCO3 solution until the water phase reached neutral pH. The two phases were separated. Organics were washed with water, brine and dried (Na2SO4). The solution was filtered and concentrated to give crude methyl 2-fluoro-3-nitrobenzoate which was used as is in the next step. (5.1 g, 25.2 mmol, 93 %) as a pale yellow solid.

methyl 2-fluoro-3-nitrobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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methyl 2-fluoro-3-nitrobenzoate Suppliers

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View Lastest Price from methyl 2-fluoro-3-nitrobenzoate manufacturers

Henan Fengda Chemical Co., Ltd
Product
Methyl 2-fluoro-3-nitrobenzoate 946126-94-9
Price
US $8.00-0.80/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-01-22
Hebei Yanxi Chemical Co., Ltd.
Product
methyl 2-fluoro-3-nitrobenzoate 946126-94-9
Price
US $0.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
20 tons
Release date
2023-11-27
Hebei Guanlang Biotechnology Co., Ltd.
Product
methyl 2-fluoro-3-nitrobenzoate 946126-94-9
Price
US $30.00-10.00/KG
Min. Order
50KG
Purity
99%
Supply Ability
500000kg
Release date
2022-09-20

946126-94-9, methyl 2-fluoro-3-nitrobenzoateRelated Search:


  • methyl 2-fluoro-3-nitrobenzoate
  • Benzoic acid, 2-fluoro-3-nitro-, Methyl ester
  • 2-Fluoro-3-(methoxycarbonyl)nitrobenzene
  • 2-fluoro-3-nitrobenzoate
  • 946126-94-9