7-Chloro-1,2,3,4-tetrahydroquinoline

Product Name: 7-Chloro-1,2,3,4-tetrahydroquinoline
CAS No.: 90562-35-9
Chemical Name: 7-Chloro-1,2,3,4-tetrahydroquinoline
Synonyms: 7-Chloro-1,2,3,4-tetrahydroquinoline;Quinoline, 7-chloro-1,2,3,4-tetrahydro-
CBNumber: CB82550091
Molecular Formula: C9H10ClN
Formula Weight: 167.64
MOL File: 90562-35-9.mol

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7-Chloro-1,2,3,4-tetrahydroquinoline Property

Boiling point:: 273.0±29.0 °C(Predicted)
Density: 1.162±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
pka: 4.26±0.20(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933491090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C384628
Product name: 7-Chloro-1,2,3,4-tetrahydroquinoline
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Ark Pharm

Product number: P000246398
Product name: 7-Chloro-1,2,3,4-tetrahydroquinoline
Purity: 95+%
Packaging: 100mg
Price: $43
Updated: 2021/12/16

Ark Pharm

Product number: P000246398
Product name: 7-Chloro-1,2,3,4-tetrahydroquinoline
Purity: 95+%
Packaging: 1g
Price: $128
Updated: 2021/12/16

Apolloscientific

Product number: OR933042
Product name: 7-Chloro-1,2,3,4-tetrahydroquinoline
Purity: >98%
Packaging: 1g
Price: $270
Updated: 2021/12/16

Ark Pharm

Product number: P000246398
Product name: 7-Chloro-1,2,3,4-tetrahydroquinoline
Purity: 95+%
Packaging: 5g
Price: $404
Updated: 2021/12/16

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7-Chloro-1,2,3,4-tetrahydroquinoline Chemical Properties,Usage,Production

Synthesis

612-61-3

90562-35-9

General procedure for the synthesis of 7-chloro-1,2,3,4-tetrahydroquinoline from 7-chloroquinoline: In a 10 mL Schlenk tube, Fe(OTf)2 (0.005 mmol, 1.8 mg), 7-chloroquinoline (0.5 mmol, 72 mg), Hantzsch ester A (1.25 mmol, 318 mg) and 1.0 mL of CHCl3. The reaction mixture was stirred at 40 °C for 2 hours. After completion of the reaction, the reaction solution was concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography to afford pure 7-chloro-1,2,3,4-tetrahydroquinoline (63.8 mg, 96% yield).

References

[1] Journal of the American Chemical Society, 2018, vol. 140, # 12, p. 4417 - 4429
[2] Tetrahedron Letters, 2017, vol. 58, # 36, p. 3571 - 3573
[3] Patent: US2003/229026, 2003, A1. Location in patent: Page 25

7-Chloro-1,2,3,4-tetrahydroquinoline Preparation Products And Raw materials

Raw materials

Preparation Products

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7-Chloro-1,2,3,4-tetrahydroquinoline Suppliers

China 46 India 1 United States 2 Global 49

PharmaBlock Sciences (Nanjing),Inc.

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7-Chloro-1,2,3,4-tetrahydroquinoline

Quinoline, 7-chloro-1,2,3,4-tetrahydro-

90562-35-9