Ethyl 4-(aminomethyl)benzoate
- Product Name
- Ethyl 4-(aminomethyl)benzoate
- CAS No.
- 366-84-7
- Chemical Name
- Ethyl 4-(aminomethyl)benzoate
- Synonyms
- RARECHEM AL BW 1094;ethyl 4-(aminomethyl)benzoate;4-AMINOMETHYL-BENZOIC ACID ETHYL ESTER;Benzoic acid, 4-(aminomethyl)-, ethyl ester
- CBNumber
- CB8491930
- Molecular Formula
- C10H13NO2
- Formula Weight
- 179.22
- MOL File
- 366-84-7.mol
Ethyl 4-(aminomethyl)benzoate Property
- Melting point:
- 215 °C(Solv: ethanol (64-17-5))
- Boiling point:
- 293.9±23.0 °C(Predicted)
- Density
- 1.093±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- pka
- 8.69±0.10(Predicted)
- Appearance
- Light yellow to yellow Liquid
N-Bromosuccinimide Price
- Product number
- 3372AL
- Product name
- Ethyl4-(aminomethyl)benzoate
- Packaging
- 5g
- Price
- $691
- Updated
- 2021/12/16
- Product number
- 144382
- Product name
- Ethyl 4-(aminomethyl)benzoate
- Purity
- 95%
- Packaging
- 1g
- Price
- $731
- Updated
- 2021/12/16
- Product number
- CHM0122074
- Product name
- ETHYL 4-(AMINOMETHYL)BENZOATE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $765.23
- Updated
- 2021/12/16
- Product number
- 3372AL
- Product name
- Ethyl4-(aminomethyl)benzoate
- Packaging
- 10g
- Price
- $1011
- Updated
- 2021/12/16
- Product number
- CHM0122074
- Product name
- ETHYL 4-(AMINOMETHYL)BENZOATE
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $1065.66
- Updated
- 2021/12/16
Ethyl 4-(aminomethyl)benzoate Chemical Properties,Usage,Production
Synthesis
56-91-7
64-17-5
366-84-7
Example 1: Preparation of ethyl 4-(aminomethyl)benzoate Add 7.5 g (50 mmol) of 4-(aminomethyl)benzoic acid to a 250 mL three-necked round-bottomed flask. 100mL of anhydrous ethanol was added. Under the condition of ice bath, 20.8 g (175 mmol) of thionyl chloride was slowly added dropwise, and after completion of the dropwise addition, the reaction was stirred at room temperature for 30 min, followed by heating and refluxing for 4 hours. Upon completion of the reaction, the heating was stopped and the ethanol was removed by distillation under reduced pressure to give a white solid product. The resulting solid was dissolved in 150 mL of ethyl acetate, and the pH was adjusted to 7-8 by slowly adding 35% aqueous sodium hydroxide under the condition of an ice bath. the organic layer and the aqueous layer were separated, and the organic layer was washed with saturated saline three times, each time 30 mL. the organic layer was dried with anhydrous sodium sulfate, filtered, and concentrated to give a yellow solid product in 90% yield.
References
[1] Patent: CN104016942, 2016, B. Location in patent: Paragraph 0090; 0091; 0092
[2] Journal of the American Chemical Society, 1943, vol. 65, p. 2281,2283
[3] Organic and Biomolecular Chemistry, 2013, vol. 11, # 36, p. 6023 - 6028
[4] Journal of the American Society for Mass Spectrometry, 2018, vol. 29, # 4, p. 694 - 703
Ethyl 4-(aminomethyl)benzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Ethyl 4-(aminomethyl)benzoate manufacturers
- Product
- 4-AMINOMETHYL-BENZOIC ACID ETHYL ESTER 366-84-7
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02