ChemicalBook > CAS DataBase List > 1-Boc-3-piperidone

1-Boc-3-piperidone

Product Name
1-Boc-3-piperidone
CAS No.
98977-36-7
Chemical Name
1-Boc-3-piperidone
Synonyms
TERT-BUTYL 3-OXOPIPERIDINE-1-CARBOXYLATE;N-BOC-3-PIPERIDINONE;N-Boc-3-piperidone;1-BOC-piperidone;1-BOC-3-PIPERIDINONE;1-(TERT-BUTOXYCARBONYL)-3-PIPERIDONE;3-OXO-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;1-Boc-3-Pipe;3-Oxopiperidine;BOC-3-PIPERIDONE
CBNumber
CB8428473
Molecular Formula
C10H17NO3
Formula Weight
199.25
MOL File
98977-36-7.mol
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1-Boc-3-piperidone Property

Melting point:
35-40 °C (lit.)
Boiling point:
289.8±33.0 °C(Predicted)
Density 
1.099±0.06 g/cm3(Predicted)
Flash point:
>230 °F
storage temp. 
2-8°C
pka
-1.71±0.20(Predicted)
form 
Liquid
color 
Clear colorless
Water Solubility 
It is insoluble in water.
BRN 
5936353
InChI
InChI=1S/C10H17NO3/c1-10(2,3)14-9(13)11-6-4-5-8(12)7-11/h4-7H2,1-3H3
InChIKey
RIFXIGDBUBXKEI-UHFFFAOYSA-N
SMILES
N1(C(OC(C)(C)C)=O)CCCC(=O)C1
CAS DataBase Reference
98977-36-7(CAS DataBase Reference)
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Safety

Safety Statements 
24/25
WGK Germany 
3
HazardClass 
KEEP COLD
HS Code 
29339900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
650811
Product name
1-Boc-3-piperidone
Purity
97%
Packaging
25g
Price
$80.7
Updated
2024/03/01
Sigma-Aldrich
Product number
650811
Product name
1-Boc-3-piperidone
Purity
97%
Packaging
5g
Price
$30
Updated
2023/06/20
TCI Chemical
Product number
B3309
Product name
1-(tert-Butoxycarbonyl)-3-piperidone
Purity
>98.0%(GC)
Packaging
5g
Price
$38
Updated
2024/03/01
TCI Chemical
Product number
B3309
Product name
1-(tert-Butoxycarbonyl)-3-piperidone
Purity
>98.0%(GC)
Packaging
25g
Price
$121
Updated
2024/03/01
Alfa Aesar
Product number
L19276
Product name
1-Boc-3-piperidone, 97%
Packaging
1g
Price
$20.65
Updated
2024/03/01
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1-Boc-3-piperidone Chemical Properties,Usage,Production

Chemical Properties

White to yellow low melting solid

Uses

1-Boc-3-piperidone, is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff.

Synthesis

With 179g compound 3(1-BOC-3-piperidines alcohol) drop in the 2L reaction flask, drop into pimelinketone 1300g, aluminum isopropylate 88g, methylene dichloride 400ml is warming up to 80 ℃, insulation reaction 8h, reaction finishes to be cooled to room temperature, adds 10% sodium hydroxide 200ml, stirring at normal temperature 30min, filter, the filtrate normal pressure reclaims methylene dichloride, reclaim under reduced pressure pimelinketone again, reclaim finish after, add the 300ml dichloromethane extraction three times, it is dry concentrated to merge oil reservoir, gets 1-BOC-3-piperidone crude product.
Refining: with 1-BOC-3-piperidone crude product is that 60pa, temperature are to distill under 104 ~ 105 ℃ the condition at pressure, gets 1-BOC-3-piperidone elaboration 163g, 92.9%.

1-Boc-3-piperidone Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Boc-3-piperidone Suppliers

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View Lastest Price from 1-Boc-3-piperidone manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
1-Boc-3-piperidone 98977-36-7
Price
US $0.00-0.00/KG
Min. Order
1g
Purity
99%
Supply Ability
2000tons
Release date
2019-12-31
Shanghai Joiny Pharmaceutical Co.,LTD
Product
1-Boc-3-piperidone 98977-36-7
Price
US $0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
1000kg
Release date
2024-12-05
Hebei Ganmiao New material Technology Co., LTD
Product
1-Boc-3-Piperidinone 98977-36-7
Price
US $10.00-8.00/kg
Min. Order
1kg
Purity
99.9%
Supply Ability
20ton
Release date
2024-06-07

98977-36-7, 1-Boc-3-piperidoneRelated Search:

tert-Butyl peroxybenzoate Buprofezin Butylparaben 4,4-Piperidinediol hydrochloride 3-Piperidinone 2-Piperidone Butyl benzoate tert-Butyl carbazate tert-Butanol Cyhalofop-butyl Diisobutyl phthalate Haloperidol Butyl acrylate 2-Butoxyethanol RESMETHRIN Butyl acetate Isobutyl chloroformate N-(tert-Butoxycarbonyl)-4-piperidone

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  • 1-N-Boc-3-Piperidine
  • Piperidin-3-one, N-BOC protected 97%
  • tert-Butyl 3-oxopiperidine-1-carboxylate, 3-Oxopiperidine, N-BOC protected
  • N-(tert-Butoxycarbonyl)-3-piperidone
  • 1-Boc-3-piperidone 97%
  • N - bok - 3 - piperidine ketone
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  • 98977-36-7
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  • 989777-36-7
  • Building Blocks
  • Piperidones
  • Heterocyclic Building Blocks
  • Pyrans, Piperidines & Piperazines
  • Building Blocks
  • Heterocyclic Building Blocks
  • Piperidones
  • Piperidine
  • Piperidines
  • Pharmaceutical Intermediates
  • pharmacetical
  • Pyrans, Piperidines &Piperazines