1-Naphthoyl chloride
- Product Name
- 1-Naphthoyl chloride
- CAS No.
- 879-18-5
- Chemical Name
- 1-Naphthoyl chloride
- Synonyms
- SKL745;SKL1287;Naphthoyl chlorid;1-Napthoylchloride;TIMTEC-BB SBB006741;1-NAPHTHOYL CHLORIDE;1-NAPHTOHYL CHLORIDE;1-NaphthoylChloride>ALPHA-NAPHTHOYL CHLORIDE;1-Naphthoyl chloride,99%
- CBNumber
- CB8735331
- Molecular Formula
- C11H7ClO
- Formula Weight
- 190.63
- MOL File
- 879-18-5.mol
1-Naphthoyl chloride Property
- Melting point:
- 16-19 °C (lit.)
- Boiling point:
- 190 °C/35 mmHg (lit.)
- Density
- 1.265 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.652(lit.)
- Flash point:
- >230 °F
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- solubility
- Chloroform (Slightly)
- form
- Powder, Flakes or Crystals
- Specific Gravity
- 1.265
- color
- White to almost white
- Water Solubility
- Reacts with water.
- Sensitive
- Moisture Sensitive
- BRN
- 775785
- Stability:
- Stable. Incompatible with water, moisture, strong oxidizing agents, bases.
- CAS DataBase Reference
- 879-18-5(CAS DataBase Reference)
- NIST Chemistry Reference
- 1-Naphthalenecarbonyl chloride(879-18-5)
- EPA Substance Registry System
- 1-Naphthalenecarbonyl chloride (879-18-5)
Safety
- Hazard Codes
- C
- Risk Statements
- 34-37-14
- Safety Statements
- 26-36/37/39-45-28A-60-30-20-8
- RIDADR
- UN 3261 8/PG 2
- WGK Germany
- 3
- F
- 21
- Hazard Note
- Corrosive
- TSCA
- Yes
- HazardClass
- 8
- PackingGroup
- II
- HS Code
- 29163990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P363Wash contaminated clothing before reuse.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 250252
- Product name
- 1-Naphthoyl chloride
- Purity
- 97%
- Packaging
- 10g
- Price
- $71.7
- Updated
- 2025/07/31
- Product number
- 250252
- Product name
- 1-Naphthoyl chloride
- Purity
- 97%
- Packaging
- 50g
- Price
- $194
- Updated
- 2025/07/31
- Product number
- N0047
- Product name
- 1-Naphthoyl Chloride
- Packaging
- 25G
- Price
- $95
- Updated
- 2025/07/31
- Product number
- N497040
- Product name
- 1-Naphthoyl Chloride
- Packaging
- 10g
- Price
- $45
- Updated
- 2021/12/16
- Product number
- J52988
- Product name
- 1-Naphthoyl Chloride
- Packaging
- 5g
- Price
- $15
- Updated
- 2021/12/16
1-Naphthoyl chloride Chemical Properties,Usage,Production
Chemical Properties
Low melting solid/Liquid
Uses
1-Naphthoyl chloride has been used as derivatization reagent in analysis of short-chained dodecyl alcohol ethoxylates and dodecyl alcohol by solid-phase extraction combined with dispersive liquid-liquid micro extraction method, as fluorescent labeling reagent in determination of T-2 and HT-2 toxins by HPLC with fluorescence detection, in Arndt-Eistert synthesis in the presence of trimethylsilyldiazomethane and in preparation of 2-ethyl-1-pentyl-3-(1-naphthoyl)indole.
Uses
1-Naphthoyl chloride has been used:
- as derivatization reagent in analysis of short-chained dodecyl alcohol ethoxylates and dodecyl alcohol by solid-phase extraction combined with dispersive liquid-liquid microextraction method
- as fluorescent labeling reagent in determination of T-2 and HT-2 toxins by HPLC with fluorescence detection
- in Arndt-Eistert synthesis in the presence of trimethylsilyldiazomethane
- in preparation of 2-ethyl-1-pentyl-3-(1-naphthoyl)indole
Synthesis
86-55-5
879-18-5
General method: Method A: 1-Naphthalenecarboxylic acid (5.8 mmol) was dissolved in dry toluene (40 mL) and thionyl chloride (8.0 mmol) was added. After refluxing the reaction for 2 hours, evaporate under reduced pressure to remove the solvent and excess thionyl chloride to give 1-naphthalenecarboxylic acid as a colorless liquid in quantitative yield. Upon cooling, the product formed colorless needle-like crystals with a melting point of 18-19°C (literature value 26°C [54]). 1-Naphthalenecarbonyl chloride (5.8 mmol), triethylamine (8.7 mmol) and the corresponding substituted aniline (5.8 mmol) were dissolved in anhydrous dichloromethane (30 mL), and the mixture was stirred at room temperature for 12 hours. After completion of the reaction, the solvent was removed by evaporation under reduced pressure, the solid residue was washed with 10% hydrochloric acid solution, the crude product was recrystallized with isopropanol and decolorized by the addition of activated carbon.
References
[1] Molecules, 2014, vol. 19, # 7, p. 10386 - 10409
[2] Patent: WO2009/91324, 2009, A1. Location in patent: Page/Page column 29
[3] Organic Letters, 2005, vol. 7, # 3, p. 367 - 369
[4] Chemische Berichte, 1905, vol. 38, p. 180
[5] Chemische Berichte, 1868, vol. 1, p. 42
1-Naphthoyl chloride Preparation Products And Raw materials
Raw materials
Preparation Products
1-Naphthoyl chloride Suppliers
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- The Netherlands
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View Lastest Price from 1-Naphthoyl chloride manufacturers
- Product
- 1-Naphthoyl chloride 879-18-5
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2024-11-08
- Product
- 1-Naphthoyl chloride 879-18-5
- Price
- US $590.00-330.00/kg
- Min. Order
- 1kg
- Purity
- 99% Purity (What/sapp: +86 18145728414)
- Supply Ability
- 1000 Tons/Month
- Release date
- 2023-06-29
- Product
- 1-Naphthoyl chloride 879-18-5
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99.99%
- Supply Ability
- 20 tons
- Release date
- 2025-04-08