3-Morpholinobenzaldehyde
Uses- Product Name
- 3-Morpholinobenzaldehyde
- CAS No.
- 446866-87-1
- Chemical Name
- 3-Morpholinobenzaldehyde
- Synonyms
- 3-MORPHOLINOBENZALDEHYDE;4-(3-Formylphenyl)morpholine;3-MORPHOLIN-4-YL-BENZALDEHYDE;3-(4-morpholinyl)benzaldehyde;Benzaldehyde, 3-(4-morpholinyl)-;3-(Morpholin-4-yl)benzaldehyde98%;3-(Morpholin-4-yl)benzaldehyde 98%;3-Morpholinobenzaldehyde ISO 9001:2015 REACH
- CBNumber
- CB8394684
- Molecular Formula
- C11H13NO2
- Formula Weight
- 191.23
- MOL File
- 446866-87-1.mol
3-Morpholinobenzaldehyde Property
- Melting point:
- 68 °C
- Boiling point:
- 357.9±37.0 °C(Predicted)
- Density
- 1.163±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- solid
- pka
- 3.80±0.40(Predicted)
- color
- Yellow
Safety
- Hazard Codes
- Xn
- Risk Statements
- 21/22-36/37/38
- Safety Statements
- 22-26-36/37/39
- Hazard Note
- Harmful
- HS Code
- 2913000090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M725330
- Product name
- 3-Morpholinobenzaldehyde
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR9592
- Product name
- 3-(Morpholin-4-yl)benzaldehyde
- Purity
- 98%
- Packaging
- 1g
- Price
- $113
- Updated
- 2021/12/16
- Product number
- 4H56-1-5T
- Product name
- 3-(Morpholin-4-yl)benzaldehyde
- Packaging
- 1g
- Price
- $181
- Updated
- 2021/12/16
- Product number
- OR9592
- Product name
- 3-(Morpholin-4-yl)benzaldehyde
- Purity
- 98%
- Packaging
- 5g
- Price
- $362
- Updated
- 2021/12/16
- Product number
- 4H56-1-5T
- Product name
- 3-(Morpholin-4-yl)benzaldehyde
- Packaging
- 5G
- Price
- $580
- Updated
- 2021/12/16
3-Morpholinobenzaldehyde Chemical Properties,Usage,Production
Uses
3-Morphyrinylbenzaldehyde can be used as a pharmaceutical synthesis intermediate.
Synthesis
To a 500 mL round-bottomed flask was added 3-bromobenzaldehyde (6.44 g, 35.0 mmol, 1.00 eq.), morpholine (9.13 g, 105 mmol, 3.00 eq.), tris(dibenzylideneacetone)dipalladium (1.81 g, 1.75 mmol, 0.05 eq.), dicyclohexyl(2',6'-diisopropoxybiphenyl-2-yl)phosphine ( 3.26 g, 7.00 mmol, 0.20 equiv), cesium carbonate (34.2 g, 105 mmol) under nitrogen, 3.00 equiv), toluene (100 mL). The resulting solution was stirred overnight at 90??C and quenched with water (50 mL). The resulting solution was extracted with dichloromethane (3 x 200 mL), the organic layers were combined, washed with brine (3 x 100 mL), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The residue was chromatographed on a silica gel column with ethyl acetate/petroleum ether (3/17) to give 3-morpholino benzaldehyde (2.10 g, 32% yield) as a yellow oil.
3-Morpholinobenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Morpholinobenzaldehyde manufacturers
- Product
- 3-Morpholinobenzaldehyde 446866-87-1
- Price
- US $0.00-0.00/KG
- Min. Order
- 10g
- Purity
- 99.0%+
- Supply Ability
- 100 tons
- Release date
- 2019-12-25
- Product
- 3-Morpholinobenzaldehyde 446866-87-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-25