3,6-Dibromo-9-phenyl-9H-carbazole
- Product Name
- 3,6-Dibromo-9-phenyl-9H-carbazole
- CAS No.
- 57103-20-5
- Chemical Name
- 3,6-Dibromo-9-phenyl-9H-carbazole
- Synonyms
- DK944;3,6-DibroMo-;3,6-Dibromo-9-phenyL;6-dibroMo -9-phenylcarbazole;3,6-DibroMo-9-phenylarbazole;3,6-DibroMo-N-phenylarbazole;3,6-DIBROMO-9-PHENYLCARBAZOLE;3,6-Dirbomo-9-phenylcarbazole;3,6-Dibromo-9-phenyl-9H-cazole;3,6-Dibromo-9-phenylcaarbazole
- CBNumber
- CB8409636
- Molecular Formula
- C18H11Br2N
- Formula Weight
- 401.09
- MOL File
- 57103-20-5.mol
3,6-Dibromo-9-phenyl-9H-carbazole Property
- Melting point:
- 160-164℃
- Boiling point:
- 505.3±43.0 °C(Predicted)
- Density
- 1?+-.0.1 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- soluble in dichloromethane
- form
- powder to crystal
- color
- White to Light yellow to Light orange
- InChIKey
- JBWRZTKHMKVFMQ-UHFFFAOYSA-N
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-41
- Safety Statements
- 26-39-24/25
- WGK Germany
- 3
- HS Code
- 29339900
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H318Causes serious eye damage
H413May cause long lasting harmful effects to aquatic life
- Precautionary statements
-
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- 731773
- Product name
- 3,6-Dibromo-9-phenylcarbazole
- Purity
- 98%
- Packaging
- 1g
- Price
- $62.2
- Updated
- 2023/06/20
- Product number
- D2981
- Product name
- 3,6-Dibromo-9-phenylcarbazole
- Purity
- >98.0%(GC)(N)
- Packaging
- 1g
- Price
- $41
- Updated
- 2025/07/31
- Product number
- D2981
- Product name
- 3,6-Dibromo-9-phenylcarbazole
- Purity
- >98.0%(GC)(N)
- Packaging
- 5g
- Price
- $125
- Updated
- 2025/07/31
- Product number
- D422820
- Product name
- 3,6-Dirbomo-9-phenylcarbazole
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- D422820
- Product name
- 3,6-Dirbomo-9-phenylcarbazole
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
3,6-Dibromo-9-phenyl-9H-carbazole Chemical Properties,Usage,Production
Chemical Properties
off-white powder
Synthesis
1150-62-5
57103-20-5
General procedure for the synthesis of 3,6-dibromo-9-phenylcarbazole from N-phenylcarbazole: 0.1640 moles of N-phenyl-9H-carbazole was added to a 2000 ml three-necked flask, 320 ml of acetic acid and 960 ml of methylene chloride were added to dissolve it, and the reaction system was placed in an ice-water bath for cooling. Slowly 0.3280 moles of liquid bromine was added dropwise and after completion of the dropwise addition, the reaction mixture was stirred and reacted at room temperature overnight. Upon completion of the reaction, the remaining liquid bromine in the reaction solution was neutralized with 1.5 liters of 1 mol/L aqueous sodium hydroxide and the organic phase was separated. The organic phase was washed three times sequentially with water, the organic phase was collected and the solvent was removed by rotary evaporator. The resulting solid was washed with 300 mL of petroleum ether (60-90 °C), filtered, and the solid was dried under vacuum at 55 °C to give 0.1440 mol of the target product 3,6-dibromo-9-phenylcarbazole in 87.8% yield.
References
[1] Organic Electronics: physics, materials, applications, 2014, vol. 15, # 11, p. 2667 - 2676
[2] Tetrahedron, 1998, vol. 54, # 42, p. 12707 - 12714
[3] Journal of Materials Chemistry, 2011, vol. 21, # 25, p. 9139 - 9148
[4] Patent: JP2015/63518, 2015, A. Location in patent: Paragraph 0253; 0254
[5] Patent: CN105906612, 2016, A. Location in patent: Paragraph 0051; 0052
3,6-Dibromo-9-phenyl-9H-carbazole Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,6-Dibromo-9-phenyl-9H-carbazole manufacturers
- Product
- 3,6-DIBROMO-9-PHENYLCARBAZOLE 57103-20-5
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 5tons
- Release date
- 2024-12-03
- Product
- 3,6-Dibromo-9-phenylcarbazole 57103-20-5
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.00%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-12
- Product
- 3,6-Dibromo-9-phenyl-9H-carbazole 57103-20-5
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-30