4-IODO-3-METHYL-PHENOL
- Product Name
- 4-IODO-3-METHYL-PHENOL
- CAS No.
- 133921-27-4
- Chemical Name
- 4-IODO-3-METHYL-PHENOL
- Synonyms
- 4-Iodo-3-methyL;3-methyl-4-iodophenol;4-IODO-3-METHYL-PHENOL;4-Iodine-3-methylphenol;Phenol, 4-iodo-3-methyl-
- CBNumber
- CB8847670
- Molecular Formula
- C7H7IO
- Formula Weight
- 234.03
- MOL File
- 133921-27-4.mol
4-IODO-3-METHYL-PHENOL Property
- Boiling point:
- 276.7±28.0 °C(Predicted)
- Density
- 1.854±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- 9.46±0.18(Predicted)
- Appearance
- Off-white to light brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- I709053
- Product name
- 4-Iodo-3-methylphenol
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- I709053
- Product name
- 4-Iodo-3-methylphenol
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 075231
- Product name
- 4-Iodo-3-methylphenol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $20
- Updated
- 2021/12/16
- Product number
- 078711
- Product name
- 4-Iodo-3-methylphenol
- Purity
- 97%
- Packaging
- 1g
- Price
- $21
- Updated
- 2021/12/16
- Product number
- 075231
- Product name
- 4-Iodo-3-methylphenol
- Purity
- 95+%
- Packaging
- 5g
- Price
- $72
- Updated
- 2021/12/16
4-IODO-3-METHYL-PHENOL Chemical Properties,Usage,Production
Synthesis
2835-99-6
133921-27-4
Example 25: Synthesis of (E)-4-((2-(4-((Z)-1-(4-hydroxyphenyl)-2-phenylbut-1-en-1-yl)-3-methylphenoxy)ethyl)amino)-N,N-dimethylbut-2-enamide Step-1: Synthesis of 4-iodo-3-methylphenol 4-Amino-3-methylphenol (10 g, 81 mmol) was dissolved in THF (45 mL) and cooled to 0°C. Under stirring, 3M HCl (35 mL) was slowly added, followed by NaNO2 (6.1 g, 89 mmol), and the reaction was carried out for 10 min. Next, an aqueous solution of potassium iodide (53.89 g, 166 mmol) (140 mL) was added dropwise to the reaction mixture, and stirring was continued for 15 min by keeping 0°C. After completion of the reaction, the reaction mixture was extracted with EtOAc. The organic layer was washed with water and brine sequentially and concentrated under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography (230-400 mesh) to afford the title compound 4-iodo-3-methylphenol (9 g, 47% yield) using 10% EtOAc in hexane solution as eluent.
References
[1] Patent: WO2016/196342, 2016, A1. Location in patent: Page/Page column 129
[2] Patent: US6689922, 2004, B1. Location in patent: Page column 85
[3] Journal of the Chemical Society, 1951, p. 1184,1186
[4] Patent: US6562823, 2003, B1
4-IODO-3-METHYL-PHENOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-IODO-3-METHYL-PHENOL manufacturers
- Product
- 4-IODO-3-METHYL-PHENOL 133921-27-4
- Price
- US $1.30/g
- Min. Order
- 1g
- Purity
- 98%
- Supply Ability
- 1kg,10kg,100kg
- Release date
- 2020-10-28