3-SULFAMOYL-BENZOIC ACID

Product Name: 3-SULFAMOYL-BENZOIC ACID
CAS No.: 636-76-0
Chemical Name: 3-SULFAMOYL-BENZOIC ACID
Synonyms: Nsc22977;NSC 85501;BUTTPARK 148\07-55;3-sulfaMoylbenzoate;3-SULFAMOYL-BENZOIC;TIMTEC-BB SBB010997;3-Sulfamoylbenzoicaci;3-Sulfamylbenzoic acid;m-Sulfamidobenzoic acid;m-Sulfamoylbenzoic acid
CBNumber: CB8334565
Molecular Formula: C7H7NO4S
Formula Weight: 201.2
MOL File: 636-76-0.mol

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3-SULFAMOYL-BENZOIC ACID Property

Melting point:: 251-252℃
Boiling point:: 476.1±47.0 °C(Predicted)
Density: 1.536±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: pK1:3.54 (25°C)
Appearance: White to off-white Solid

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Safety

Hazard Codes: Xi
Risk Statements: 36
Safety Statements: 26-24/25-22
HazardClass: IRRITANT
HS Code: 29350090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: W7552
Product name: 3-Sulfamoylbenzoicacid
Packaging: 250mg
Price: $26
Updated: 2021/12/16

ChemScene

Product number: CS-W000555
Product name: 3-Sulfamoylbenzoicacid
Purity: 97.77%
Packaging: 1g
Price: $52
Updated: 2021/12/16

AK Scientific

Product number: J51005
Product name: 3-Sulfamoylbenzoicacid
Packaging: 1g
Price: $65
Updated: 2021/12/16

Matrix Scientific

Product number: 033834
Product name: 3-Sulfamoyl-benzoic acid
Packaging: 500mg
Price: $155
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK166248
Product name: 3-Sulfamoylbenzoicacid
Packaging: 1g
Price: $159
Updated: 2021/12/16

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3-SULFAMOYL-BENZOIC ACID Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

4025-64-3

636-76-0

General procedure for the synthesis of 3-sulfobenzoic acid from 3-chlorosulfonylbenzoic acid: 25 g of 3-(chlorosulfonyl)benzoic acid (commercially available, Aldrich) was added in batches to 250 mL of 25% ammonium hydroxide solution under ice bath conditions. The reaction mixture was stirred at room temperature for 15 hours. Upon completion of the reaction, the solvent was concentrated by distillation under reduced pressure to about 50 mL. Subsequently, the mixture was acidified with concentrated hydrochloric acid to pH < 2. The precipitated white solid was collected by filtration and dried with a vacuum desiccator to afford 22 g (96% yield) of 3-sulfobenzoic acid. The product was characterized as follows: 1H NMR (DMSO-d6) δ 13.44 (br s, 1H), 8.38 (s, 1H), 8.14 (d, J = 7.5 Hz, 1H), 8.04 (d, J = 7.9 Hz, 1H), 7.72 (t, J = 7.9 Hz, 1H), 7.49 (s, 2H); HPLC (max plot) 97%; Rt 0.68 min; LC/MS (ES-): 199.8.

References

[1] Patent: WO2007/23186, 2007, A1. Location in patent: Page/Page column 45
[2] European Journal of Medicinal Chemistry, 2014, vol. 89, p. 503 - 523
[3] Journal of the American Chemical Society, 2011, vol. 133, # 40, p. 16235 - 16242
[4] ChemMedChem, 2015, vol. 10, # 9, p. 1548 - 1558
[5] Patent: US2013/35364, 2013, A1. Location in patent: Paragraph 0233-0235

3-SULFAMOYL-BENZOIC ACID Preparation Products And Raw materials

Raw materials

Hexane Ammonium hydroxide Sodium sulfate Chlorosulfonic acid Ethyl acetate Hydrochloric acid Benzoic acid

Preparation Products

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3-SULFAMOYL-BENZOIC ACID Suppliers

China 71 Germany 2 India 2 Switzerland 1 Ukraine 1 United Kingdom 4 United States 13 Global 94

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636-76-0, 3-SULFAMOYL-BENZOIC ACIDRelated Search:

3-[(Methylamino)sulphonyl]benzoic acid Sodium 3-nitrobenzenesulphonate 4-Chloro-3-nitro-5-sulphamoylbenzoic acid 4-AMINOSULFONYL-1-HYDROXY-2-NAPHTHOIC ACID, 97 2-CHLORO-5-SULFAMOYLBENZOIC ACID 2,4-Dichloro-5-sulfamoylbenzoic acid 2-Methoxy-5-sulfamoylbenzoic acid 2-Aminobenzoic acid-5-sulfonamide Bumetanide 4-Chloro-5-sulphamoylbenzoic acid Furosemide Methyl 5-(aminosulfonyl)-2,4-dichlorobenzoate 4-METHYL-3-(MORPHOLINE-4-SULFONYL)BENZOIC ACID 2-chloro-5-(methylsulphamoyl)benzoic acid 2-HYDROXY-5-(MORPHOLINE-4-SULFONYL)-BENZOIC ACID 2-CHLORO-5-(MORPHOLINE-4-SULFONYL)-BENZOIC ACID 4-METHYL-3-SULFAMOYLBENZOIC ACID 2-fluoro-5-[(2-fluorophenyl)sulfamoyl]benzoic acid

BUTTPARK 148\07-55

3-SULFAMOYL-BENZOIC ACID

TIMTEC-BB SBB010997

Benzoic acid, 3-(aminosulfonyl)-

M-carboxybenzenesulfonamide

m-Sulfamoylbenzoic acid

Nsc22977

3-SULFAMOYL-BENZOIC

3-sulfaMoylbenzoate

3-Sulfamoyl-benzoic acid ,97%

m-Sulfamidobenzoic acid

NSC 85501

3-Sulfamylbenzoic acid

3-Sulfamoylbenzoicaci

636-76-0

Acids and Derivatives

Boron, Nitrile, Thio,& TM-Cpds