ChemicalBook > CAS DataBase List > 1-Boc-3-piperidone

1-Boc-3-piperidone

Product Name
1-Boc-3-piperidone
CAS No.
98977-36-7
Chemical Name
1-Boc-3-piperidone
Synonyms
TERT-BUTYL 3-OXOPIPERIDINE-1-CARBOXYLATE;N-BOC-3-PIPERIDINONE;N-Boc-3-piperidone;1-BOC-piperidone;1-BOC-3-PIPERIDINONE;1-(TERT-BUTOXYCARBONYL)-3-PIPERIDONE;3-OXO-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;1-Boc-3-Pipe;3-Oxopiperidine;BOC-3-PIPERIDONE
CBNumber
CB8428473
Molecular Formula
C10H17NO3
Formula Weight
199.25
MOL File
98977-36-7.mol
More
Less

1-Boc-3-piperidone Property

Melting point:
35-40 °C (lit.)
Boiling point:
289.8±33.0 °C(Predicted)
Density 
1.099±0.06 g/cm3(Predicted)
Flash point:
>230 °F
storage temp. 
2-8°C
pka
-1.71±0.20(Predicted)
form 
Liquid
color 
Clear colorless
Water Solubility 
It is insoluble in water.
BRN 
5936353
InChI
InChI=1S/C10H17NO3/c1-10(2,3)14-9(13)11-6-4-5-8(12)7-11/h4-7H2,1-3H3
InChIKey
RIFXIGDBUBXKEI-UHFFFAOYSA-N
SMILES
N1(C(OC(C)(C)C)=O)CCCC(=O)C1
CAS DataBase Reference
98977-36-7(CAS DataBase Reference)
More
Less

Safety

Safety Statements 
24/25
WGK Germany 
3
HazardClass 
KEEP COLD
HS Code 
29339900
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
650811
Product name
1-Boc-3-piperidone
Purity
97%
Packaging
25g
Price
$80.7
Updated
2024/03/01
Sigma-Aldrich
Product number
650811
Product name
1-Boc-3-piperidone
Purity
97%
Packaging
5g
Price
$30
Updated
2023/06/20
TCI Chemical
Product number
B3309
Product name
1-(tert-Butoxycarbonyl)-3-piperidone
Purity
>98.0%(GC)
Packaging
5g
Price
$38
Updated
2024/03/01
TCI Chemical
Product number
B3309
Product name
1-(tert-Butoxycarbonyl)-3-piperidone
Purity
>98.0%(GC)
Packaging
25g
Price
$121
Updated
2024/03/01
Alfa Aesar
Product number
L19276
Product name
1-Boc-3-piperidone, 97%
Packaging
1g
Price
$20.65
Updated
2024/03/01
More
Less

1-Boc-3-piperidone Chemical Properties,Usage,Production

Chemical Properties

White to yellow low melting solid

Uses

1-Boc-3-piperidone, is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff.

Synthesis

With 179g compound 3(1-BOC-3-piperidines alcohol) drop in the 2L reaction flask, drop into pimelinketone 1300g, aluminum isopropylate 88g, methylene dichloride 400ml is warming up to 80 ℃, insulation reaction 8h, reaction finishes to be cooled to room temperature, adds 10% sodium hydroxide 200ml, stirring at normal temperature 30min, filter, the filtrate normal pressure reclaims methylene dichloride, reclaim under reduced pressure pimelinketone again, reclaim finish after, add the 300ml dichloromethane extraction three times, it is dry concentrated to merge oil reservoir, gets 1-BOC-3-piperidone crude product.
Refining: with 1-BOC-3-piperidone crude product is that 60pa, temperature are to distill under 104 ~ 105 ℃ the condition at pressure, gets 1-BOC-3-piperidone elaboration 163g, 92.9%.

1-Boc-3-piperidone Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

1-Boc-3-piperidone Suppliers

JW & Y Pharmlab Co., Ltd.
Tel
021-64340559 13651849907;
Fax
021- 64345308
Email
xinyu_shi@jwypharmlab.com.cn
Country
China
ProdList
12041
Advantage
58
Shanghai Hobor Chemical Co., Ltd
Tel
21-21-61026752 13918007836
Fax
021-51685238
Email
sales@hoborchem.com
Country
China
ProdList
394
Advantage
60
Tianchang city Chunfeng Fine Synthetic Material Plant
Tel
0550-7039583 0550-7552998 13905508100
Fax
+86 (550) 702-4815
Email
ycgquan@163.com
Country
China
ProdList
16
Advantage
64
Chengdu Aminotp Pharmaceutical Technology Co.,Ltd.
Tel
028-85755578 18140172005
Fax
028-85755578
Email
sales@aminotp.com
Country
China
ProdList
309
Advantage
58
Jinan Dexinjia Bio&Tech Co., Ltd
Tel
0531-82375886 13001715031
Fax
0531-82375893
Email
3517280075@qq.com
Country
China
ProdList
1205
Advantage
58
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40240
Advantage
62
INTATRADE GmbH
Tel
+49 3493/605464
Fax
+49 3493/605470
Email
sales@intatrade.de
Country
Germany
ProdList
3576
Advantage
66
ITIC MEDCHEM(SUZHOU) CO.,LTD.
Tel
0512-68323967 18015559028
Fax
+86-512-69200360
Email
sales@iticmedchem.com
Country
China
ProdList
416
Advantage
61
Chembest Research Laboratories Limited
Tel
021-20908456
Fax
021-58180499
Email
sales@BioChemBest.com
Country
China
ProdList
6009
Advantage
61
More
Less

View Lastest Price from 1-Boc-3-piperidone manufacturers

Hebei Ganmiao New material Technology Co., LTD
Product
1-Boc-3-Piperidinone 98977-36-7
Price
US $10.00-8.00/kg
Min. Order
1kg
Purity
99.9%
Supply Ability
20ton
Release date
2024-06-07
Anhui Yiao New Material Technology Co., Ltd
Product
1-Boc-3-piperidone 98977-36-7
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1 ton
Release date
2023-11-02
Wuhan Boyuan Import & Export Co., LTD
Product
1-Boc-3-piperidone 98977-36-7
Price
US $20.00-16.00/kg
Min. Order
1kg
Purity
99.50%
Supply Ability
30tons
Release date
2023-06-06

98977-36-7, 1-Boc-3-piperidoneRelated Search:


  • T-BUTYL-3-PIPERIDONE-1-CARBOXYLATE
  • TERT-BUTYL 3-OXOPIPERIDINE-1-CARBOXYLATE
  • N-Boc-3-piperidone
  • N-BOC-3-PIPERIDINONE
  • 3-OXOPIPERIDINE, N-BOC PROTECTED
  • 3-OXO-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER
  • 1-PIPERIDINECARBOXYLIC ACID, 3-OXO-, 1,1-DIMETHYLETHYL ESTER
  • 1-N-BOC-3-PIPERIDONE
  • 1-(TERT-BUTOXYCARBONYL)-3-PIPERIDINONE
  • 1-(TERT-BUTOXYCARBONYL)-3-PIPERIDONE
  • 1-BOC-3-PIPERIDINONE
  • 1-BOC-3-PIPERIDONE
  • 1-BOC-PIPERIDIN-3-ONE
  • BOC-3-PIPERIDONE
  • N-(TERT-BUTOXYCARBONYL)-3-PIPERIDINONE
  • 3-ketopiperidine-1-carboxylic acid tert-butyl ester
  • 3-oxo-1-piperidinecarboxylic acid tert-butyl ester
  • 1-(<i>tert</i>-Butoxycarbonyl)-3-piperidone
  • Piperidin-3-one, N-BOC protected
  • 1-Boc-3-piperidone 98977-36-7
  • 98977-36-7 tert-Butyl 3-oxopiperidine-1-carboxylate
  • 1-BOC-3-oxopiperidine
  • 1,1-Dimethylethyl 3-Oxo-1-Piperidine Carboxylate
  • Tert-butyl-3-oxo-1-piperidinecarboxylate
  • 1-Boc-3-piperidone,97%
  • 1-N-TERT-BUTOXYCARBONYL-3-PIPERIDONE
  • 3-Oxopiperidine, N-BOC protected 97%
  • 1-N-Boc-piperdine-3-one
  • N-BOC-3-piperidone,97%
  • 1-N-Boc-3-Piperidine
  • Piperidin-3-one, N-BOC protected 97%
  • tert-Butyl 3-oxopiperidine-1-carboxylate, 3-Oxopiperidine, N-BOC protected
  • N-(tert-Butoxycarbonyl)-3-piperidone
  • 1-Boc-3-piperidone 97%
  • N - bok - 3 - piperidine ketone
  • 1-Boc-3-piperidone tert-Butyl 3-oxopiperidine-1-carboxylate
  • 3-Oxopiperidine
  • 1-(tert-Butoxycarbonyl)-3-piperidone &gt
  • Ibrutinib Impurity 58
  • 1-BOC-piperidone
  • 3-Oxo-piperidin-1-carboxylic acid tert-butyl ester
  • 1-Boc-3-Pipe
  • 98977-36-7
  • 99175-10-5
  • 9877-36-7
  • 989777-36-7
  • Building Blocks
  • Piperidones
  • Heterocyclic Building Blocks
  • Pyrans, Piperidines & Piperazines
  • Building Blocks
  • Heterocyclic Building Blocks
  • Piperidones
  • Piperidine
  • Piperidines
  • Pharmaceutical Intermediates
  • pharmacetical
  • Pyrans, Piperidines &Piperazines