ChemicalBook > CAS DataBase List > 2-BROMO-4-METHOXY-PHENYLAMINE

2-BROMO-4-METHOXY-PHENYLAMINE

Product Name
2-BROMO-4-METHOXY-PHENYLAMINE
CAS No.
32338-02-6
Chemical Name
2-BROMO-4-METHOXY-PHENYLAMINE
Synonyms
SKL231;2-Bromo-p-anisidine;4-Amino-3-bromoanisole;2-BROMO-4-METHOXYANILINE;2-Bromo-4-methoxyaniline 95%;2-BROMO-4-METHOXY-PHENYLAMINE;BenzenaMine, 2-broMo-4-Methoxy-;4-Amino-3-bromoanisole, 2-Bromo-p-anisidine;4-AMino-3-broMoanisole[2-BroMo-4-Methoxyaniline];N2,N4-diethyl-6-ethylsulfanyl-1,3,5-triazine-2,4-diamine
CBNumber
CB8840949
Molecular Formula
C7H8BrNO
Formula Weight
202.05
MOL File
32338-02-6.mol
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2-BROMO-4-METHOXY-PHENYLAMINE Property

Melting point:
64 °C
Boiling point:
76-98 °C(Press: 2 Torr)
Density 
1.531±0.06 g/cm3(Predicted)
storage temp. 
2-8°C(protect from light)
solubility 
Chloroform (Slightly), DMSO (Slightly)
form 
liquid
pka
3.14±0.10(Predicted)
color 
Clear, dark red
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Safety

HazardClass 
IRRITANT
HS Code 
2922290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B699470
Product name
2-Bromo-4-methoxyaniline
Packaging
10g
Price
$250
Updated
2021/12/16
TRC
Product number
B699470
Product name
2-Bromo-4-methoxyaniline
Packaging
25g
Price
$530
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049713
Product name
2-BROMO-4-METHOXY-PHENYLAMINE
Purity
95.00%
Packaging
1G
Price
$733.43
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049713
Product name
2-BROMO-4-METHOXY-PHENYLAMINE
Purity
95.00%
Packaging
5G
Price
$1241.63
Updated
2021/12/16
Apolloscientific
Product number
OR61502
Product name
2-Bromo-4-methoxyaniline
Purity
96%
Packaging
25g
Price
$186
Updated
2021/12/16
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2-BROMO-4-METHOXY-PHENYLAMINE Chemical Properties,Usage,Production

Uses

2-Bromo-4-methoxyaniline is a useful reagent and reactant in organometallics, and organic reactions.

Synthesis

104-94-9

32338-02-6

General procedure for the synthesis of 2-bromo-4-methoxyaniline from 4-methoxyaniline: N-bromosuccinimide (NBS, 152 g, 853 mmol) was added batchwise to a tetrahydrofuran (THF, 3 L) solution of 4-methoxyaniline (100 g, 812 mmol) at -10 °C, keeping the temperature constant and stirring continuously for 30 min. After completion of the reaction, the mixture was concentrated under reduced pressure. The residue was purified by column chromatography (eluent: petroleum ether/ethyl acetate, 15:1, v/v) to afford the target product 2-bromo-4-methoxyaniline as a red oil (30.58 g, 18.6% yield). The nuclear magnetic resonance hydrogen spectrum (1H NMR, 400 MHz, CDCl3) data were as follows: δ = 7.01 (d, J = 2.4 Hz, 1H), 6.74-6.70 (m, 2H), 3.85-3.74 (m, 2H), 3.73 (s, 3H).

References

[1] Russian Journal of Applied Chemistry, 2009, vol. 82, # 9, p. 1570 - 1576
[2] Journal of the Chilean Chemical Society, 2011, vol. 56, # 4, p. 863 - 865
[3] Organic Letters, 2006, vol. 8, # 19, p. 4291 - 4293
[4] Journal of the Brazilian Chemical Society, 2010, vol. 21, # 3, p. 496 - 501
[5] Synthetic Communications, 2010, vol. 40, # 6, p. 868 - 876

2-BROMO-4-METHOXY-PHENYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-4-METHOXY-PHENYLAMINE Suppliers

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View Lastest Price from 2-BROMO-4-METHOXY-PHENYLAMINE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
2-broMo-4-Methoxyaniline 32338-02-6
Price
US $0.01-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000KG
Release date
2019-12-30
Shaanxi Dideu Medichem Co. Ltd
Product
2-Bromo-4-methoxyaniline 32338-02-6
Price
US $1.00-1.00/KG
Min. Order
1KG
Purity
99%+
Supply Ability
100 tons
Release date
2019-12-26
Career Henan Chemical Co
Product
2-BROMO-4-METHOXY-PHENYLAMINE 32338-02-6
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-07-11

32338-02-6, 2-BROMO-4-METHOXY-PHENYLAMINERelated Search:

2,6-Dibromo-4-(trifluoromethoxy)aniline THIFLUZAMIDE 2-Bromo-4-trifluoromethoxyaniline 4-BROMO-3-METHOXY-PHENYLAMINE 4-BROMO-2-METHOXY-PHENYLAMINE 5-BROMO-6-NITROBENZO(1,3)DIOXOLE 1-BROMO-4,5-DIMETHOXY-2-NITROBENZENE 6-BROMO-7-NITRO-2,3-DIHYDRO-1,4-BENZODIOXINE 1-[2-BROMO-4-(TRIFLUOROMETHOXY)PHENYL]-2,5-DIMETHYL-1H-PYRROLE 2-Bromo-6-nitro-4-trifluoromethoxyaniline 3-BROMO-5-METHOXY-2,6-DINITRO-BENZOIC ACID METHYL ESTER BENZYL-(2-DIBENZYLAMINO)-3-BROMO-5-METHOXYBENZOATE 3-BROMO-5-BENZYLOXY-2,6-DINITROBENZOIC ACID BENZYL ESTER 2-BROMO-4-(TRIFLUOROMETHOXY)ANILINE HYDROCHLORIDE N-(7-BROMO-2,3-DIHYDRO-1,4-BENZODIOXIN-6-YL)-2-CHLOROACETAMIDE BUTTPARK 50\07-89 BUTTPARK 35\07-02 IFLAB-BB F2124-0435

  • 2-BROMO-4-METHOXY-PHENYLAMINE
  • 2-Bromo-p-anisidine
  • 2-N,4-N-diethyl-6-ethylsulfanyl-1,3,5-triazine-2,4-diamine
  • ethyl-[4-(ethylamino)-6-(ethylthio)-s-triazin-2-yl]amine
  • N2,N4-diethyl-6-ethylsulfanyl-1,3,5-triazine-2,4-diamine
  • 2-Bromo-4-methoxyaniline 95%
  • 4-Amino-3-bromoanisole, 2-Bromo-p-anisidine
  • 4-AMino-3-broMoanisole[2-BroMo-4-Methoxyaniline]
  • 2-BROMO-4-METHOXYANILINE
  • BenzenaMine, 2-broMo-4-Methoxy-
  • SKL231
  • 4-Amino-3-bromoanisole
  • 32338-02-6
  • Anilines, Aromatic Amines and Nitro Compounds