4-BROMO-8-METHYLQUINOLINE

Product Name: 4-BROMO-8-METHYLQUINOLINE
CAS No.: 36075-68-0
Chemical Name: 4-BROMO-8-METHYLQUINOLINE
Synonyms: 4-BROMO-8-METHYLQUINOLINE;Quinoline, 4-bromo-8-methyl-;4-BROMO-8-METHYLQUINOLINE ISO 9001：2015 REACH
CBNumber: CB8431765
Molecular Formula: C10H8BrN
Formula Weight: 222.08
MOL File: 36075-68-0.mol

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4-BROMO-8-METHYLQUINOLINE Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Off-white to light yellow Solid
InChI: InChI=1S/C10H8BrN/c1-7-3-2-4-8-9(11)5-6-12-10(7)8/h2-6H,1H3
InChIKey: IDGLXERCZWXTCV-UHFFFAOYSA-N
SMILES: N1C2C(=CC=CC=2C)C(Br)=CC=1

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B697688
Product name: 4-Bromo-8-methylquinoline
Packaging: 250mg
Price: $75
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0104722
Product name: 4-BROMO-8-METHYLQUINOLINE
Purity: 95.00%
Packaging: 5MG
Price: $503.11
Updated: 2021/12/16

AK Scientific

Product number: V5488
Product name: 4-Bromo-8-methylquinoline
Packaging: 10g
Price: $851
Updated: 2021/12/16

Ambeed

Product number: A213520
Product name: 4-Bromo-8-methylquinoline
Purity: 98%
Packaging: 100mg
Price: $45
Updated: 2021/12/16

Ambeed

Product number: A213520
Product name: 4-Bromo-8-methylquinoline
Purity: 98%
Packaging: 250mg
Price: $71
Updated: 2021/12/16

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4-BROMO-8-METHYLQUINOLINE Chemical Properties,Usage,Production

Synthesis

23432-44-2

36075-68-0

General procedure for the synthesis of 4-bromo-8-methylquinoline from 8-methyl-4-hydroxyquinoline: To a 100 mL round-bottomed flask was added 8-methyl-4-hydroxyquinoline (500 mg, 3.14 mmol, 1.00 equiv) and N,N-dimethylformamide (20 mL). Phosphorus tribromide (851 mg, 3.14 mmol, 1.20 eq.) was added slowly and dropwise with stirring at room temperature. The reaction mixture was stirred continuously for 15 hours at room temperature. Upon completion of the reaction, the reaction was quenched with an ice-water mixture (100 mL). Subsequently, the pH of the reaction solution was adjusted to 10 with 2 mol/L NaOH solution.The precipitated solid was collected by filtration to give 660 mg of 4-bromo-8-methylquinoline in 95% yield as a light yellow solid. Mass spectra (electrospray ionization, m/z) [M + 1]: 222 and 224.

References

[1] Patent: WO2017/205296, 2017, A1. Location in patent: Paragraph 669

4-BROMO-8-METHYLQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMO-8-METHYLQUINOLINE Suppliers

China 46 India 1 United States 7 Global 54

Hangzhou J&H Chemical Co., Ltd.

Tel: 0571-87396432
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Energy Chemical

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Aikon International Limited

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SHANGHAI FDC-CHEMICAL CO.,LTD

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36075-68-0, 4-BROMO-8-METHYLQUINOLINERelated Search:

4-BROMO-7-NITROQUINOLINE 4-bromo-1H-pyrazolo[3,4-b]pyridine 4-BROMO-8-FLUOROQUINOLINE 4-BROMO-8-HYDROXYQUINOLINE 4-BROMO-8-CHLOROQUINOLINE 4-BROMO-8-METHOXYQUINOLINE 4-BROMO-8-TRIFLUOROMETHYLQUINOLINE 2,8-BIS(TRIFLUOROMETHYL)-4-BROMOQUINOLINE 4-BROMO-2,8-DIMETHYLQUINOLINE 4-BROMO-6-CHLORO-8-METHYLQUINOLINE 4-BROMO-8-CYANOQUINOLINE 4-BROMO-8-METHYLQUINOLINE

4-BROMO-8-METHYLQUINOLINE

Quinoline, 4-bromo-8-methyl-

4-BROMO-8-METHYLQUINOLINE ISO 9001：2015 REACH

36075-68-0