1-Methylpyrrolidine-2-methanol
- Product Name
- 1-Methylpyrrolidine-2-methanol
- CAS No.
- 3554-65-2
- Chemical Name
- 1-Methylpyrrolidine-2-methanol
- Synonyms
- Einecs 222-608-7;1-METHYL-2-PYRROLIDINEMETHANOL;1-Methylpyrrolidine-2-methanol;2-PyrrolidineMethanol,1-Methyl-;(1-METHYLPYRROLIDIN-2-YL)METHANOL;(1-methyl-2-pyrrolidinyl)methanol;[(2S)-1-methyl-2-pyrrolidinyl]methanol
- CBNumber
- CB8448141
- Molecular Formula
- C6H13NO
- Formula Weight
- 115.17
- MOL File
- 3554-65-2.mol
1-Methylpyrrolidine-2-methanol Property
- Boiling point:
- 67-68 °C(Press: 12 Torr)
- Density
- 0.973±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- form
- solid
- pka
- 14.77±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
- InChI
- 1S/C6H13NO/c1-7-4-2-3-6(7)5-8/h6,8H,2-5H2,1H3
- InChIKey
- VCOJPHPOVDIRJK-UHFFFAOYSA-N
- SMILES
- CN1CCCC1CO
- CAS DataBase Reference
- 3554-65-2(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- R422
- Product name
- 1-Methylpyrrolidine-2-methanol
- Packaging
- 1g
- Price
- $13
- Updated
- 2021/12/16
- Product number
- 065627
- Product name
- (1-Methylpyrrolidin-2-yl)methanol
- Packaging
- 5g
- Price
- $29
- Updated
- 2021/12/16
- Product number
- 065627
- Product name
- (1-Methylpyrrolidin-2-yl)methanol
- Packaging
- 25g
- Price
- $89
- Updated
- 2021/12/16
- Product number
- J96213
- Product name
- 1-Methylpyrrolidine-2-methanol
- Packaging
- 25g
- Price
- $90
- Updated
- 2021/12/16
- Product number
- CHM0078581
- Product name
- 1-METHYLPYRROLIDINE-2-METHANOL
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $823.44
- Updated
- 2021/12/16
1-Methylpyrrolidine-2-methanol Chemical Properties,Usage,Production
Definition
ChEBI: 1-Methylpyrrolidine-2-methanol is a N-alkylpyrrolidine.
Synthesis
50-00-0
498-63-5
3554-65-2
a) A mixture of (RS)-pyrrolidin-2-ylmethanol (1.00 g, 9.90 mmol, 1.0 eq.), 35% aqueous formaldehyde (10 mL) and 10% (1-methylpyrrolidin-2-yl)methanol was reacted with Pd/C (200 mg) for 18 hours with stirring under hydrogen atmosphere. Upon completion of the reaction, the mixture was filtered through a pad of diatomaceous earth and the filtrate was concentrated under reduced pressure and subsequently purified by silica gel column chromatography (eluent: 20% methanol/chloroform) to give a colorless liquid product (650 mg, 56% yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 3.65 (dd, J = 10.0, 3.6 Hz, 1H), 3.43 (dd, J = 10.8, 2.0 Hz, 1H), 3.10-3.05 (m, 1H), 2.40-2.35 (m, 1H), 2.33 (s, 3H), 2.32-2.25 (m , 1H), 1.93-1.68 (m, 4H); mass spectrum (APCI+): m/z 116 [M + H]+.
References
[1] Patent: WO2012/127212, 2012, A1. Location in patent: Page/Page column 101
1-Methylpyrrolidine-2-methanol Preparation Products And Raw materials
Raw materials
Preparation Products
1-Methylpyrrolidine-2-methanol Suppliers
- Tel
- 821-50328103-801 18930552037
- Fax
- 86-21-50328109
- 3bsc@sina.com
- Country
- China
- ProdList
- 15838
- Advantage
- 69
- Tel
- 400-021-7337 2355568890
- Fax
- 0086-21-50182339
- sales@demochem.com
- Country
- China
- ProdList
- 2572
- Advantage
- 57
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44802
- Advantage
- 61
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9309
- Advantage
- 66
- Tel
- 001-857-928-2050 or 1-888-588-9418
- Fax
- 001-617-206-9595
- sales@chemreagents.com
- Country
- United States
- ProdList
- 10186
- Advantage
- 62
- Tel
- 021-54306202 13764082696
- info@hanhongsci.com
- Country
- China
- ProdList
- 42934
- Advantage
- 64
- Tel
- 010-82954736 13391601435
- sales@isomersyn.com
- Country
- China
- ProdList
- 3295
- Advantage
- 57
- Tel
- 13355009207 13355009207
- Fax
- 0539-6365991
- 3007715519@qq.com
- Country
- China
- ProdList
- 18729
- Advantage
- 57
- Tel
- 18270980682
- Fax
- 021 51613951
- mlcheng@sunwaypharm.cn
- Country
- China
- ProdList
- 8667
- Advantage
- 57
View Lastest Price from 1-Methylpyrrolidine-2-methanol manufacturers
- Product
- 1-Methyl-2-pyrrolidineMethanol 3554-65-2
- Price
- US $1.00/Kg
- Min. Order
- 1Kg
- Purity
- 98%
- Supply Ability
- 20T
- Release date
- 2024-07-19
- Product
- 1-Methylpyrrolidine-2-methanol 3554-65-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2020-01-08