ChemicalBook > CAS DataBase List > N-ME-PHE-OME HCL

N-ME-PHE-OME HCL

Product Name
N-ME-PHE-OME HCL
CAS No.
19460-86-7
Chemical Name
N-ME-PHE-OME HCL
Synonyms
N-Me-Phe-OMe;N-ME-PHE-OME HCL;H-ME-PHE-OME HCL;H-L-MEPHE-OME HCL;N-Me-L-Phe-OMe·HCl;N-Me-Phe-OMe hydrochoride;N-ME-PHENYLALANINE-OME HCL;N-ME-PHE-OME HCL USP/EP/BP;N-Methyl-L-phenylalanine methyl ester HCl;Methyl methyl-L-phenylalaninate hydrochloride
CBNumber
CB8184759
Molecular Formula
C11H16ClNO2
Formula Weight
229.7
MOL File
19460-86-7.mol
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N-ME-PHE-OME HCL Property

storage temp. 
Sealed in dry,Room Temperature
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

H334May cause allergy or asthma symptoms or breathing difficulties if inhaled

H350May cause cancer

H372Causes damage to organs through prolonged or repeated exposure

Precautionary statements

P201Obtain special instructions before use.

P202Do not handle until all safety precautions have been read and understood.

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P272Contaminated work clothing should not be allowed out of the workplace.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P284Wear respiratory protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P308+P313IF exposed or concerned: Get medical advice/attention.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
M335050
Product name
N-Me-Phe-OMehydrochoride
Packaging
100mg
Price
$65
Updated
2021/12/16
Usbiological
Product number
283842
Product name
N-alpha-Methyl-L-phenylalanine methyl ester hydrochloride
Packaging
250mg
Price
$368
Updated
2021/12/16
Chem-Impex
Product number
06354
Product name
Nα-Methyl-L-phenylalaninemethylesterhydrochloride,98%(HPLC)
Purity
98%(HPLC)
Packaging
100MG
Price
$56
Updated
2021/12/16
Chem-Impex
Product number
06354
Product name
-Methyl-L-phenylalanine methyl ester hydrochloride
Purity
≥ 98% (HPLC)
Packaging
250MG
Price
$90
Updated
2021/12/16
Activate Scientific
Product number
AS112830
Product name
N-Me-Phe-OMe HCl
Purity
97%
Packaging
1g
Price
$170
Updated
2021/12/16
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N-ME-PHE-OME HCL Chemical Properties,Usage,Production

Chemical Properties

White powder

Uses

N-Me-Phe-OMe HCl

Synthesis

37553-64-3

19460-86-7

GENERAL PROCEDURE: To a stirring solution of Nα-Boc-protected peptide (1 mmol) in dichloromethane (2 mL) was slowly added a solution of 3.3 M HCl in dioxane (5 mL) at 0 °C. The reaction system was gradually warmed up to 20 °C and maintained at this temperature for 1 hour. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure. The residue was placed in anhydrous ether and stirred to induce precipitation of the crystalline product. For poorly crystalline or strongly hygroscopic compounds, the residue is dissolved in dry chloroform, the solvent is subsequently evaporated, and the product is placed in a vacuum desiccator and dried using P4O10 or KOH as the desiccant. Part of the product needs to be purified by silica gel column chromatography using eluent mixture B or gel filtration through biogel P2 or Fractogel TCK HW 40 followed by lyophilization to obtain the pure product.

References

[1] Tetrahedron, 2012, vol. 68, # 35, p. 7070 - 7076

N-ME-PHE-OME HCL Preparation Products And Raw materials

Raw materials

Preparation Products

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