2-AMINO-5-BROMOBENZOPHENONE
- Product Name
- 2-AMINO-5-BROMOBENZOPHENONE
- CAS No.
- 39859-36-4
- Chemical Name
- 2-AMINO-5-BROMOBENZOPHENONE
- Synonyms
- IFLAB-BB F1386-0357;2-BENZOYL-4-BROMOANILINE;2-AMINO-5-BROMOBENZOPHENONE;5-BROMO-2-AMINOBENZOPHENONE;2-Benzoyl-4-bromobenzenamine;2-Amino-5-bromobenzophenone, >=97%;(2-AMINO-5-BROMO-PHENYL)-PHENYL-METHANONE;Methanone, (2-amino-5-bromophenyl)phenyl-;2-Benzoyl-4-bromoaniline 5-Bromo-2-aminobenzophenone
- CBNumber
- CB8170910
- Molecular Formula
- C13H10BrNO
- Formula Weight
- 276.13
- MOL File
- 39859-36-4.mol
2-AMINO-5-BROMOBENZOPHENONE Property
- Melting point:
- 109-113℃
- Boiling point:
- 424.6±35.0 °C(Predicted)
- Density
- 1.484±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- DMF: 30 mg/ml; DMSO: 30 mg/ml; Ethanol: 30 mg/ml
- pka
- -0.01±0.10(Predicted)
- form
- Powder
- color
- Yellow
- InChI
- InChI=1S/C13H10BrNO/c14-10-6-7-12(15)11(8-10)13(16)9-4-2-1-3-5-9/h1-8H,15H2
- InChIKey
- LXJVUGANBDAASB-UHFFFAOYSA-N
- SMILES
- C(C1=CC(Br)=CC=C1N)(C1=CC=CC=C1)=O
- CAS DataBase Reference
- 39859-36-4(CAS DataBase Reference)
Safety
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HS Code
- 2922.39.4500
- HazardClass
- 6.1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- A3311
- Product name
- 2-Amino-5-bromobenzophenone
- Packaging
- 1G
- Price
- $93
- Updated
- 2025/07/31
- Product number
- A3311
- Product name
- 2-Amino-5-bromobenzophenone
- Packaging
- 5G
- Price
- $279
- Updated
- 2025/07/31
- Product number
- A601960
- Product name
- (2-Amino-5-bromophenyl)phenyl-methanone
- Packaging
- 5g
- Price
- $140
- Updated
- 2021/12/16
- Product number
- 119112
- Product name
- 2-Benzoyl-4-bromoaniline
- Purity
- 95+%
- Packaging
- 1g
- Price
- $118
- Updated
- 2021/12/16
- Product number
- FA140254
- Product name
- (2-Amino-5-bromophenyl)(phenyl)methanone
- Packaging
- 2g
- Price
- $104
- Updated
- 2021/12/16
2-AMINO-5-BROMOBENZOPHENONE Chemical Properties,Usage,Production
Chemical Properties
Pale Yellow Solid
Uses
2-Amino-5-bromobenzophenone is a benzophenone (B204980) derivative that is widely used in the synthesis of pharmaceutical compounds.
Synthesis
2835-77-0
39859-36-4
The general procedure for the synthesis of 2-benzoyl-4-bromoaniline from 2-aminobenzophenone is as follows: reference is made to the synthesis of Example A16 (2-amino-5-bromophenyl)-phenyl-methanone, which can be accessed from US 20040127536 A1 and is based on the work of D. Roche, K. Prasad, O. Repic, TJ Blacklock in Tetrahedron Lett. 41, 2083-2085 (2000). This was done as follows: 2-aminobenzophenone (30 g, 152 mmol) was suspended in acetic acid (300 mL). Potassium bromide (19.9 g, 167 mmol), sodium perborate tetrahydrate (28 g, 183 mmol) and ammonium molybdate tetrahydrate (1.5 g) were subsequently added and the mixture was stirred continuously for 3 h at 0 °C. The dense yellow precipitate formed during the reaction was washed with ice water (300 mL) and subsequently separated by filtration, washed again with ice water and dried. Finally, 40.3 g (96% yield) of yellow solid product was obtained. Mass spectrometry analysis showed: m/z = 276 (M).
References
[1] Tetrahedron, 2007, vol. 63, # 13, p. 2811 - 2823
[2] Patent: US2006/94754, 2006, A1. Location in patent: Page/Page column 11
[3] Organic Letters, 2010, vol. 12, # 12, p. 2841 - 2843
[4] Chemical Communications, 2010, vol. 46, # 29, p. 5244 - 5246
[5] European Journal of Organic Chemistry, 2017, vol. 2017, # 31, p. 4600 - 4608
2-AMINO-5-BROMOBENZOPHENONE Preparation Products And Raw materials
Raw materials
Preparation Products
2-AMINO-5-BROMOBENZOPHENONE Suppliers
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View Lastest Price from 2-AMINO-5-BROMOBENZOPHENONE manufacturers
- Product
- 2-AMINO-5-BROMOBENZOPHENONE 39859-36-4
- Price
- US $10.00/ASSAYS
- Min. Order
- 1ASSAYS
- Purity
- 99%
- Supply Ability
- 1 ton
- Release date
- 2025-08-05
- Product
- 2-AMINO-5-BROMOBENZOPHENONE 39859-36-4
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2024-11-26
- Product
- 2-AMINO-5-BROMOBENZOPHENONE 39859-36-4
- Price
- US $1.00/kg
- Min. Order
- 2kg
- Purity
- 2-AMINO-5-BROMOBENZOPHENONE
- Supply Ability
- 100
- Release date
- 2024-10-25