ChemicalBook > CAS DataBase List > ETHYL DIBROMOACETATE

ETHYL DIBROMOACETATE

Product Name: ETHYL DIBROMOACETATE
CAS No.: 617-33-4
Chemical Name: ETHYL DIBROMOACETATE
Synonyms: ethyl 2,2-dibroMoacetate;ETHYL DIBROMOACETATE;dibromo-aceticaciethylester;Dibromoacetic acid, ethyl ester;Ethyl dibromoacetate, tech., 83%;Ethyl dibromoacetate , 83%, tech.;Ethyl dibromoacetate, pract., 95%;Acetic acid, dibromo-, ethyl ester;Acetic acid, 2,2-dibromo-, ethyl ester
CBNumber: CB8338109
Molecular Formula: C4H6Br2O2
Formula Weight: 245.9
MOL File: 617-33-4.mol

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ETHYL DIBROMOACETATE Property

Melting point:: 76-78°
Boiling point:: 77 °C (12 mmHg)
Density: 1.902
refractive index: 1.492-1.502
Flash point:: 76-78°C/12mm
storage temp.: RT, stored under nitrogen
solubility: Soluble in hexane, ether, CH2Cl2, acetone, EtOAc, ethanol.
Appearance: Colorless to light yellow Liquid
EPA Substance Registry System: Acetic acid, dibromo-, ethyl ester (617-33-4)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 37/39-26
RIDADR: 3265
TSCA: Yes

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0142130
Product name: ETHYL DIBROMOACETATE
Purity: 95.00%
Packaging: 500G
Price: $5135.13
Updated: 2021/12/16

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ETHYL DIBROMOACETATE Chemical Properties,Usage,Production

Description

Ethyl dibromoacetate is used in preparation of α-bromo and α,α-dialkyl substituted esters; undergoes Reformatsky/Darzens reactions with aldehydes and ketones.

Chemical Properties

clear colorless to slighlty brown liquid

Uses

Ethyl dibromoacetate can be used to produce diphenoxy-acetic acid ethyl ester. It is used in organic synthesis.

Purification Methods

Wash the ester briefly with conc aqueous NaHCO3, then with aqueous CaCl2. Dry it with CaSO4 and distil it under reduced pressure. [Hornyak & Amis J Am Chem Soc 79 2079 1957, Beilstein 2 H 219, 2 I 97, 2 III 484, 2 IV 533.]

ETHYL DIBROMOACETATE Preparation Products And Raw materials

Raw materials

Preparation Products

ETHYL 1,3-DITHIOLANE-2-CARBOXYLATE

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617-33-4, ETHYL DIBROMOACETATERelated Search:

Lactofen Ethyl bromodifluoroacetate Bromoacetic acid Ethyl bromoacetate DIBROMOACETIC ACID ETHYL DIBROMOACETATE ETHYL TRIFLUOROACETYLDIBROMOACETATE 3,3-dibromodihydro-5-methylfuran-2(3H)-one 5,5-DIBROMOMELDRUM'S ACID benzyl tribromoacetate Ethyl dibromofluoroacetate DIETHYL DIBROMOMALONATE RARECHEM AL BI 0117

Ethyl dibromoacetate, tech., 83%

Ethyl dibromoacetate , 83%, tech.

ethyl 2,2-dibroMoacetate

ETHYL DIBROMOACETATE

Acetic acid, dibromo-, ethyl ester

Dibromoacetic acid, ethyl ester

dibromo-aceticaciethylester

Ethyl dibromoacetate, pract., 95%

Acetic acid, 2,2-dibromo-, ethyl ester

617-33-4

Br2CHCOOC2H5

Br2CHCO2CH2CH3