ChemicalBook > CAS DataBase List > 3,6-Dibromo-9-phenyl-9H-carbazole

3,6-Dibromo-9-phenyl-9H-carbazole

Product Name
3,6-Dibromo-9-phenyl-9H-carbazole
CAS No.
57103-20-5
Chemical Name
3,6-Dibromo-9-phenyl-9H-carbazole
Synonyms
DK944;3,6-DibroMo-;3,6-Dibromo-9-phenyL;6-dibroMo -9-phenylcarbazole;3,6-DibroMo-9-phenylarbazole;3,6-DibroMo-N-phenylarbazole;3,6-DIBROMO-9-PHENYLCARBAZOLE;3,6-Dirbomo-9-phenylcarbazole;3,6-Dibromo-9-phenyl-9H-cazole;3,6-Dibromo-9-phenylcaarbazole
CBNumber
CB8409636
Molecular Formula
C18H11Br2N
Formula Weight
401.09
MOL File
57103-20-5.mol
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3,6-Dibromo-9-phenyl-9H-carbazole Property

Melting point:
160-164℃
Boiling point:
505.3±43.0 °C(Predicted)
Density 
1?+-.0.1 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
solubility 
soluble in dichloromethane
form 
powder to crystal
color 
White to Light yellow to Light orange
InChIKey
JBWRZTKHMKVFMQ-UHFFFAOYSA-N
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Safety

Hazard Codes 
Xn
Risk Statements 
22-41
Safety Statements 
26-39-24/25
WGK Germany 
3
HS Code 
29339900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

H413May cause long lasting harmful effects to aquatic life

Precautionary statements

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
731773
Product name
3,6-Dibromo-9-phenylcarbazole
Purity
98%
Packaging
1g
Price
$62.2
Updated
2023/06/20
TCI Chemical
Product number
D2981
Product name
3,6-Dibromo-9-phenylcarbazole
Purity
>98.0%(GC)(N)
Packaging
1g
Price
$41
Updated
2025/07/31
TCI Chemical
Product number
D2981
Product name
3,6-Dibromo-9-phenylcarbazole
Purity
>98.0%(GC)(N)
Packaging
5g
Price
$125
Updated
2025/07/31
TRC
Product number
D422820
Product name
3,6-Dirbomo-9-phenylcarbazole
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
D422820
Product name
3,6-Dirbomo-9-phenylcarbazole
Packaging
100mg
Price
$60
Updated
2021/12/16
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3,6-Dibromo-9-phenyl-9H-carbazole Chemical Properties,Usage,Production

Chemical Properties

off-white powder

Synthesis

1150-62-5

57103-20-5

General procedure for the synthesis of 3,6-dibromo-9-phenylcarbazole from N-phenylcarbazole: 0.1640 moles of N-phenyl-9H-carbazole was added to a 2000 ml three-necked flask, 320 ml of acetic acid and 960 ml of methylene chloride were added to dissolve it, and the reaction system was placed in an ice-water bath for cooling. Slowly 0.3280 moles of liquid bromine was added dropwise and after completion of the dropwise addition, the reaction mixture was stirred and reacted at room temperature overnight. Upon completion of the reaction, the remaining liquid bromine in the reaction solution was neutralized with 1.5 liters of 1 mol/L aqueous sodium hydroxide and the organic phase was separated. The organic phase was washed three times sequentially with water, the organic phase was collected and the solvent was removed by rotary evaporator. The resulting solid was washed with 300 mL of petroleum ether (60-90 °C), filtered, and the solid was dried under vacuum at 55 °C to give 0.1440 mol of the target product 3,6-dibromo-9-phenylcarbazole in 87.8% yield.

References

[1] Organic Electronics: physics, materials, applications, 2014, vol. 15, # 11, p. 2667 - 2676
[2] Tetrahedron, 1998, vol. 54, # 42, p. 12707 - 12714
[3] Journal of Materials Chemistry, 2011, vol. 21, # 25, p. 9139 - 9148
[4] Patent: JP2015/63518, 2015, A. Location in patent: Paragraph 0253; 0254
[5] Patent: CN105906612, 2016, A. Location in patent: Paragraph 0051; 0052

3,6-Dibromo-9-phenyl-9H-carbazole Preparation Products And Raw materials

Raw materials

Preparation Products

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3,6-Dibromo-9-phenyl-9H-carbazole Suppliers

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View Lastest Price from 3,6-Dibromo-9-phenyl-9H-carbazole manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
3,6-DIBROMO-9-PHENYLCARBAZOLE 57103-20-5
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
5tons
Release date
2024-12-03
Shanghai Daken Advanced Materials Co.,Ltd
Product
3,6-Dibromo-9-phenylcarbazole 57103-20-5
Price
US $0.00/KG
Min. Order
1KG
Purity
98.00%
Supply Ability
150KG /month
Release date
2021-11-12
Henan Fengda Chemical Co., Ltd
Product
3,6-Dibromo-9-phenyl-9H-carbazole 57103-20-5
Price
US $200.00-1.00/KG
Min. Order
1KG
Purity
99%, 99.5% Sublimated
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-30

57103-20-5, 3,6-Dibromo-9-phenyl-9H-carbazoleRelated Search:

3-Bromo-9H-carbazole 2,7-Dibromocarbazole 2-HYDROXYCARBAZOLE 2-chloro-9H-carbazole 4-BroMo-9H-carbazole 3,6-BIS(TERT-BUTYL)CARBAZOLE 2-BROMOCARBAZOLE 3,6-DIPHENYL-9H-CARBAZOLE 9H-Carbazole, 3,6-dibromo-9-[4-(dodecyloxy)phenyl]- 3,6-dibromo-9-(4-biphenylyl)carbazole 3,6-dibromo-9-(4-methoxyphenyl)carbazole 3,6-dibromo-9-{4-[(2-ethylhexyl)oxy]phenyl}-9H-carbazole 3,6-dibromo-9-(4-octoxyphenyl)carbazole 9-([1,1'-biphenyl]-3-yl)-3,6-dibromo-9H-carbazole 2,6-DIBROMONAPHTHALENE 3,6-Dibromocarbazole 3,6-Dibromo-9-phenyl-9H-carbazole

  • 3,6-DibroMo-9-phenylarbazole
  • 3,6-DibroMo-9-phenylarbazole,98%
  • 3,6-DibroMo-9-phenylcarbazole,,6-DIBROMO-9-PHENYLCARBAZOLE
  • 3,6-DIBROMO-9-PHENYLCARBAZOLE
  • 3,6-DibroMo-N-phenylarbazole
  • 9H-Carbazole, 3,6-dibroMo-9-phenyl- 3,6-DibroMo-9-phenyl-9H-carbazole
  • 6-dibroMo -9-phenylcarbazole
  • 3,6-DibroMo-
  • 3,6-Dibromo-9-phenylcarbazole&gt
  • 3,6-Dibromo-9-phenyL
  • 9H-Carbazole, 3,6-dibromo-9-phenyl-
  • 3,6-DIBROMO-9-PHENYLCARBAZOLE ISO 9001：2015 REACH
  • 3,6-Dirbomo-9-phenylcarbazole
  • DK944
  • 3,6-Dibromo-N-phenylcarbazole---
  • 3,6-Dibromo-9-phenyl-9H-carbazole
  • 3,6-Dibromo-9-phenylcaarbazole
  • 3,6-Dibromo-9-phenyl-9H-cazole
  • 57103-20-5
  • C18H11Br2N
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